Shimadzu GC-2014 Manuals

Manuals and User Guides for Shimadzu GC-2014. We have 4 Shimadzu GC-2014 manuals available for free PDF download: Instruction Manual, Operation Manual, Service Manual

Shimadzu GC-2014 Instruction Manual (318 pages)

Gas Chromatograph

Brand: Shimadzu | Category: Laboratory Equipment | Size: 3 MB

Table of Contents
5
1 Installation

13
2 Before Use

29
3 Installing Packed Columns and Setting Analytical Flow Lines

43
4 Installing Capillary Columns and Setting Analytical Flow Lines

59
5 Analysis

73
- Analysis Flow Chart
  73
  - Preparation
    73
  - Setting Parameters
    73
  - Analysis
    74
- Notes for Analysis
  75
6 Basic Key Operation

79
- Keypad Description and Operation
  79
  - Keypad Operation
    80
  - Screen
    81
  - Status Indicators
    82
- Adjusting the Display
  83
- Basic Key Operations
  84
  - Screen Display
    84
  - Moving the Cursor
    85
  - Entering Numeric Values
    86
  - Changing a Selection
    86
  - Changing Item Names
    87
- Getting Help
  89
  - Screen Description
    89
  - PF Menu
    89
7 Starting and Stopping the GC [SYSTEM]

91
- SYSTEM] Key Main Screen
  91
  - Screen Description
    91
  - Parameter
    92
  - PF Menu
    93
- Specifying Clean up Parameters
  94
  - Screen Description
    94
  - Parameter List
    95
  - PF Menu
    97
- Specifying Start Procedures
  98
- Specifying the Stop Procedures
  100
  - Screen
    100
  - Parameter List
    100
  - System Shut down Examples
    101
8 Setting the Analytical Parameters and File Management

103
- SET] Key Main Screen
  103
  - Main Screen
    103
  - Parameter List
    104
  - PF Menu
    106
- File Management
  107
  - Screen Description
    107
  - PF Menu
    107
  - Copying a File
    108
  - Renaming a File
    108
  - Initializing a File
    109
- Specifying the Analytical Flow Line Components ([Line Config])
  110
  - Screen Description
    110
- Changing Items Displayed with [Customiz]
  113
  - Screen Description
    113
9 Monitoring the GC

115
- MONIT] Key Main Screen
  115
  - Screen Description
    115
  - Parameter List
    117
  - PF Menu
    117
- Monitoring the Temperature with [Temp Mon]
  118
  - Screen Description
    118
  - PF Menu
    118
- Monitoring the Flow Rate with [Flow Mon]
  119
  - Screen Description
    119
  - PF Menu
    119
- Zero Point Adjustment
  120
  - Screen Description
    120
10 Starting and Stopping Analysis

121
- Making an Injecting and Starting an Analysis
  121
  - Verifying the Gas Chromatograph Status
    121
  - Making Manual Injection
    122
  - Starting the Analysis
    123
- Terminating the Analysis
  124
  - External Devices
    124
11 Creating an Oven Temperature Program

125
- COL] Key Main Screen
  125
  - Screen Description
    125
  - Parameter List
    126
  - PF Menu
    126
- Temperature Programs
  127
  - Isothermal Analysis
    127
  - Programmed Analysis
    127
  - Creating a Temperature Program
    127
12 Injection Port

131
- Packed Column Injection Port (Dual INJ)
  131
  - Setting the Temperature with [INJ] Key
    132
  - Setting the Flow Rate
    134
  - Entering Columns Parameters
    136
  - Creating a Flow Rate Program
    137
- Split/Splitless Injection System
  138
  - Setting the Temperature with [INJ] Key
    139
  - Setting the Flow Rate with [FLOW] Key
    141
  - Setting Column Parameters
    145
  - Gas Saver
    146
  - Pressure Program
    147
  - Creating a Flow Rate Program
    149
  - Split Ratio Program
    151
  - Septum Purge
    153
  - High Pressure Injection and Splitter Fix Mode
    155
- Direct Injection System
  157
  - Setting the Temperature
    158
  - Setting the Flow Rate
    159
- AFC and APC Offset Calibration
  161
- Setting the Flow Rate Parameters
  162
13 Detector

165
- Hydrogen Flame Ionization Detector (FID)
  165
- Thermal Conductivity Detector (TCD)
  176
  - Principle of TCD Operation
    176
  - Setting the Detector
    177
  - TCD Zero Point Adjustment
    181
- Filter Signal Time Constant
  182
- Background Compensation
  183
14 Diagnosis

