Shimadzu GC-2010 Plus Manuals

Shimadzu GC-2010 Plus Manuals

Manuals and User Guides for Shimadzu GC-2010 Plus. We have 1 Shimadzu GC-2010 Plus manual available for free PDF download: Instruction Manual

Shimadzu GC-2010 Plus Instruction Manual

Shimadzu GC-2010 Plus Instruction Manual (352 pages)

Gas Chromatograph

Brand: Shimadzu | Category: Laboratory Equipment | Size: 4 MB

Table of Contents

Table of Contents
11
1 Overview

21
- System Features
  21
  - Basic Performance
    21
  - Operation
    21
  - High Speed Analysis Enabled
    21
- Specifications
  22
  - Column Oven
    22
  - Temperature Program
    22
  - Injection Port
    22
  - Detector
    23
  - Auxiliary Heated Zone
    23
  - Carrier Gas Flow Control Unit
    24
  - Detector Gas Flow Controller
    24
  - Display
    24
  - Dimensions, Weight and Power Supply
    24
2 Installation

25
- Shipment Verification
  25
- Component Description
  27
- Installation Site
  33
  - Ambient Temperature and Humidity
    33
  - Installation Location
    33
  - Corrosive Gas and Dust
    33
  - Electro-Magnetic Fields and Power Supply Noise
    33
  - Other Precautions
    33
  - Rear Clearance
    34
  - Left Clearance
    34
- Moving the GC
  35
- Power Supply and Wiring
  36
- Gas Supply Plumbing
  39
- Connecting External Device Cables
  47
3 Afc, Apc

53
- AFC and APC Overview
  53
- Definition of Terms
  54
- Flow Line Diagram
  55
- AFC and APC Control
  56
  - AFC Control
    56
  - Split Mode: "SPLIT" (AFC)
    56
  - Split Mode: "SPLITLESS" (AFC)
    58
  - Split Mode: "DIRECT
    59
  - Control by APC
    60
- AFC and APC Control Ranges
  62
- AFC and APC Offset Calibration
  64
4 Installing the Column

67
5 Basic Key Operation

73
- Keypad Description and Operation
  73
  - Keypad Operation
    74
  - Screen
    75
  - Status Indicators
    76
- Adjusting the Display
  77
- Basic Key Operations
  78
  - Screen Display
    78
  - Moving the Cursor
    79
  - Entering Numeric Values
    80
  - Changing a Selection
    80
  - Changing Item Names
    81
- Getting Help
  83
  - Screen Help
    83
  - PF Menu
    83
6 Analysis Flow Chart

85
- Preparation
  85
- Setting Parameters
  85
- Analysis
  86
7 Starting and Stopping the GC [SYSTEM]

91
- SYSTEM] Key Main Screen
  91
  - Screen Description
    91
  - Parameter
    92
  - PF Menu
    93
- Specifying Clean up Parameters
  94
  - Screen Description
    94
  - Parameter List
    95
  - PF Menu
    97
- Specifying Start Procedures
  98
- Specifying the Stop Procedures
  100
  - Screen
    100
  - Parameter List
    100
  - System Shut down Examples
    101
8 Setting the Analytical Parameters and File Management

103
- SET] Key Main Screen
  103
  - Main Screen
    103
  - Parameter List
    104
  - PF Menu
    106
- File Management
  107
  - Screen Description
    107
  - PF Menu
    107
  - Copying a File
    108
  - Renaming a File
    108
  - Initializing a File
    109
- Specifying the Analytical Flow Line Components ([Line Config])
  110
  - Screen Description
    110
- Changing Items Displayed with [Customiz]
  113
  - Screen Description
    113
9 Monitoring the GC

115
- MONIT] Key Main Screen
  115
  - Screen Description
    115
  - Parameter List
    117
  - PF Menu
    117
- Monitoring the Temperature with [Temp Mon]
  118
  - Screen Description
    118
  - PF Menu
    118
- Monitoring the Flow Rate with [Flow Mon]
  119
  - Screen Description
    119
  - PF Menu
    119
- Zero Point Adjustment
  120
  - Screen Description
    120
10 Starting and Stopping Analysis

121
- Making an Injecting and Starting an Analysis
  121
  - Verifying the Gas Chromatograph Status
    121
  - Making Manual Injection
    121
  - Starting the Analysis
    122
- Terminating the Analysis
  123
  - External Devices
    123
11 Creating an Oven Temperature Program

