Parr Instrument 6400 Operating Instructions Manual
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Parr Instrument 6400 Operating Instructions Manual

Automatic isoperibol calorimeter
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587M
6400
Automatic Isoperibol Calorimeter
Operating Instruction Manual
For models produced after October 2010

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Summary of Contents for Parr Instrument 6400

  • Page 1 587M 6400 Automatic Isoperibol Calorimeter Operating Instruction Manual For models produced after October 2010...

  • Page 3: Table Of Contents

    6400 Table of Contents Preface Closing the bomb Cool/Rinse Scope Drain Related Instructions Fill Cycle Purpose Pre-Period Explanation of Symbols Bomb Firing Safety Information Post-Period Intended Usage General Specifications Chapter 4 Environmental Conditions Menu Descriptions Provisions for Lifting and Carrying Main Menu Cleaning &...
  • Page 4 Quarterly Maintenance Standardizing the Calorimeter 50 to 100 Test Maintenance Standard Materials 500 Test Maintenance Automatic Statistical Calculations 5000 Test Maintenance 6400 Maintenance Checklist Chapter 7 Calculations Chapter 11 Calculating the Heat of Combustion Troubleshooting General Calculations Bomb Exhaust Troubleshooting...

  • Page 5: Figure

    6400 Internal Plumbing Diagram Factory Default Settings Figure 14-10 Table 15-2 6400 Water Tank and Jacket Cooling Solenoid Settings for ISO & BSI Methods w w w . p a r r i n s t . c o m...

  • Page 6: Preface

    This manual contains instructions for installing and in the respective printer package and should be operating the Parr 6400 Calorimeter. For ease of made a part of this book. use, the manual is divided into 15 chapters.

  • Page 7: Explanation Of Symbols

    3. For continued protection against possible If the instrument is used in a manner not specified hazard, replace fuses with same type and rating by Parr Instrument Company, the protection pro- of fuse. vided by the equipment may be impaired.

  • Page 8: General Specifications

    Advanced trouble- shooting instructions beyond the scope of this Frequency: Calorimeters can be operated from manual can be obtained by calling Parr Instrument either a 50 or 60 Hertz power supply without affect- Company in order to determine which part(s) may ing the operation or calibration.
  • Page 9 6400 Notes w w w . p a r r i n s t . c o m...

  • Page 10: Installation

    Environmental Conditions The 6400 Calorimeter is completely assembled and given a thorough test before it is shipped from the factory. If the user follows these instructions, instal- lation of the calorimeter should be completed with little or no difficulty.

  • Page 11: Required Consumables, Utilities And Power Requirements

    2500 psig, maximum. A red light will flash in the upper left corner of the display when the water is being cooled. The 6400 Calorimeter requires availability of ni- trogen or air, oil and water free, with appropriate connection, 2500 psig, maximum.

  • Page 12: 6400 Calorimeter Back Panel

    Installation Figure 1-2 6400 Calorimeter Back Panel P a r r I n s t r u m e n t C o m p a n y...

  • Page 13: Water Connection

    1576 Rinse Tank should be made with a piece of 1/8” distilled water through the large opening at the top nylon pressure hose (HX0012TB024). See Figure 1-3. Figure 1-3 6400 External Plumbing 06-05-07 w w w . p a r r i n s t . c o m...

  • Page 14: Gas Connection

    The A1050DD Bomb Rinse Container Assembly is the protecting cap from the tank and inspect the available as an accessory to the 6400 Calorimeter. threads on the tank outlet to be sure they are clean See Figure 14-19. This device allows for complete and in good condition.

  • Page 15: Communication Connections

    Ethernet port for connection to a computer. Sartorius Interface Field Length The 6400 will also allow the user to specify the The polarity field must con- IP addresses of one or more Balance Interface polarity tain either a “+” or a space.

  • Page 16: 6400 Calorimeter Peripherals

    Installation Figure 1-4 6400 Calorimeter Peripherals Figure 1-5 Multiple Alternate Configurations P a r r I n s t r u m e n t C o m p a n y...

