YSI 63 Operation Manual

YSI 63 Operation Manual

Handheld ph,conductivity,salinity and temperature system

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YSI Model 63
Handheld pH,
Conductivity,
Salinity and
Temperature
System
Operations
Manual

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Summary of Contents for YSI 63

  • Page 1 YSI Model 63 Handheld pH, Conductivity, Salinity and Temperature System Operations Manual...
  • Page 3: Table Of Contents

    Table of Contents 1. Introduction........................ 1 2. Preparing the Meter....................2 2.1 Unpacking ........................... 2 2.2 Warranty Card ........................2 2.3 Batteries..........................2 2.4 Transport Chamber......................3 2.5 Hand Strap........................... 3 2.6 The Meter Case ........................3 3. Preparing the Probe ....................4 3.1 Installing the pH Sensor ......................
  • Page 4 9. Principles of Operation ................... 26 9.1 pH ............................26 9.2 Conductivity ........................27 9.3 Salinity ..........................28 9.4 Temperature ........................28 10. Warranty and Repair ..................... 29 10.1 Cleaning Instructions....................... 30 10.2 Packing Instructions ......................31 11. Required Notice ..................... 32 12.
  • Page 5: Introduction

    The pH sensor can be easily replaced in the field. The Model 63 has a non-detachable cable available in lengths of 10, 25, 50 or 100 feet (3, 7.6, 15.2 or 30.5 meters). The probe body has been manufactured with stainless steel to add rugged durability and sinking weight.
  • Page 6: Preparing The Meter

    YSI Model 63 should ever need repair. Batteries There are a few things you must do to prepare your YSI Model 63 for use. First, locate the six AA-size alkaline batteries and the battery cover kit which were included. Then locate the markings inside each of the two battery-chamber sleeves that illustrate the correct way to install the batteries.
  • Page 7: Transport Chamber

    Insert the round sponge (provided with the Model 63) into the bottom of the chamber. Put 6-8 drops of tap water into the sponge. The wet sponge creates a humid environment for the pH sensor to prevent it from drying out during transport in the field (up to one week).
  • Page 8: Preparing The Probe

    Preparing the Probe The YSI Model 63 is shipped without the pH sensor installed. The pH sensor must be installed before using the system (see section 3.1 Installing the pH Sensor, below). The sensor is shipped with a protective bottle filled with a mixture of pH 4 buffer and KCl solution. Do not remove the bottle until you are ready to use the instrument.
  • Page 9: Operation

    Operation The following diagram is an overview of the operation of the Model 63. See the following sections for details of operation. Figure 4...
  • Page 10: Turning The Instrument On

    The user can choose from two sets of pH buffer values for 3-point calibration. The first set consists of the standard YSI pH buffer values of pH 7 (YSI 3822), pH 4 (YSI 3821) and pH 10 (YSI 3823). The second set available is the NIST pH 6.86, 4.01 and 9.18. Note that the first calibration point must be either pH 7 or pH 6.86.
  • Page 11 4. To enter the calibration menu, use two fingers to press and release both the UP ARROW and DOWN ARROW keys at the same time. The Model 63 display will show CAL at the bottom, STAND will be flashing and the pH reading will show 7.00 (the buffer to be used to adjust the offset).
  • Page 12 6. When the reading is stable (does not change by 0.01 pH in 10 seconds), the decimal point will stop flashing. Press and hold the ENTER key to save the calibration point. The Model 63 will flash SAVE on the display along with OFS to indicate that the offset value has been saved.
  • Page 13 11. When the reading is stable (does not change by 0.01 pH in 10 seconds), the decimal point will stop flashing. Press and hold the ENTER key to save the first SLOPE. The Model 63 will flash SAVE on the display along with SLP to indicate that the first slope value has been saved.
  • Page 14 7, the third buffer must be greater than pH 7. 16. Press the ENTER key. The Model 63 display will now show CAL at the bottom, SLOPE will stop flashing and the pH calibration value (automatically sensed by the instrument) is shown with one of the decimal points flashing.
  • Page 15: Conductivity Calibration

    • For fresh water choose a 1 mS/cm conductivity standard (YSI Catalog# 3167) • For brackish water choose a 10 mS/cm conductivity standard (YSI Catalog # 3168) 3. Place at least 7 inches of solution in the plastic container (provided with the Model 63) or a clean glass beaker.
  • Page 16: Making Measurements

    ENTER key. The word “SAVE” will flash across the display for a second indicating that the calibration has been accepted. The YSI Model 63 is designed to retain its last conductivity calibration permanently. Therefore, there is no need to calibrate the instrument after battery changes or power down.
  • Page 17 Temperature °C NOTE: When the Model 63 is turned off, it will “remember” which mode you used last and will return to that mode the next time it is turned on. If turned off while in recall or erase mode, it will default to pH mode when turned on.
  • Page 18: Autoranging & Range Searching

