Parr Instrument 6400 Manuals

Parr Instrument 6400 Manuals

Manuals and User Guides for Parr Instrument 6400. We have 1 Parr Instrument 6400 manual available for free PDF download: Operating Instructions Manual

Parr Instrument 6400 Operating Instructions Manual

Parr Instrument 6400 Operating Instructions Manual (110 pages)

Automatic Isoperibol Calorimeter

Brand: Parr Instrument | Category: Measuring Instruments | Size: 6.07 MB

Table of Contents

Figure

3
- Table of Contents
  3
Figure

5
Preface

6
- Purpose
  6
- Related Instructions
  6
- Scope
  6
- Explanation of Symbols
  7
- Intended Usage
  7
- Safety Information
  7
- Cleaning & Maintenance
  8
- Environmental Conditions
  8
- General Specifications
  8
- Provisions for Lifting and Carrying
  8
Table

8
Chapter

10
- Environmental Conditions
  10
Installation

10
- Swagelok Tube Fittings
  10
Table

10
- Electrical Connection
  11
- Front Panel Meter
  11
- Required Consumables, Utilities and Power Requirements
  11
- 6400 Calorimeter Back Panel
  12
- Figure 1-2
  
  12
- 6400 External Plumbing
  13
- Figure 1-3
  
  13
- Water Connection
  13
- Bomb Exhaust Connections
  14
- Gas Connection
  14
- Balance Connections
  15
- Communication Connections
  15
- Printer Connections
  15
- 6400 Calorimeter Peripherals
  16
- Figure 1-5
  
  16
- Figure
  
  16
- Figure 1-4
  
  16
- Multiple Alternate Configurations
  16
Table

17
Chapter

18
- Initial Fill
  18
Quick Start

18
Chapter

20
- Control Keys
  20
- Menu Keys
  20
- Menu System
  20
Operation

20
- Default Settings
  21
- Programming
  21
- Sample Preparation
  21
  - Figure 3-1
    
    23
  - Bucket Fill Flow Diagram
    25
    
    Figure 3-3
    25
    
    Figure 3-4
    26
    
    Pre-Period
    26
    
    Pre-Period/Post-Period Flow Diagram
    26
    
    Bomb Firing
    27
    
    Post-Period
    27
    
    Cool/Rinse
    28
    
    Figure 3-5
    28
    
    Rinse & Cool Flow Diagram
    28
- Volatile Sample Technique
  23
- Cotton Thread Assembly
  24
  - Fill Cycle
    25
- Test Process
  24
  - Closing the Bomb
    24
Figure 3-6 Drain Flow Diagram

29
Chapter

30
- Calorimeter Operation Menu
  30
  - Temperature Vs. Time Plot
    31
  - Temperature Plot Setup Menu
    31
- Main Menu
  30
Menu Descriptions

30
- Operating Controls Menu
  32
  - Spiking Controls
    32
  - Bomb Rinse Tank Controls
    33
- Program Information and Control Menu
  34
  - Software & Hardware Info
    34
  - User/Factory Settings
    35
- Calibration Data and Controls Menu
  36
  - Bomb 1
    37
  - Control Plot Chart Plot
    37
- Thermochemical Corrections Menu
  38
  - Calculation Factors Menu
    39
  - Net Heat/Dry Heat Factors
    40
- Data Entry Controls Menu
  40
- Reporting Controls Menu
  42
- Communication Controls Menu
  43
  - Balance Port Communications
    43
  - Balance Port Settings
    44
- Diagnostics Menu
  45
  - Data Logger Controls
    46
  - Data Log Items
    47
  - User Defined Buttons
    47
  - I/O Diagnostics
    47
- File Management Menu
  45
  - Run Data File Manager
    45
Chapter

48
Reports

48
Chapter

50
- Automatic Statistical Calculations
  50
- Standard Materials
  50
Standardizations

50
Chapter

54
Calculations

54
- General Calculations
  54
- Thermochemical Corrections
  54
- ASTM and ISO Methods Differ
  55
- Acid and Sulfur Corrections
  56
- Thermochemical Calculation Details
  56
- ASTM Treatment for Acid and Sulfur
  58
- ISO Calculations
  58
- Conversion to Net Heat of Combustion
  59
- Conversion to Other Moisture Bases
  59
- Spiking Samples
  59
Calculating the Heat of Combustion

54
Chapter

60
Computer Communications

60
- Computer Connections
  60
- Samba Server Feature (Optional)
  61
- 6400 Data File Naming Convention
  68
- Bar Code Port
  68
- 6400 Calorimeter Run Data Template
  69
- Table 8-2
  
  69
Chapter

70
- Clearing Memory
  70
Memory Management

70
- Removable SD Memory
  70
5 Chapter

72
- Bomb Removal
  72
- Inspection of Critical Sealing Surfaces
  72
Maintenance

72
- 50 To 100 Test Maintenance
  73
- 500 Test Maintenance
  73
- Daily Maintenance
  73
- Fuses
  73
- Quarterly Maintenance
  73
- 5000 Test Maintenance
  74
- 6400 Maintenance Checklist
  75
Bomb Exhaust Troubleshooting

76
- Troubleshooting
  76
Troubleshooting 74

77
- Jacket Temperature Troubleshooting
  77
- Error List
  78
Chapter

80
- Return for Repair
  80
Technical Service

80
Chapter

82
- A1250DD2 Controller Assembly
  82
- A1265DD Bucket and Stirrer Tube Assembly
  82
Parts Lists

82
Chapter

84
- Figure 14-1 1138 Parts Diagram
  
  84
- 1138 Parts Diagram Key
  85
Drawings

84
- Figure 14-2 6400 Cutaway Right
  
  86
  - Figure
    
    87
    
    Figure
    88
    
    A1250DD2 Control Schematic
    89
  - 6400 Cover Open
    88
- 6400 Cutaway Left
  87
  - Figure
    
    89
  - A1448DD Temperature Control Assembly
    94
  - A1455DD Propeller Assembly
    94
    
    Figure 14-11
    94
    
    A1268DD Stirrer Motor and Mount
    95
    
    Figure 14-13
    95
    
    6400 Bucket Assembly
    96
    
    Figure 14-14
    96
    
    6400 Air Can Assembly, Cutaway Left
    97
    
    Figure 14-15
    97
    
    6400 Air Can Assembly, Cutaway Front
    98
    
    Figure 14-16
    98
    
    A1450DD Bomb Head Assembly, View 1
    99
    
    Figure 14-17
    99
    
    A1450DD Bomb Head Assembly, View 2
    100
    
    Figure 14-18
    100
    
    A1050DD Rinse Collection Assembly
    101
    
    Figure 14-19
    101
    
    Figure 14-20
    102
    
    Wiring Diagram
    102
    
    Figure 14-21
    103
    
    Wiring Diagram
    103
    
    Figure 14-22
    104
    
    Fuse Diagram
    104
  - Figure 14-12
    
    94
- A1251DD Oxygen Solenoid Assembly
  90
- A1447DD Water Solenoid Assembly
  90
  - Figure
    
    90
    
    Figure
    91
    
    6400 Internal Plumbing Diagram
    92
    
    Figure
    92
    
    6400 Water Tank and Jacket Cooling Solenoid
    93
  - Figure 14-7
    
    90
  - A1456DD Rinse Valve Assembly
    91
Tables

106
- Factory Default Settings
  106
Table

106
Table

107
- Settings for ISO & BSI Methods
  108

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