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432
Waters 432 Manuals
Manuals and User Guides for Waters 432. We have
1
Waters 432 manual available for free PDF download: Operator's Manual
Waters 432 Operator's Manual (113 pages)
Conductivity Detector
Brand:
Waters
| Category:
Security Sensors
| Size: 2 MB
Table of Contents
Table of Contents
15
Preface
23
Chapter 1 Introduction
26
Waters 432 Conductivity Detector
26
Flow Cell Schematic
28
Limiting Equivalent Conductance of Ions in Water at 25 °C
29
Chapter 2 Installing the Detector
30
Selecting the Installation Site
30
Unpacking and Inspection
31
AC Power Connection
32
Rear Panel
33
Power Cord Wire Identification
33
Changing the Voltage Setting
34
Nominal Operating Voltage
34
I/O Signal Connections
35
I/O Signal Descriptions
35
I/O Terminal Strip
36
I/O Signal Descriptions
36
Powerline Controller Connections
37
IEEE-488 Address Switch
38
IEEE-488 DIP Switch Setting
38
Empower and Millennium Connections
39
Bus SAT/IN Module (Front Panel)
40
Bus SAT/IN to Bus LAC/E Connections
42
Bus SAT/IN to 432 Detector Connections
43
Data Module Connections
44
Bus SAT/IN Cable Connections
44
Data Module Signal Cable Connections
44
Chart Recorder Connections
45
Chart Marker Input Connections
45
Data Module Chart Mark Cable Connections
45
Chart Recorder Cable Connections
45
Auto Zero Input Connections
46
Alliance Separations Module Connections
46
Autosampler Chart Mark Cable Connections
46
Alliance Separations Module Connections to the 432 Detector Auto-Zero on Inject
47
Connections for Generating Auto-Zero on Inject
47
Making Fluidic Connections
48
Alliance Separations Module Connections to the 432 Detector Chart Mark on Inject
48
Connections for Generating Chart Mark on Inject
48
Fluid Connections
49
Cutting Polymeric Tubing
50
Ferrule and Compression Screw Assembly
51
Passivating the System
53
Pulse Dampener
53
Verifying the Detector
54
Chapter 3 Operating the Detector
56
Controls and Indicators
56
Front Panel
56
Key Descriptions
58
Setting the Beep Function
60
Startup and Shutdown
61
Operating Recommendations
62
Chapter 4 Performing Ion Analysis
64
Fundamental Considerations
64
Soda Lime Tube
67
Configuring the System
68
System Configuration for Ion Analysis
68
Eluents for Ion Analysis
69
Preparing Anion Eluent
70
Preparing Cation Eluent
70
Standards for Ion Analysis
70
Preparing Anion Standards
71
Shelf-Life of Standards
71
Injecting Anion Standards
72
Salts for Anion Standard Concentrates
72
Anion Concentrate Dilutions
72
Preparing Cation Standards
74
Chromatogram of a 7-Anion Standard
74
Salts for Cation Standard Concentrates
75
Cation Concentrate Dilutions
75
Injecting Cation Standards
76
Chromatogram of an 8-Cation Standard
77
Chapter 5 Maintenance
78
Routine Maintenance
78
Replacing the Fuse
78
Maintaining the Flow Cell
79
Installing Operating Voltage Fuses
79
Flow Cell Assembly
81
Cleaning the Detector Exterior
82
Troubleshooting
82
Troubleshooting Guide
85
Appendix A Specifications
87
Operational Specifications
87
Mechanical Specifications
87
Electrical Specifications
87
Environmental Specifications
87
A-4 Electrical Specifications
88
A-5 Communications
89
Appendix B Spare Parts
90
Spare Parts
90
Appendix C Ion Chromatography Methods
91
General-Purpose Anion Analysis Using Conductivity and UV Detection
91
Required Instrumentation
91
Common Anion Standards
92
Analysis Conditions
92
Preparing Eluent
93
Preparing Standards
93
Preparing a Sample
93
Empower Data Processing Method
94
IC Processing Method Using Peak Apex for Retention Time
94
Method Validation
95
Method Linearity
95
Calibration Curves for Chloride, Fluoride, and Bromide
95
Calibration Curves for Nitrite and Nitrate
96
Calibration Curves for Sulfate and Phosphate
96
Quantitation Precision
97
Method Detection Limits
97
Quantitation Accuracy
98
Analyte Recovery
99
Example of Use
100
Using Direct UV Detection
100
Typical Drinking Water, no Dilution Required
100
Direct UV Detection
101
Preparing Lithium Borate/Gluconate 50X Stock Concentrate
102
Preparing Lithium Borate/Gluconate Eluent
102
Alkali and Alkaline Earth Cations, Ammonium, and Amines
103
Required Instrumentation
103
Preparing Eluent
104
Preparing Standards
104
Analysis Conditions
104
Preparing a Sample
105
Empower Data Processing Method
105
Method Detection Limits
106
IC Processing Method Using Peak Apex for Retention Time
106
Examples of Use
107
Typical Drinking Water, no Dilution Required
107
Typical Municipal Wastewater, Diluted 1:50, Overlay of Duplicate Injections
107
Preparing Stock Reagent
108
Appendix D Validation Support
109
Index
111
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