Related Manuals for Hach Polymetron 9586
Summary of Contents for Hach Polymetron 9586
- Page 1 DOC023.52.93069 Polymetron 9586 Oxygen Scavenger Analyzer 05/2018, Edition 6 User Manual...
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Page 3: Table Of Contents
Table of Contents Specifications ......................3 General information ....................4 Safety information ......................4 Use of hazard information ..................5 Precautionary labels .................... 5 EMC compliance statement (Korea) ..............5 Certification ......................6 Product components ....................6 Product overview ......................7 Installation ........................ - Page 4 Table of Contents Calibration with the process sample ..............27 Exit calibration procedure ................... 28 Change calibration options ................. 28 Reset calibration options ..................29 Maintenance ....................... 29 Cleaning and decontamination .................. 29 Fuse replacement ...................... 29 Battery replacement ....................29 Troubleshooting .......................
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Page 5: Specifications
Specifications Specifications are subject to change without notice. Panel Specification Details Dimensions 817 x 300 x 140 mm (32.2 x 11.8 x 5.5 in) Weight 14.6 kg (32.15 lbs) Sample flow rate 10—15 liters/hour Working pressure 0.5—6 bar (7—87 psi) Ambient temperature 0—60 °C (-32—140 °F) Relative humidity... -
Page 6: General Information
Specification Details Power requirements AC powered controller: 100-240 VAC ±10%, 50/60 Hz; Power 50 VA with 7 W sensor/network module load, 100 VA with 28 W sensor/network module load (optional Modbus, RS232/RS485, Profibus DPV1 or HART network connection). 24 VDC powered controller: 24 VDC—15%, + 20%; Power 15 W with 7 W sensor/network module load, 40 W with 28 W sensor/network module load (optional Modbus, RS232/RS485, Profibus DPV1 or HART network connection). -
Page 7: Use Of Hazard Information
Use of hazard information D A N G E R Indicates a potentially or imminently hazardous situation which, if not avoided, will result in death or serious injury. W A R N I N G Indicates a potentially or imminently hazardous situation which, if not avoided, could result in death or serious injury. -
Page 8: Certification
Certification Canadian Radio Interference-Causing Equipment Regulation, IECS-003, Class A: Supporting test records reside with the manufacturer. This Class A digital apparatus meets all requirements of the Canadian Interference-Causing Equipment Regulations. FCC Part 15, Class "A" Limits Supporting test records reside with the manufacturer. The device complies with Part 15 of the FCC Rules. -
Page 9: Product Overview
Product overview The analyzer is designed to continuously measure the amount of oxygen scavengers (hydrazine or carbohydrazide) in water. Figure 1 Front and rear view 1 Controller 6 Chemical zero cartridge (option) 2 Measuring cell 7 Pressure regulator 3 Chemical zero on/off (option) 8 Sample in, 4/6 mm tube 4 Flow meter 9 Sample drain, 6/8 mm tube, atmospheric pressure... -
Page 10: Analyzer Mounting
Analyzer mounting C A U T I O N Personal injury hazard. Instruments or components are heavy. Use assistance to install or move. Make sure that the wall mounting is able to hold 4 times the weight of the equipment. N O T I C E The analyzer must be aligned vertically to guarantee accuracy. -
Page 11: Wiring Overview
Wiring overview Figure 2 shows an overview of the wiring connections inside the controller with the high voltage barrier removed. The left side of the figure shows the back side of the controller cover. Note: Remove connector caps from the connectors before module installation. Figure 2 Wiring connections overview 1 Service cable connection 5 AC and DC power connector... - Page 12 W A R N I N G Potential Electrocution Hazard. If this equipment is used outdoors or in potentially wet locations, a Ground Fault Interrupt device must be used for connecting the equipment to its mains power source. D A N G E R Electrocution Hazard.
- Page 13 Table 2 DC power wiring information (DC powered models only) Terminal Description Color—North America Color—EU +24 VDC 24 VDC return Black Black — Protective Earth (PE) Ground lug Green Green with yellow stripe English 11...
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Page 14: Alarms And Relays
Alarms and relays The controller is equipped with four unpowered, single pole relays rated 100-250 VAC, 50/60 Hz, 5 amp resistive maximum. Contacts are rated 250 VAC, 5 amp resistive maximum for the AC powered controller and 24 VDC, 5A resistive maximum for the DC powered controller. The relays are not rated for inductive loads. - Page 15 W A R N I N G Potential electrocution hazard. AC mains powered controllers (115 V–230 V) are designed for relay connections to AC mains circuits (i.e., voltages greater than 16 V-RMS, 22.6 V-PEAK or 35 VDC). The wiring compartment is not designed for voltage connections in excess of 250 VAC. 24 VDC powered controllers W A R N I N G Potential electrocution hazard.