  • Page 17: Table

    6400 Notes w w w . p a r r i n s t . c o m...

  • Page 18: Quick Start

    Quick Start chances for incomplete combustion). haPter 5. Carefully place the capsule into the capsule Quick Start holder, attach 10 cm of ignition thread and install the bomb head in the calorimeter. Initial Fill 6. Close the calorimeter cover making sure that the When you first fill the calorimeter with water the latch is engaged.
  • Page 19 6400 Notes w w w . p a r r i n s t . c o m...

  • Page 20: Operation

    Operation value. Some keys lead to multiple choices. haPter Always clear the current value before entering a new value. Once entered the screen will return Operation to the previous menu and the new value will be displayed in the lower right corner of the key. Menu System 4.

  • Page 21: Programming

    Programming Sample Preparation Sample Size The program in the 6400 Calorimeter can be exten- sively modified to tailor the unit to a wide variety To stay within safe limits, the bomb should never be of operating conditions, reporting units, laboratory...
  • Page 22 Operation combustions. If moisture is to be added to retard Foodstuffs and Cellulosic Materials the combustion rate, drop the water directly onto Fibrous and fluffy materials generally require one of the loose sample or onto a pellet after the sample three modes for controlling the burn rate.

  • Page 23: Volatile Sample Technique

    6400 Operation Volatile Sample Holders Use the following procedure when filling and han- Volatile samples are defined as one with an initial dling any of these tape-sealed sample holders: boiling point below 180 ºC. Volatile samples can be handled in a Parr 43AS Alloy Capsule which has a 1.

  • Page 24: Test Process

    Operation Combustion Capsules Carefully place the Non-volatile samples to be tested in Parr oxygen capsule into the capsule bombs are weighed and burned in shallow capsules holder. A cotton thread measuring approximately 1” diameter and 7/16” (845DD2) is used as an deep.

  • Page 25: Fill Cycle

    6400 Operation Fill Cycle Once the calorimeter is started and the cover is closed, the fill sequence begins. Figure 3-3 Bucket Fill Flow Diagram The calorimeter checks the bomb ignition circuitry for continuity. 2. The water fill solenoid opens and water is pumped from the internal tank into and through the bucket that surrounds the bomb.

  • Page 26: Pre-Period

    Operation Pre-Period At the completion of the fill sequence, the pre-period begins. Figure 3-4 Pre-Period/Post-Period Flow Diagram 1. The water fill solenoid valve closes and isolates the water in the bucket from the rest of the system. Water within this bucket is circulated by the stirrer. Water continues to circulate from the closed water system through the jacket surrounding the bucket.

  • Page 27: Bomb Firing

    6400 Operation Bomb Firing Post-Period Once the initial equilibrium is confirmed, the con- A minimal temperature rise will confirm that the troller initiates the firing sequence. There are no sample has ignited. After this verification, the post- changes to the circulation pattern, as shown in period begins.

  • Page 28: Cool/Rinse

    Operation Cool/Rinse At the completion of the post-period, the rinse and cool sequence begins. Figure 3-5 Rinse & Cool Flow Diagram 1. Chilled water is circu- lated through the bucket to cool the bomb to the starting temperature. 2. The release valve in the bottom of the bomb is opened and the residual pressure is released...

  • Page 29: Figure 3-6 Drain Flow Diagram

    6400 Operation Drain At the completion of the bomb rinse sequence, the drain sequence begins. Figure 3-6 Drain Flow Diagram The water in the bucket is drained out of the bucket and routed to the drain connection. Once the bucket is drained, the calorimeter may be opened to remove the bomb head and load the next sample.

  • Page 30: Menu Descriptions

    Menu Descriptions Calorimeter Operation Menu haPter The Calorimeter will normally be operated from the Menu Descriptions Calorimeter Operation Menu, although tests can always be started from any menu screen. Note: Keys which make global changes to the setup of the calorimeter contain a YES or NO response to make certain that the user wishes to proceed.