    (within the specifications of the instrument) all you need to do to get the most accurate reading is to put the probe in the sample. This feature makes the Model 63 as simple as possible to operate.
  • Page 19: Recalling Stored Data

    ID number in the lower right corner. Site identity 2. Press the ENTER key to review the last set of data that was saved. The Model 63 will display the pH and temperature. Another press of the ENTER key will display the conductivity and the temperature.
  • Page 20: Erasing Stored Data

    7. When you have finished recalling data, press MODE two times to return to normal operation. NOTE: The Model 63 will recall data as a list. When the UP ARROW is pressed the Model 63 will display the Site ID# for the previously recorded data. For example: If you are reviewing Site ID# 5 and the UP ARROW is pressed, the Model 63 will display Site ID#4.
  • Page 21: Display Backlight

    Display Backlight At times it may be necessary to take measurements with the Model 63 in dark or poorly lit areas. To help in this situation, the Model 63 comes equipped with a backlight which will illuminate the display so that it can be easily read. To activate the backlight, press and hold the LIGHT key.
  • Page 22: Advanced Conductivity Setup

    For that reason, we have made the YSI Model 63 flexible to accommodate these “advanced users.” If, for example, you are using the YSI Model 63 for a process control application which requires that the conductivity readings be compensated to 20...
  • Page 23: Changing The Reference Temperature

    Changing Conductivity From Autoranging To Manual Ranging If your application is easier to perform using a manual range which you select, the YSI Model 63 allows you to turn off the default autoranging feature. While you are making conductivity or temperature compensated conductivity measurements, simply press and release the UP ARROW key.
  • Page 24: Maintenance

    Maintenance pH Sensor Precautions 1. When making measurements or performing the calibration procedure, make certain that the level of sample or pH buffer is high enough to cover both the pH and temperature sensors. 2. Rinse the probe with deionized water between changes of calibration buffer solutions. 3.
  • Page 25: Ph Sensor Storage

    pH Sensor Storage For short term storage between measurements in the field (up to one week), place the probe in the transport chamber in the side of the instrument case. Make sure that the sponge inside the chamber is wet (tap water). For long term storage (over one week), place the probe in the storage bottle (provided) containing a mixture of 50% pH 4 buffer and 50% 1.5M KCl.
  • Page 26: Discussion Of Measurement Errors

    Performing a calibration will eliminate any error which might arise because of cell constant change. YSI cells are calibrated to within one percent of the stated cell constant at a single point. We consider these products to be usefully linear over most instrument ranges. The cell constant can...
  • Page 27 Temperature Error = ± 1% maximum The solution temperature error is the product of the temperature coefficient and the temperature offset from 25°C, expressed as a percentage of the reading that would have been obtained at 25°C. The error is not necessarily a linear function of temperature. The statement of error is derived from a 25°C temperature offset and a 3%/°C temperature coefficient.
  • Page 28: Troubleshooting

    Troubleshooting Error Messages The instrument performs a Power On Self Test each time it is turned on. The following error messages are provided to facilitate troubleshooting. They appear on the LCD when an error is detected. Symptom Possible Cause Action •...
  • Page 29 Symptom Possible Cause Action • • 10. Conductivity/Salinity Display When calibrating: User cell Recalibrate with known good reads “OVEr” constant cal K is >5.25 standards (pg 11) • • When measuring: Conductivity Clean conductivity cell (pg 21) • reading is >200 mS Return system for service (pg 29) •...
  • Page 30: Principles Of Operation

    Ag/AgCl reference electrode, is proportional to the pH of the media. Our testing of the Model 63 pH sensor indicates that it should provide long life, good response time and accurate readings in most environmental waters, including fresh water of low ionic strength.
  • Page 31: Conductivity

    Number of pH Calibration Points When calibrating the YSI Model 63, you have the choice of 1-point 2-point, or 3-point calibration. Perform a 2 or 3 point calibration at least once per day for accurate results.
  • Page 32: Salinity

    For this reason, the Model 63 software also allows the user to output conductivity data in either raw or temperature compensated form.
  • Page 33: Warranty And Repair

    Endeco/YSI Inc. • 13 Atlantis Drive • Marion, MA • 02738 • Phone: 508 748-0366 • Fax: 508 748-2543 Europe YSI LTD • Lynchford House • Lynchford Lane • Farnborough, Hampshire • GU14 GLT • Phone: 441 252 514711 • Fax: 441 252 511855 YSI Authorized Service Centers California EviroServices &...
  • Page 34: Cleaning Instructions

    Disposition costs will be the responsibility of the sender. When service is required, either at the user's facility or at YSI, the following steps must be taken to insure the safety of our service personnel.
  • Page 35: Packing Instructions