185
- Standard Diagnosis
  185
  - Screen Description
    185
  - PF Menu
    185
  - Diagnosis Parameters
    186
  - Diagnosis Parameter List
    187
  - Starting the Diagnosis
    189
  - PF Menu
    189
  - Stopping/Exiting the Diagnosis
    190
  - PF Menu
    190
  - Diagnosis Results
    191
  - PF Menu
    191
- Log Reading Menu
  193
  - Screen Description
    193
  - Parameter List
    193
  - GC Operation Log
    194
  - Analysis Log
    195
  - Parameter Log
    197
  - Error Log
    198
  - Diagnostic Log
    199
- Analysis Counter
  200
  - Screen Description
    200
  - Parameter List
    201
  - PF Menu
    201
- Coolant Consumption Counter
  202
  - Screen Description
    202
  - Parameter List
    203
  - PF Menu
    203
- Standard Installation Test
  204
  - Screen Description
    204
  - PF Menu
    204
  - Test Procedure
    205
- Peak Generator
  206
  - Screen Description
    206
  - Parameter List
    206
  - PF Menu
    206
15 Optional Devices

207
- Auto Injector Parameters
  207
  - Screen Description
    207
  - Parameter List
    208
  - PF Menu
    209
  - AOC Priority Analysis
    210
  - Parameter List
    210
  - PF Menu
    211
  - Other AOC Parameters
    211
  - Other AOC Parameter
    212
  - PF Menu
    213
  - Auto-Sampler Carousel and Other Optional Parameters
    214
  - Parameter List
    214
- Setting AUX Temperature
  215
  - Screen Description
    215
  - Parameter List
    215
  - PF Menu
    215
  - On/Off Setting
    216
  - On/Off Parameter List
    216
- Setting the AUX APC Parameters
  217
  - Screen Description
    217
  - Parameter List
    218
  - PF Menu
    218
- Setting the AUX AMC Parameters
  219
  - Screen Description
    219
  - Parameter List
    220
  - PF Menu
    220
- Setting the CRG Parameters
  221
  - Screen Description
    221
  - Parameter List
    222
  - PF Menu
    222
16 Special Functions

223
- Time Scheduler
  223
  - Description Screen
    223
  - Parameter List
    223
  - Setting the Mode
    224
  - Editing a Time Schedule
    225
  - PF Menu
    225
  - Creating a New Time Schedule
    226
  - PF Menu
    226
  - Parameters Available in the Time Scheduler
    227
  - Changing Schedule Parameters
    227
  - Time Schedule Example
    228
  - Starting/Stopping a Time Schedule
    229
  - PF Menu
    229
  - Copying and Deleting a Time Schedule
    230
- Batch Schedule
  231
  - Screen Description
    231
  - Parameter List
    232
  - PF Menu
    232
  - Creating a New Batch Schedule
    233
  - Parameter List
    234
  - PF Menu
    235
  - Editing a Batch Schedule
    235
  - Batch Processing Setup Example
    236
- Time Program
  237
  - Screen Description
    237
  - PF Menu
    237
  - Creating a New Time Program
    238
  - PF Menu
    238
  - Time Program Parameters
    239
  - Editing a Time Program
    240
  - Time Program Setup Example
    241
- Pre-Run Program
  243
  - Screen Description
    243
  - PF Menu
    243
  - Creating a New Pre-Run Program
    244
  - Editing a Pre-Run Program
    244
  - After Pre-Run Program Is Finished
    244
  - Pre-Run Program Set up Example
    245
- Direct Operation
  246
  - Screen Description
    246
  - Parameter List
    246
  - PF Menu
    246
- GC Configuration
  247
  - Screen Description
    247
  - Parameter List
    247
  - Setting the Date and Time
    248
  - Setting the Maximum Temperature Limits
    249
  - Setting Transmission Parameters
    250
  - Setting the Ready Check Parameters
    251
  - Parameter Configuration
    253
  - Customizing Component Names
    258
  - Setting the Link Device Code
    262
  - Temperature Offset
    263
  - Other Settings
    264
- Service and Maintenance
  267
  - Screen Description
    267
  - Parameter List
    267
  - Installation (Position)
    268
  - Installation (Piping)
    270
  - Initialization
    273
  - Power Consumption
    274
- Stopwatch
  275
  - Screen Description
    275
  - PF Menu
    275
  - Timing with Inverse Measurement
    275
- Key Lock and Parameter Lock
  276
  - Screen Description
    276
  - Key Locking
    277
  - Parameter Locking
    278
- ROM Version no
  281
  - Screen Description
    281
  - Parameter List
    281
17 Printing