  • Page 31: Temperature Vs. Time Plot

    6400 Menu Descriptions Temperature vs. Time Plot Bucket Plot Symbol: Toggles between - » No Point » Small Dot » Round » Square » Up Triangle » Down Triangle » Diamond Bucket Min Value: Press this key to access its numeric dialog box to set a minimum bucket value.

  • Page 32: Operating Controls Menu

    Menu Descriptions Operating Controls Menu Spiking Controls Method of Operation: Offers an operating mode of Use Spiking: When set to ON, the calorimeter will prompt for the weight of the spike added either dynamic or equilibrium. In most cases, the dynamic mode with its curve matching capability and will compensate for the heat of combus- will save approximately 3-4 minutes per test and will...

  • Page 33: Bomb Rinse Tank Controls

    6400 Menu Descriptions Bomb Rinse Tank Controls Rinse Flush Time: This value is used to estab- lish a time between rinse cycles. During this time the rinse solenoid is turned OFF . This off time permits the rinse water to drain out before the next rinse cycle begins.

  • Page 34: Program Information And Control Menu

    Menu Descriptions Program Information and Control Menu Software and Hardware Info: This screen displays important information such as the main software version, I/O board information, CPU information, and IP address assigned. Software & Hardware Info Date & Time: Accesses a sub-menu to set the cur- rent date and time.

  • Page 35: User/Factory Settings

    (Note that the calorimeter will not let you fier for recalling user settings. Parr offers a exit this function without re-booting the system). unique program within the 6400 identified as Currently, there is only one bomb selection for the “64-FAST” . The program will “overlay” the 6400.

  • Page 36: Calibration Data And Controls Menu

    EE value of a bomb and bucket combination and accesses the sub-menu on which this limit is set. Note: The 6400 is a .1 Process Sigma calorim- Most test methods suggest 10 tests. Tests in excess eter.

  • Page 37: Bomb 1

    The ID can be up to 8 characters. Protect EE Value: Toggles between OFF and ON. When set to OFF , the 6400 automatically updates the EE value as new tests are run. When set to ON, it keeps the EE value protect-...

  • Page 38: Thermochemical Corrections Menu

    When any fixed correction is set to ON, the specified acid correction for determination runs. Press it on value will be used in the final reports, and the 6400 the RIGHT side to access the Acid Correction nu- will not prompt for actual corrections to be entered.

  • Page 39: Calculation Factors Menu

    6400 Menu Descriptions Calculation Factors: Accesses the Calculation Fac- Sulfur Multiplier: Values entered by the user to tors sub-menu, which provides for setting a number be used for the sulfur correction are multiplied of options for the way the thermochemical correc- by this value to get the product into units of tions are applied.

  • Page 40: Net Heat/Dry Heat Factors

    Menu Descriptions Data Entry Controls Menu Net Heat/Dry Factors: Accesses the Net Heat/Dry Factors sub-menu, which provides for setting the net heat of combustion and Dry Factors Thermochemical Corrections. Net Heat/Dry Heat Factors Prompt for Bomb ID: Toggles ON or OFF . In the ON position the controller will prompt for a Bomb ID (1-4) when a test is started.

  • Page 41: Net Heat Data Entry Controls

    6400 Menu Descriptions Hydrogen Entry Mode: This key steps through Next Auto Sample ID Number: Establishes the the options for entering hydrogen content for initial sample number for a series of tests and calculating the net heat of combustion either...

  • Page 42: Moisture Data Entry Controls

    Menu Descriptions Reporting Controls Menu Moisture as Determined (MAD) Entry Mode: This key steps through the options for entering the moisture as determined correction value either manually or through the touch screen or automatically through the balance (USB) port. Moisture as Received (MAR) Entry Mode: This key steps through the options for entering the moisture as received correction value either manually or through the touch screen or auto-...