125
- COL] Key Main Screen
  125
  - Screen Description
    125
  - Parameter List
    126
  - PF Menu
    126
- Temperature Programs
  127
  - Isothermal Analysis
    127
  - Programmed Analysis
    127
  - Creating a Temperature Program
    127
12 Injection Port

131
- Introduction
  131
- Glass Insert and Packing Requirements
  132
- Removing and Inserting the Glass Insert
  134
- Removing and Installing the Septum
  140
- Split/Splitless Injection System
  142
  - Setting the Temperature with [INJ] Key
    143
  - Setting the Flow Rate with [FLOW] Key
    145
  - Setting Column Parameters
    148
  - Gas Saver
    149
  - Pressure Program
    150
  - Creating a Flow Rate Program
    152
  - Split Ratio Program
    154
  - Septum Purge
    156
  - High Pressure Injection Splitter Mode and Back Flush
    158
- Direct Injection System
  161
  - Setting the Temperature
    162
  - Setting the Flow Rate
    163
- Setting the Flow Rate Parameters
  166
13 Detector

169
- Introduction
  169
- Hydrogen Flame Ionization Detector (FID)
  170
  - Principle of FID Operation
    170
  - Setting the Detector
    171
  - Setting the Detector Gas Flows
    176
- Thermal Conductivity Detector (TCD)
  180
  - Principle of TCD Operation
    180
  - Setting the Detector
    181
  - Setting the Detector Gas Flows
    185
- Filter Signal Time Constant
  189
- Setting the Output Signals
  190
  - Detector Signal Output
    190
  - Background Compensation
    191
  - Detector Signal Subtraction
    193
14 Diagnosis

195
- Standard Diagnosis
  195
  - Screen Description
    195
  - PF Menu
    195
  - Diagnosis Parameters
    196
  - Diagnosis Parameter List
    197
  - Starting the Diagnosis
    199
  - PF Menu
    199
  - Stopping/Exiting the Diagnosis
    200
  - PF Menu
    200
  - Diagnosis Results
    201
  - PF Menu List
    201
- Log Reading Menu
  203
  - Screen Description
    203
  - Parameter List
    203
  - GC Operation Log
    204
  - Analysis Log
    205
  - Parameter Log
    207
  - Error Log
    208
  - Diagnostic Log
    209
- Analysis Counter
  210
  - Screen Description
    210
  - Parameter List
    211
  - PF Menu
    211
- Coolant Consumption Counter
  212
  - Screen Description
    212
  - Parameter List
    213
  - PF Menu
    213
- Standard Installation Test
  214
  - Screen Description
    214
  - PF Menu
    214
  - Test Procedure
    215
- Peak Generator
  216
  - Screen Description
    216
  - Parameter List
    216
  - PF Menu
    216
15 Optional Devices

217
- Auto Injector Parameters
  217
  - Screen Description
    217
  - Parameter List
    218
  - PF Menu
    219
  - AOC Priority Analysis
    220
  - Parameter List
    220
  - PF Menu
    221
  - Other AOC Parameters
    221
  - Other AOC Parameter
    222
  - PF Menu
    223
  - Auto-Sampler Carousel and Other Optional Parameters
    224
  - Parameter List
    224
  - PF Menu
    224
- Setting aux Temperature
  225
  - Screen Description
    225
  - Parameter List
    225
  - PF Menu
    225
  - On/Off Setting
    226
  - On/Off Parameter List
    226
- Setting the aux APC Parameters
  227
  - Screen Description
    227
  - Parameter List
    228
  - PF Menu List
    228
  - Setting a Program
    229
  - Using Restrictor Tubing
    230
  - Parameter List
    230
- Setting the CRG Parameters
  231
  - Screen Description
    231
  - Parameter List
    232
  - PF Menu
    232
16 Special Functions