283
- Connection to Chromatopac
  283
- Parameters to be Printed
  283
- AOC Commands
  287
- Program Parameters
  289
- Event no
  291
18 Error Messages

295
- System Errors
  295
- Temperature Control Errors
  298
- Pressure/Flow Rate Errors
  301
- Communication Errors
  305
- Detector Errors
  306
- Program Errors
  308
- Operations Errors
  309
- Optional Device Error (AOC-20I/S)
  312
- Warning Messages
  313

Shimadzu GC-2014 Operation Manual (148 pages)

Gas Chromatograph

Brand: Shimadzu | Category: Laboratory Equipment | Size: 2 MB

Introduction
3
Important
3
Notice
3
GC Models and Supplied Equipment
4
Safety-Related Signal Words
4
- Safety Precautions
  5
Gas Usage Precautions
7
Installation Location
9
In the Event of an Emergency or Power Outage
10
Precaution for Maintenance
11
1 General

19
- Features
  20
- Names of Components
  21
- Specifications
  28
2 Before Using GC-2014

31
- Verifying Package
  32
- Handling of Instrument
  34
- Opening/Closing Column Oven Door
  34
- Power ON/OFF
  34
- Removing INJ/DET Cover
  35
- Opening Flow Controller Cover
  35
- Screen Operation
  38
- Displaying Main Screen
  38
- Displaying Sub Screen
  39
- Switching PF Menus
  39
- Moving Cursor
  40
- Operation When You Have Multiple Choices
  41
- Screen Help
  42
- Analysis Using Packed Column
  44
- Preparation
  44
- Installing SUS (Stainless Steel) Packed Column in Oven
  46
- Installing Septum to Injection Port
  50
- Installing Glass Packed Column in Oven
  52
- Checking Gas Leak
  56
- External Device Setup
  58
- Setting for Analysis
  59
- Actual Analysis
  64
- Analysis Using Capillary Column
  67
- Preparation
  67
- Installation to Injection Port
  71
- Installing Adaptor
  74
- Installing Capillary Column in Oven
  77
- Checking Gas Leak
  81
- External Device Setup
  83
- Setting for Analysis
  84
- Actual Analysis
  90
- AOC (Optional) Setting
  93
- Specifying AOC
  93
- Starting AOC
  94
- TCD Setting
  95
- Screen Description
  95
- Zero Point Adjustment for TCD
  96
4 Maintenance and Inspection

97
- Parts for Maintenance
  98
  - If You Are Using Packed Column
    98
  - If You Are Using Capillary Column
    100
- Inspection/Maintenance Intervals
  101
- General Maintenance Procedures
  102
  - If You Are Using Packed Column
    102
  - If You Are Using Capillary Column
    104
- Septum
  105
  - If You Are Using Packed Column
    105
  - If You Are Using Capillary Column
    106
- O-Ring for Glass Insert
  107
  - If You Are Using Capillary Column
    107
- Glass Insert
  109
  - If You Are Using Packed Column
    109
  - If You Are Using Capillary Column
    110
- Graphite Ferrule
  112
  - If You Are Using Packed Column
    112
  - If You Are Using Capillary Column
    113
- Packed Column
  114
- Capillary Column
  115
- Flow Controller (SPL, WBI Only)
  116
  - Maintenance Intervals
    117
  - Maintenance Procedures
    117
    
    Trap Inspection
    117
    
    Trap Replacement
    118
    
    Conditioning Molecular Sieve Filter
    118
- Fid
  119
  - Maintenance Intervals
    119
  - Maintenance Procedures
    120
    
    Removing/Installing Igniter
    120
    
    FID Jet
    121
    
    Removing FID Parts
    121
    
    Removing FID High Voltage Unit
    122
    
    Removing FID Jet
    123
    
    Installing FID Jet
    123
- Trouble Shooting
  126
- Error Messages (Extract)
  138
- How to Use CD-ROM
  143
- About the Provided CD-ROM
  143
- To Read the Instruction Manual in CD-ROM
  143
- Key Function List
  144

Shimadzu GC-2014 Service Manual (122 pages)

Brand: Shimadzu | Category: Laboratory Equipment | Size: 2 MB

Disclaimer
2
Product Guarantee
2
Introduction
3
Notation Used for Precautionary Information
3
Table of Contents
5
Chapter 1 Installation