  • Page 43: Communication Controls Menu

    6400 Menu Descriptions Communication Controls Menu Customize Balance Setting. Sets the com- munication parameters for the balance port. Standard options for data bits, parity, stop bits, handshaking, baud rate and balance type are provided to match any devices that might be connected to these ports.

  • Page 44: Balance Port Settings

    Menu Descriptions File Management Menu » Transfer Timeout (seconds). This value determines how long the interface will wait before giving up on a weight trans- fer. The value is entered in seconds. » Balance Handler Strings. This key leads to a submenu that allows balance template to be customized for unique balances or needs.

  • Page 45: File Management Menu

    6400 Menu Descriptions Run Data File Manager Diagnostics Menu The white upper portion of the Run Data File Manag- Provides the user with the means to test many of er screen presents all tests in memory in a scrollable the components and subsystems of the calorimeter.

  • Page 46: Data Logger Controls

    Menu Descriptions Data Logger Controls Data Log Items Data Logger: This key toggles the data logging Select Data Log Items: Press this key to access function ON/OFF . the Data Log Items sub-menu, which provides keys for fifteen items that can be individu- Data Log Interval: This key displays the inter- ally selected for logging.

  • Page 47: Data Log Items

    6400 Menu Descriptions User Defined Buttons I/O Diagnostics: Combine Det. Reports: Pressing this key com- Press this key to display the I/O Diagnostics sub- bines all determination reports into a single menu, which allows the user to manipulate digital file named /tmp/bigdetfile.txt.

  • Page 48: Reports

    Reports ization runs, only solution runs (not applicable to The 6400 Calorimeter can transmit its stored test the 6400) or all runs. data in either of two ways. The AUTO REPORT DESTINATION key on the Reporting Controls Menu •...
  • Page 49 6400 Notes w w w . p a r r i n s t . c o m...

  • Page 50: Standardizations

    Automatic Statistical Calculations The 6400 Calorimeter includes a provision for Hm + e1 + e2 + e3 calculating and using a mean energy equivalent for each of up to 4 separate bomb and bucket combina- tions.

  • Page 51: Calorimeter Control Limit Values In J/G When Benzoic Acid Is Used As A Test Sample

    6400 Standardizations Any outliers or other tests which should not be value by entering this number on Calibration Data & included in the average EE Value must be deleted Controls Page - Calibration Run Limit. from the memory using the memory management procedures (see Chapter 8).

  • Page 52: Calorimeter Control Limit Values In Cal/G When Benzoic Acid Is Used As A Test Sample

    Standardizations Table 6-2 Calorimeter Control Limit Values in cal/g When Benzoic Acid is Used as a Test Sample Accepted heat of combustion taken as 6318 cal/g. Instrument precision 0.10%. Control limits based on 99% confidence (3 sigma) values. Values are in cal/g. MAXIMUM PERMISSIBLE NUMBER OF UCL FOR THE RANGE...

  • Page 53: Calorimeter Control Limit Values In Btu/Lb When Benzoic Acid Is Used As A Test Sample

    6400 Standardizations Table 6-3 Calorimeter Control Limit Values in BTU/lb When Benzoic Acid is Used as a Test Sample Accepted heat of combustion taken as 11373 BTU/lb. Instrument precision 0.10%. Control limits based on 99% confidence (3 sigma) values. Values are in BTU/lb.

  • Page 54: Calculations

    It is commonly The 6400 Calorimeter will automatically make all of expressed in calories per degree Celsius. Since it the calculations necessary to produce a gross heat is directly related to the mass of the calorimeter, of combustion for the sample.

  • Page 55: Astm And Iso Methods Differ

    Since this charge is controlled by the size of the capacitor The 6400 Calorimeter can be set up to apply the acid and the charging voltage, and because the capacitor correction by either the ASTM or ISO convention, as is fully discharged for each test, the energy released the user prefers.