    10.2 Packing Instructions 1. Clean and decontaminate items to insure the safety of the handler. 2. Complete and include the Cleaning Certificate. 3. Place the product in a plastic bag to keep out dirt and packing material. 4. Use a large carton, preferably the original, and surround the product completely with packing material.
  • Page 36: Required Notice

    11. Required Notice The Federal Communications Commission defines this product as a computing device and requires the following notice: This equipment generates and uses radio frequency energy and if not installed and used properly, may cause interference to radio and television reception. There is no guarantee that interference will not occur in a particular installation.
  • Page 37: Accessories And Replacement Parts

    12. Accessories and Replacement Parts The following parts and accessories are available from YSI or any Franchise Dealer authorized by YSI. YSI Order Number Description Conductivity Calibration Solution 1,000 µ/cm (1 Quart) 3161 Conductivity Calibration Solution 10,000 µ/cm (1 Quart) 3163 Conductivity Calibration Solution 100,000 µ/cm (1 Quart)
  • Page 38: Appendix A - Specifications

    13. Appendix A - Specifications Materials: ABS, Stainless Steel, and other materials Dimensions: Height: 9.5 inches (24.13 cm) Thickness: 2.2 inches (5.6 cm) Width: 3.5 inches max. (8.89 cm) Weight: 1.7 pounds (w/ 10’ cable) (.77 kg) Display: 2.3”W x 1.5”L (5.8 cm W x 3.8 cm L) Power: 6 AA-size Alkaline Batteries (included) Approximately 100 hours operation from each new set of batteries...
  • Page 39 Adjustable Conductivity Reference Temperature: 15°C to 25°C Adjustable Temperature Compensation Factor for Conductivity: 0% to 4% pH Response Time: 3 sec for 95% of the change at 25°C Temperature Response Time: 20 sec for 95% of the change Temperature Compensation: Automatic Range: User selected or Autoranging for Conductivity Data Storage: 50 points with ID number.
  • Page 40: Appendix B - Health And Safety

    14. Appendix B - Health and Safety YSI pH 4, 7 & 10 Buffer Solutions: 3821, 3822, 3823 pH 4 Ingredients: " Potassium Hydrogen Phthalate " Formaldehyde " Water pH 7 Ingredients: " Sodium Phosphate, Dibasic " Potassium Phosphate, Monobasic "...
  • Page 41: Appendix C - Ph Buffer Values

    15. Appendix C - pH Buffer Values YSI pH 4, 7 and 10 Buffer Solutions: 3821, 3822, 3823 The following table lists the values of YSI pH buffer solutions at various temperatures. Temperature pH 4 pH 7 pH 10 0°C 4.01...
  • Page 42: Appendix D - Temperature Correction Data

    16. Appendix D - Temperature Correction Data Conductivity Temperature Correction Data for Typical Solutions A. Potassium Chloride (KCl) Concentration: 1 mole/liter Concentration: 1 x 10 mole/liter °C °C mS/cm mS/cm %/°C (to 25°C) %/°C (to 25°C) 65.10 1.67 7.13 1.78 73.89 1.70 8.22...
  • Page 43 B. Sodium Chloride (NaCl) Saturated solutions at all temperatures Concentration: 0.5 mole/liter °C °C mS/cm mS/cm %/°C (to 25°C) %/°C (to 25°C) 134.50 1.86 25.90 1.78 155.55 1.91 29.64 1.82 177.90 1.95 33.61 1.86 201.40 1.99 37.79 1.90 225.92 2.02 42.14 1.93 251.30...
  • Page 44 C. Lithium Chloride (LiCl) Concentration: 1 mole/liter Concentration: 1 x 10 mole/liter °C °C mS/cm mS/cm %/°C (to 25°C) %/°C (to 25°C) 39.85 1.82 5.07 1.87 46.01 1.85 5.98 1.85 52.42 1.89 6.87 1.85 59.07 1.92 7.75 1.85 65.97 1.95 8.62 1.85 73.10...
  • Page 45 E. Ammonium Chloride Concentration: 1 mole/liter Concentration: 1 x 10 mole/liter °C °C mS/cm mS/cm %/°C (to 25°C) %/°C (to 25°C) 64.10 1.60 6.96 1.82 74.36 1.53 7.98 1.88 83.77 1.45 9.09 1.93 92.35 1.37 10.27 1.97 100.10 1.29 11.50 2.00 107.00 1.21...
  • Page 46 1725 Brannum Lane Yellow Springs, Ohio 45387 USA 031178 937 767-7241 • 800 765-4974 • Fax 937 767-9353 A31178A Info@ysi.com • www.YSI.com September 99  1998 YSI Incorporated...

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