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Page 16: Analog Output Connections
Analog output connections W A R N I N G Potential Electrocution Hazard. Always disconnect power to the instrument when making electrical connections. W A R N I N G Potential electrocution hazard. In order to maintain the NEMA/IP environmental ratings of the enclosure, use only conduit fittings and cable glands rated for at least NEMA 4X/IP66 to route cables in to the instrument. -
Page 17: Discrete Input Wiring Connections
4. Make connections with twisted-pair shielded wire and connect the shield at the controlled component end or at the control loop end. • Do not connect the shield at both ends of the cable. • Use of non-shielded cable may result in radio frequency emission or susceptibility levels higher than allowed. - Page 18 Figure 4 Discrete input wiring connections Table 4 Input connections Discrete inputs Connector position - Switch input Connector position - Voltage input Input 1+ Input 1- Input 2+ Input 2- Input 3+ Input 3- Figure 5 Jumper settings 1 Input 1 configuration jumpers 3 Input 3 configuration jumpers 5 Jumpers positioned to the right for voltage inputs...
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Page 19: Connect The Optional Digital Communication Output
9. Refer to the instructions supplied with the network module for more details. For information about Modbus registers, go to http://www.hach-lange.com http://www.hach.com and search Modbus registers or go to any sc200 product page. Install a Secure Digital (SD) memory card... -
Page 20: Install The Reagents
Install the reagents W A R N I N G Chemical exposure hazard. Obey laboratory safety procedures and wear all of the personal protective equipment appropriate to the chemicals that are handled. Refer to the current safety data sheets (MSDS/SDS) for safety protocols. 1. -
Page 21: Display
Figure 7 Keypad and front panel overview 1 Instrument display 5 BACK key. Moves back one level in the menu structure. 2 Cover for secure digital memory card slot 6 MENU key. Moves to the Settings Menu from other screens and submenus. 3 HOME key. -
Page 22: Additional Display Formats
Figure 8 Example of Main Measurement screen 1 Home screen icon 7 Warning status bar 2 Sensor name 8 Date 3 SD Memory card icon 9 Analog output values 4 Relay status indicator 10 Time 5 Measurement value 11 Progress bar 6 Measurement unit 12 Measurement parameter Table 5 Icon descriptions... -
Page 23: System Startup
1. From the graphical display screen use the up and down arrow keys to select a graph and push the HOME key. 2. Select an option: Option Description MEASUREMENT VALUE Set the measurement value for the selected channel. Select between Auto Scale and Manually Scale. - Page 24 Option Description DISPLAY SETUP Configures the controller display. ADJUST ORDER—View and modify the measurement display order. • SEE CURRENT ORDER—View the current display order • ADD MEASUREMENTS—Add selected measurements to the display • REMOVE MEASUREMENTS—Remove selected measurements from the display •...
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Page 25: Using The Secure Digital Memory (Sd) Card
• DataCom is used to convert files from binary to CSV format. Refer to the DataCom manual for more information on how to use the application. For a copy of the DataCom manual, software updates or other downloadable resources, go to http://www.hach-lange.com http://www.hach.com and search DataCom. -
Page 26: Access Data And Event Log Files On The Sd Card
1. Attach the card reader device to the PC (if necessary) and install the SD card that contains the files in the reader device. 2. In the SD card directory, open the HACH folder. 3. Select the Logs folder. 4. Select a device folder. -
Page 27: Firmware Updates With Sd Cards
1. Find the zip file at http://www.hach-lange.com or http://www.hach.comand copy it to the PC. 2. Extract file(s) from the zip folder and save them to the SD card. 3. Remove the SD card and update the controller and device firmware. Refer to Updating software on page 23. -
Page 28: Operation
d. Push enter to return to the MANAGE CONFIGURATION menu. 4. To copy settings from the SD card to a controller (or a device connected to it): a. Select COPY SETTINGS and push enter. b. Select the devices on the SD card. All devices are selected by default. To deselect an item, highlight the selection and push the left arrow key. -
Page 29: Zero Calibration
5. The raw temperature value is displayed. Push enter. 6. Enter the correct value if different from that displayed and push enter. 7. Push enter to confirm the calibration. The temperature offset is displayed. Zero calibration The zero value has been factory calibrated. Use the zero calibration procedure to define the unique zero point of the sensor. -
Page 30: Exit Calibration Procedure
4. Select the option for the output signal during calibration: Option Description ACTIVE The instrument sends the current measured output value during the calibration procedure. HOLD The sensor output value is held at the current measured value during the calibration procedure. TRANSFER A preset output value is sent during calibration. -
Page 31: Reset Calibration Options
Includes an operator ID with calibration data—YES or NO (default). The ID is entered during the calibration. Reset calibration options This option is reserved for Hach Lange service technicians. Maintenance D A N G E R Multiple hazards. Only qualified personnel must conduct the tasks described in this section of the document. - Page 32 Table 6 Controller (continued) Problem Resolution Make sure relay connections are secure. If using an external power source, make sure the relay wiring is correct. Make sure the relay configuration is correct. Test the relay activation through the Test/Maintenance menu. No relay activation The relay should energize and de-energize as selected.