  • Page 56: Thermochemical Calculation Details

    The 6400 Acid Correction: Calorimeter has been programmed to permit the In the 6400 there are a number of settings for the user to use standard solutions and units which are acid correction. most convenient, since the microprocessor can easily apply any conversion factors required.
  • Page 57 6400 Calculations Using the default acid and sulfur multipliers as well as The calculated nitric acid method can be applied a heat of formation of nitric acid of 14.1 cal/milliequiv- to samples containing up to 2% nitrogen without alent a 1 gram sample with 25 ml of washings and 2...

  • Page 58: Astm Treatment For Acid And Sulfur

    ASTM procedures. correction for the sulfuric acid formed is already Provision has been made in the 6400 Controller for included in the ASTM nitric acid correction (e1). This dealing with these different procedures.

  • Page 59: Spiking Samples

    White oil is also an excellent material, by determining the moisture content of the air-dry particularly for liquid samples. The 6400 Calorimeter sample and using conversion formulae published in can automatically compensate for the addition of ASTM Method D3180 and in other references on fuel spiking materials to these samples.

  • Page 60: Computer Communications

    DNS address of the router (WAN setup) must be Computer Connections set to the IP address of the router found on the If the 6400 Calorimeter is to be connected to a LAN setup page. Other routers behave differently computer, the Ethernet connection should be used.

  • Page 61: Samba Server Feature (Optional)

    IETF RFC1001 and RFC1002. Select the PROGRAM INFORMATION AND CONTROL key from the Main Menu. Next, select FEATURE The Samba server feature option in the Parr 6400 KEY and enter the feature key purchased from Parr Calorimeter offers seamless file services to Win- Instrument Company into the instrument by using the dows based clients.
  • Page 62 Computer Communications The calorimeter offers a web server service. Test reports can be viewed with a web browser using a URL of the following form. http://10.1.5.10 Where 10.1.5.10 is the IP address of the calorimeter. The following screenshot illustrates the calorimeter home page.
  • Page 63 6400 Computer Communications Clicking on the Config button will display the screen below. Changes made on this screen will change the settings in the calorimeter. w w w . p a r r i n s t . c o m...
  • Page 64 Computer Communications Clicking on the Run Data button displays a list of reports currently in the instrument memory. Clicking on a test under the select sample ID box will display the data for the selected sample ID. P a r r I n s t r u m e n t C o m p a n y...
  • Page 65 6400 Computer Communications Clicking on the System Info button will display the screen below. w w w . p a r r i n s t . c o m...
  • Page 66 Note: This is a picture only. The calorimeter cannot be remotely operated from this screen. Remote operation requires the appropriate Feature Key. Please contact Parr Instrument Company for more details about available Feature Keys. P a r r I n s t r u m e n t C o m p a n y...
  • Page 67 6400 Computer Communications Clicking on the Documentation button will display the screen below. Clicking on any of the links will open the corresponding web page. Note: Connection to the internet is required for these links. ’ w w w . p a r r i n s t . c o m...

  • Page 68: Bar Code Port

    Next, select Feature Key and enter the feature key Pre-weigh <ID>.---.pwgh.csv purchased from Parr Instrument Company into the instrument by using the touchpad. Pressing the key labeled “ABC” allows the user to switch from upper case letters, to lower case letters, to numerals, and finally to symbols.

  • Page 69: 6400 Calorimeter Run Data Template

    6400 Computer Communications Table 8-2 6400 Calorimeter Run Data Template Field Description SampleID char[16] Timestamp MM/DD/YY HH:mm:ss Mode 0 = determination, 1 = standardization Method 0 = equilibrium, 1 = dynamic State 0 = preweigh, 1 = preliminary, 2 = final...

  • Page 70: Memory Management

    Memory Management leads to the file management sub-menu. The RUN DATA FILE MANAGER key leads to a listing of the The 6400 Calorimeter will hold data for 1000 tests files. in its memory. These tests may be pre weights, •...
  • Page 71 6400 Notes w w w . p a r r i n s t . c o m...

