Cell Constant - TA Q Series Getting Started Manual

Tma hermomechanical analyzer
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When to Calibrate:
The sample thermocouple should be calibrated in the following situations:
When the TMA is first installed
When the sample thermocouple is changed
When the TMA is serviced or repaired
Periodically (approximately once a month)
If you are changing the temperature range of interest
If the run data obtained seems to be inaccurate
When the purge gas is changed.

Cell Constant

Cell constant calibration is based on a run conducted in the calibration mode in which a known standard (e.g.,
aluminum or copper) is heated through its transition temperature and data is gathered for analysis. The cell
constant is calculated by dividing the actual coefficient of expansion of the standard by the measured coeffi-
cient of expansion. The cell constant is then entered in the instrument control software for calibration of the
instrument.
Using the default cell constant value of 1.000 is usually adequate; however, for greatest accuracy, calibration
should be performed.
It is recommended that you follow the procedures of ASTM Standard Test Method E831 to perform the cell
constant calibration.
TMA Q Series Getting Started Guide
37

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