9
- Installation Space
  9
  - Rear Space
    9
  - Side Space
    9
- Installation Environment
  9
- Power Supply
  11
  - Power-Supply Voltage
    11
  - Power-Supply Capacity
    11
- Gas
  12
  - Purity
    12
  - Supply Pressure
    12
Chapter 2 Configuration of Gc-2014

13
- Configuration Diagrams for GC-2014 Series
  13
  - Gc-2014A
    13
  - Gc-2014Af
    14
  - GC-2014Afsc
    15
  - Gc-2014Afspl
    15
  - Gc-2014At
    16
  - Gc-2014Atf
    17
  - Gc-2014Atfspl
    18
- Structure of GC-2014
  24
  - External Appearance
    24
  - Structure Diagram 1
    25
  - Structure Diagram 2
    26
  - Structure Diagram 3
    27
  - Sensor and Thermocouple
    27
  - Heater and PT Sensor/Thermocouple
    28
  - Fan Motor
    28
  - Fan
    29
  - Structure of Oven Cooling Unit
    30
- Electric Circuits
  31
  - Block Diagram
    31
  - CPU Unit
    32
  - Power Unit
    37
  - TCD Controller
    41
  - FID Controller
    44
  - ECD Controller
    51
  - FPD Controller
    54
  - FTD Power Controller
    58
  - Pcb aux Temp
    61
Chapter 3 Gas-Flow Controller

63
- Configuration Diagrams for Gas-Flow Controller
  63
  - Afc
    63
  - Apc
    73
    
    3Ch APC
    73
    
    2Ch APC
    74
    
    1Ch APC
    75
- Flow-Line Diagram for Gas-Flow Controller
  76
Chapter 4 Sample Injection Unit

79
Chapter 5 Detector Unit

85
- Tcd
  85
  - Det Heater Assy, Ft
    86
- Fid
  87
  - Det Heater Assy, F
    88
- Ecd
  89
- Fpd
  91
- Ftd-2014C
  93
- Ftd-2014
  95
Chapter 6 Maintenance Parts Lists

99
- Gc-2014 Main Unit
  99
- Fid-2014, Single
  100
- Fpd-2014
  100
- Ftd-2014, Capillary
  101
- Ftd-2014, Packed
  101
- Ecd-2014
  101
- Tcd-2014
  102
- D-Fid
  102
- D-Inj
  102
- Other
  102
Chapter 7 Troubleshooting

103
- Gas and Pressure/Flow-Rate Settings
  103
  - Precautions for Flow-Rate Control Settings (CAR)
    103
    
    When the Control Mode Is "SPLIT" or "SPLITLESS
    103
    
    When the Control Mode Is "TOTAL FLOW" and the Injection Mode Is
    106
    
    Direct
    106
    
    When the Control Mode Is "PRESS" or "LINEAR VELOCITY" and the Injection Mode Is "DIRECT
    106
    
    Precautions for Flow-Rate Control Settings (Detapc)
    108
- Temperature Control
  109
- Detector
  109
  - Fid
    109
  - Fpd
    110
  - Ftd
    110
- Chromatogram and Data
  110
- Other Problems
  111
Chapter 8 Service Window

113
- Flow Adjust (CAR)
  114
- Flow Adjust (Detapc)
  115
- Flow Adjust (aux APC)
  115
- Temp. Sensor Use Time
  116
- Mode
  116
- Serial Number
  117
  - Main Body Serial Number
    117
  - Unit Serial Numbers
    118
- Maintenance Log
  118
- Fan & LCD Use Time
  119
- Init. for Shipment
  119
Chapter 9 Appendix

121

Shimadzu GC-2014 Service Manual (98 pages)

Brand: Shimadzu | Category: Laboratory Equipment | Size: 1 MB

Notice
2
Product Warranty
2
Introduction
3
Listing of Part Numbers
3
Maintenance Parts Availability
3
Conventions Used for Precautionary Information
4
Table of Contents
5
Chapter 1 Installation

9
- Installation Space
  9
  - Rear Space
    9
  - Side Space
    9
- Installation Environment
  9
- Power Supply
  11
  - Power-Supply Voltage
    11
  - Power-Supply Capacity
    11
- Gas
  12
  - Purity
    12
  - Supply Pressure
    12
- Work Related Precautions
  12
Chapter 2 Configuration of GC-2014