  • Page 72: Maintenance

    Maintenance The use of dental picks and other metallic tools to haPter pry the seals from their grooves must be avoided. These hard steel tools, if misused, can leave perma- Maintenance nent tool marks on the sealing surface, which are difficult or impossible to remove.

  • Page 73: Fuses

    6400 Maintenance Fuses 50 to 100 Test Maintenance The replacement of protective fuses for the 6400 Replace the heating wire, with 2.5” of 840DD2. Wind Calorimeter should be performed by qualified the wire 360 degrees clockwise around screws. personnel. Clean the 986DD Electrode Contact Pins with a mild abrasive, such as a pencil eraser.

  • Page 74: 5000 Test Maintenance

    The insert is keyed to the obtained by contacting Parr Instrument Company in cylinder and can not be fully inserted unless it is order to determine which part(s) may be replaced or properly oriented serviced.

  • Page 75: 6400 Maintenance Checklist

    6400 Maintenance 6400 Maintenance Checklist Quarterly Maintenance Date Date Date Date 1. Change water 2. Replace 149C 3. Clean grill on heat sink. 50 to 100 Test Maintenance Date Date Date Date 1. Replace 8400DD2 Heating Wire 2. Clean 986DD...

  • Page 76: Troubleshooting

    Troubleshooting 1. Make sure the 668DD check valve is installed at haPter the bottom of the cylinder. Troubleshooting 2. Lock the head into the cylinder and close the calorimeter lid. 3. Confirm the Exhaust is off. Bomb Exhaust Troubleshooting 4. Turn Bomb Seal on then off to retract the The bomb exhaust and sealing is controlled by 966DD2 piston.

  • Page 77: Jacket Temperature Troubleshooting

    6400 Troubleshooting Jacket Temperature Troubleshooting The third condition can be eliminated by following the procedure outlined in the section servicing the The jacket temperature is monitored with the use O-rings on the 966DD2 piston and carefully inspect- of a thermistor installed in the A1448DD tempera- ing the 1/8 nylon pressure hose and associated ture control assembly.

  • Page 78: Error List

    Troubleshooting Error List A Postperiod Timeout has Occurred The calorimeter has failed to establish an acceptable The calorimeter will run a number of diagnostic final temperature within the time allowed. checks upon itself and will advise the operator if it Possible causes for this error are listed below: detects any error conditions.
  • Page 79 6400 Troubleshooting Bomb ID – Has Been Fired – Times Which Exceeds the Bomb The heater loop break limit has been detected. The heater Service Interval. will now be shutdown. The calorimeter controller keeps track of how many This error means that the calorimeter is trying to times the bomb has been fired.

  • Page 80: Technical Service

    If you have not saved the original carton and traps, please request a packaging return kit. We prefer the calorimeter to be shipped in our cartons and traps to prevent shipping damage. Ship repair to: Parr Instrument Company Attn: Service Department RMA # XXXX 211- 53rd Street Moline, Illinois 61265...
  • Page 81 6400 Notes w w w . p a r r i n s t . c o m...

  • Page 82: Parts Lists

    Item Description A2140E I/O Board 1138/1138CL Oxygen Combustion Vessel A2141E LCD Transition Board 1795E Power Supply, 24V A2154E6 CPU Board (GCM) - 6400 1796E Power Supply, 5/12V A2163E LCD Cable 897E Capacitor, Ignition A2164E Backlight Control Cable A1250DD2 Controller Assembly...

  • Page 83: A1255Dd Bucket Stirrer Assembly

    6400 Parts Lists A1255DD Bucket Stirrer Assembly A1457DD Accessory/Installation Kit Item Description Item Description 682DD Snap Ring, Internal .50 231C2 Container, PP 10L Foldable 683DD Wave Spring, .50 OD 3415 Benzoic Acid Pellets 100 Gram Bottle 684DD Ball Bearing, .50 OD...