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Page 33: Test And Maintenance Menu
Table 6 Controller (continued) Problem Resolution Make sure the AC power connections are properly terminated in the controller. Controller will not power up, or powers up Make sure the power strip, line power, wall plug are all properly intermittently plugged in. Contact Technical Support Make sure the module is properly installed. -
Page 34: Sensor Diagnostic And Test Menu
Option Description OUTPUT CAL Lets the user calibrate the 4–20 mA outputs with a 250 ohm resistor in series to the mA output terminals. The settings for each output are adjusted until the • OUTPUT 1 correct value (4 mA or 20 mA) is supplied. •... -
Page 35: Warning And Error Conditions
Table 8 Sensor DIAG/TEST menu Option Description MODULE INFORMATION Shows information about the sensor module. SENSOR INFORMATION Shows the name and serial number that was entered by the user. CAL DAYS Shows the number of days since the last calibration. CAL HISTORY Shows a list of all calibrations by date/time stamp. -
Page 36: Error List
Table 9 Warning list for oxygen scavenger sensors (continued) Warning Description Resolution TEMP TOO LOW The measured temperature is < Increase sample temperature. 0 °C CURRENT TOO HIGH The measured current > 200 mA Make sure that the oxygen scavenger (hydrazine or carbohydrazide) level in the process water is within the operating limits of the sensor. -
Page 37: Material Safety Data Sheets (Msds)
Spare parts kit for 2 years - 09186=A=8000 (continued) Description Quantity Item no. O-Ring for Venturi injection nozzle 356099,05090 Plastic cleaning beads 588801,75008 4 × 6 mm PE tubing 2 meters 151575,00006 Measuring cell Description Item no. Measuring cell 09186=A=0100 Reference electrode 368429,00000 Working electrode... - Page 38 2. COMPOSITION / INFORMATION ON INGREDIENTS CAS no: 108-18-9 Molecular weight: 101.19 Molecular formula: C EC index number: 612-048-00-5 EINECS: 203-558-5 3. HAZARDS IDENTIFICATION Highly flammable. Irritating to eyes, respiratory system and skin. 4. FIRST AID MEASURES After skin contact: wash off with plenty of water. Remove contaminated clothing. After eye contact: rinse out with plenty of water for at least 10 minutes with the eyelid held wide open.
- Page 39 9. PHYSICAL AND CHEMICAL PROPERTIES pH value: not available Melting temperature: -96°C Boiling temperature: 83 - 84°C Ignition temperature: 295°C DIN51794 Flash point: -17°C DIN51755 Explosion limits: • Lower: 1.5 vol% • Upper: 8.5 vol% Vapor pressure: (20°C) 100 hPa Density: (20°C) 0.72 g/cm Solubility in: •...
- Page 40 14. TRANSPORT INFORMATION DOT and IATA: • Shipping Name: Diisopropylamine • UN Number: UN1158 • Hazard Class: 3.8 • Packing Group: PG II • Label(s): Flammable liquid, corrosive 15. REGULATORY INFORMATION United States: • Toxic Substance Control Act (TSCA): Listed •...
- Page 42 *DOC023.52.93069* HACH COMPANY World Headquarters HACH LANGE GMBH HACH LANGE Sàrl P.O. Box 389, Loveland, CO 80539-0389 U.S.A. Willstätterstraße 11 6, route de Compois Tel. (970) 669-3050 D-40549 Düsseldorf, Germany 1222 Vésenaz (800) 227-4224 (U.S.A. only) Tel. +49 (0) 2 11 52 88-320...