233
- Time Scheduler
  233
  - Description Screen
    233
  - Parameter List
    233
  - Setting the Mode
    234
  - Editing a Time Schedule
    235
  - PF Menu
    235
  - Creating a New Time Schedule
    236
  - PF Menu
    236
  - Parameters Available in the Time Scheduler
    237
  - Changing Schedule Parameters
    238
  - Time Schedule Example
    239
  - Starting/Stopping a Time Schedule
    240
  - PF Menu
    240
  - Copying and Deleting a Time Schedule
    241
- Batch Schedule
  242
  - Screen Description
    242
  - Parameter List
    243
  - PF Menu
    243
  - Creating a New Batch Schedule (for Single Injector)
    244
  - Parameter List
    245
  - PF Menu List
    246
  - Creating a New Batch Schedule (for Dual Injectors)
    246
  - Editing a Batch Schedule
    247
  - Batch Processing Setup Example
    248
- Time Program
  250
  - Screen Description
    250
  - PF Menu
    250
  - Creating a New Time Program
    251
  - PF Menu
    251
  - Time Program Parameters
    252
  - Editing a Time Program
    253
  - Time Program Setup Example
    254
- Pre-Run Program
  256
  - Screen Description
    256
  - PF Menu
    256
  - Creating a New Pre-Run Program
    257
  - Editing a Pre-Run Program
    257
  - After Pre-Run Program Is Finished
    257
  - Pre-Run Program Set up Example
    258
- Direct Operation
  259
  - Screen Description
    259
  - Parameter List
    259
  - PF Menu
    259
- GC Configuration
  260
  - Screen Description
    260
  - Parameter List
    260
  - Setting the Date and Time
    261
  - Setting the Maximum Temperature Limits
    262
  - Setting Transmission Parameters
    263
  - Setting the Ready Check Parameters
    264
  - Parameter Configuration
    266
  - Customizing Component Names
    270
  - Setting the Link Device Code
    273
  - Temperature Offset
    274
  - Other Settings
    275
- Service and Maintenance
  279
  - Screen Description
    279
  - Parameter List
    279
  - Installation (Position)
    280
  - Installation (Piping)
    282
  - Initialization
    284
  - Power Consumption
    285
- Stopwatch
  286
  - Screen Description
    286
  - PF Menu
    286
  - Timing with Inverse Measurement
    286
- Key Lock and Parameter Lock
  287
  - Screen Description
    287
  - Key Locking
    288
  - Parameter Locking
    289
- ROM Version no
  292
  - Screen Description
    292
  - Parameter List
    292
17 Printing

293
- Connection to Chromatopac
  293
- Parameters to be Printed
  293
- AOC Commands
  297
- Program Parameters
  299
- Event no
  301
18 Maintenance and Inspection

305
- Maintenance Parts
  305
  - Septum
    305
  - O-Ring for Glass Insert
    305
  - Glass Insert
    305
  - Graphite Ferrule
    306
  - Capillary Column
    306
  - Flow Controller
    306
  - Hydrogen Flame Ionization Detector (FID)
    306
  - Miscellaneous
    306
- Inspection and Maintenance Intervals
  307
  - Glass Insert
    307
  - Septum
    307
  - O-Ring for Glass Insert
    307
  - Graphite Ferrule
    307
  - Capillary Column
    307
  - Flow Controller
    307
  - Hydrogen Flame Ionization Detector (FID)
    307
  - Cleaning the Unit
    307
- Inspection and Maintenance: Septum
  308
  - Inspection/Maintenance Cycle
    308
  - Inspection/Maintenance
    308
- Inspection and Maintenance: O-Ring for Glass Insert
  310
  - Inspection/Maintenance Cycle
    310
  - Inspection/Maintenance
    310
- Inspection and Maintenance: Glass Insert
  314
  - Inspection/Maintenance Cycle
    314
  - Inspection/Maintenance
    314
- Inspection and Maintenance: Graphite Ferrule
  317
  - Inspection/Maintenance Cycle
    317
  - Inspection/Maintenance
    317
- Inspection and Maintenance: Capillary Column
  319
  - Inspection/Maintenance Cycle
    319
  - Inspection/Maintenance
    319
- Inspection and Maintenance: Flow Controller
  321
  - Inspection/Maintenance Cycle
    322
  - Inspection/Maintenance
    322
- Inspection and Maintenance: FID
  324
  - Inspection/Maintenance Cycle
    324
  - Inspection/Maintenance
    324
19 Troubleshooting

329
- Gas and Pressure Settings
  330
- Temperature Control
  331
- Detector
  331
- Chromatogram and Data
  334
- Error Messages
  337
  - System Errors
    337
  - Operations Errors
    338
  - Optional Device Error (AOC-20I/S)
    340
  - Communication Errors
    340
  - Detector Errors
    341
  - Other Errors
    342
  - Warning Messages
    346
20 Appendix

347
- Key Function List
  347
21 Index

349

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