13
- Configuration Diagrams for GC-2014 Series
  13
  - Gc-2014A
    13
  - Gc-2014Af
    14
  - GC-2014Afsc
    15
  - Gc-2014Afspl
    15
  - Gc-2014At
    16
  - Gc-2014Atf
    17
  - Gc-2014Atfspl
    18
- Structure of GC-2014
  24
  - External Appearance
    24
  - Structure Diagram 1
    25
  - Structure Diagram 2
    26
  - Structure Diagram 3
    27
  - Sensor and Thermocouple
    27
  - Heater and PT Sensor/Thermocouple
    28
  - Fan Motor
    28
  - Fan
    29
  - Structure of Oven Cooling Unit
    30
- Electric Circuits
  32
Chapter 3 Gas-Flow Controller

37
- Configuration Diagrams for Gas-Flow Controller
  37
  - Afc
    37
  - Manual Flow Controller
    39
    
    Fid
    39
    
    Ftd
    41
    
    Fpd
    43
    
    Aux
    45
  - APC (Optional)
    46
    
    3Ch APC
    46
    
    2Ch APC
    47
Chapter 4 Sample Injection Unit

49
Chapter 5 Detector Unit

55
- Tcd
  55
  - Det Heater Assy, Ft
    56
- Fid
  57
  - Det Heater Assy, F
    58
- Ecd
  59
- Fpd
  61
- Ftd-2014C
  63
- Ftd-2014
  66
Chapter 6 Maintenance Parts List

69
- Consumables
  69
  - GC-2014 Main Unit
    69
  - FID-2014 Single
    69
  - Fpd-2014
    69
  - FTD-2014 Capillary
    69
  - FTD-2014 Packed
    70
- Maintenance Parts
  71
  - GC-2014 Main Unit
    71
  - FID-2014 Single
    72
  - Fpd-2014
    72
  - FTD-2014 Capillary
    73
  - FTD-2014 Packed
    73
  - Ecd-2014
    73
  - Tcd-2014
    73
  - Dfid
    74
  - Wbi-2014
    74
  - Sinj
    74
  - Dinj
    74
  - Others
    74
Chapter 7 Troubleshooting

75
Chapter 8 Service Window

85
- Flow Adjust (CAR)
  86
- Flow Adjust (Detapc) (Options Only)
  87
- Flow Adjust (aux APC)
  87
- Temp. Sensor Use Time
  88
- Mode
  88
- Serial Number
  89
  - Main Body Serial Number
    89
  - Unit Serial Numbers
    90
- Maintenance Log
  90
- Fan & LCD Use Time
  91
- Init. for Shipment
  91
Chapter 9 Appendix

93
- GC-2014 Update Software Instruction Manual
  93
  - Overview
    93
  - Using Flush ROM Update
    93
  - Updating the GC-2014
    93
- Changes from the Previous GC-2014 Model
  95

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Shimadzu GC-2014 Manuals

Shimadzu GC-2014 Instruction Manual (318 pages)

Table of Contents

1 Installation

2 Before Use

3 Installing Packed Columns and Setting Analytical Flow Lines

4 Installing Capillary Columns and Setting Analytical Flow Lines

5 Analysis

6 Basic Key Operation

7 Starting and Stopping the GC [SYSTEM]

8 Setting the Analytical Parameters and File Management

9 Monitoring the GC

10 Starting and Stopping Analysis

11 Creating an Oven Temperature Program

12 Injection Port

13 Detector

14 Diagnosis

15 Optional Devices

16 Special Functions

17 Printing

18 Error Messages

Shimadzu GC-2014 Operation Manual (148 pages)

Table of Contents

1 General

2 Before Using GC-2014

4 Maintenance and Inspection

Shimadzu GC-2014 Service Manual (122 pages)

Table of Contents

Chapter 1 Installation

Chapter 2 Configuration of Gc-2014

Chapter 3 Gas-Flow Controller

Chapter 4 Sample Injection Unit

Chapter 5 Detector Unit

Chapter 6 Maintenance Parts Lists

Chapter 7 Troubleshooting

Chapter 8 Service Window

Chapter 9 Appendix

Shimadzu GC-2014 Service Manual (98 pages)

Table of Contents

Chapter 1 Installation

Chapter 2 Configuration of GC-2014

Chapter 3 Gas-Flow Controller

Chapter 4 Sample Injection Unit

Chapter 5 Detector Unit

Chapter 6 Maintenance Parts List

Chapter 7 Troubleshooting

Chapter 8 Service Window

Chapter 9 Appendix

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