  • Page 84: Drawings

    Drawings haPter Drawings Figure 14-1 1138 Parts Diagram P a r r I n s t r u m e n t C o m p a n y...

  • Page 85: 1138 Parts Diagram Key

    6400 Drawings 1138 Parts Diagram Key Item Description 888DD2 Cylinder 889DD Outer Ring 821DD O-ring 1/16 ID NBR 668DD Check Valve 882DD O-ring 1/2 ID NBR 925DD Bomb Retainer SA1632RD06 (2) 8-32 x 3/8 RHMS 902DD Ground Stud Head 899DD...

  • Page 86: Figure 14-2 6400 Cutaway Right

    Drawings Figure 14-2 6400 Cutaway Right P a r r I n s t r u m e n t C o m p a n y...

  • Page 87: Figure

    6400 Drawings Figure 14-3 6400 Cutaway Left w w w . p a r r i n s t . c o m...

  • Page 88: Figure

    Drawings Figure 14-4 6400 Cover Open 1324DD2 Locking Post P a r r I n s t r u m e n t C o m p a n y...

  • Page 89: Figure

    6400 Drawings Figure 14-5 A1250DD2 Control Schematic w w w . p a r r i n s t . c o m...

  • Page 90: Figure

    Drawings Figure 14-6 A1251DD Oxygen Solenoid Assembly Figure 14-7 A1447DD Water Solenoid Assembly P a r r I n s t r u m e n t C o m p a n y...

  • Page 91: Figure

    6400 Drawings Figure 14-8 A1456DD Rinse Valve Assembly w w w . p a r r i n s t . c o m...

  • Page 92: Figure

    Drawings Figure 14-9 6400 Internal Plumbing Diagram P a r r I n s t r u m e n t C o m p a n y...

  • Page 93: 6400 Water Tank And Jacket Cooling Solenoid

    6400 Drawings Figure 14-10 6400 Water Tank and Jacket Cooling Solenoid w w w . p a r r i n s t . c o m...

  • Page 94: A1455Dd Propeller Assembly

    Drawings Figure 14-11 A1455DD Propeller Assembly Apply thread sealant (Locktite or equivalent to set screw in 1242DD2 pulley before installing. Figure 14-12 A1448DD Temperature Control Assembly P a r r I n s t r u m e n t C o m p a n y...

  • Page 95: A1268Dd Stirrer Motor And Mount

    6400 Drawings Figure 14-13 A1268DD Stirrer Motor and Mount w w w . p a r r i n s t . c o m...

  • Page 96: 6400 Bucket Assembly

    Drawings Figure 14-14 6400 Bucket Assembly P a r r I n s t r u m e n t C o m p a n y...

  • Page 97: 6400 Air Can Assembly, Cutaway Left

    6400 Drawings Figure 14-15 6400 Air Can Assembly, Cutaway Left w w w . p a r r i n s t . c o m...

  • Page 98: 6400 Air Can Assembly, Cutaway Front

    Drawings Figure 14-16 6400 Air Can Assembly, Cutaway Front P a r r I n s t r u m e n t C o m p a n y...

  • Page 99: A1450Dd Bomb Head Assembly, View 1

    6400 Drawings Figure 14-17 A1450DD Bomb Head Assembly, View 1 w w w . p a r r i n s t . c o m...

  • Page 100: A1450Dd Bomb Head Assembly, View 2

    Drawings Figure 14-18 A1450DD Bomb Head Assembly, View 2 P a r r I n s t r u m e n t C o m p a n y...

  • Page 101: A1050Dd Rinse Collection Assembly

    6400 Drawings Figure 14-19 A1050DD Rinse Collection Assembly w w w . p a r r i n s t . c o m...

  • Page 102: Wiring Diagram

    Drawings Figure 14-20 Wiring Diagram P a r r I n s t r u m e n t C o m p a n y...

  • Page 103: Wiring Diagram

    6400 Drawings Figure 14-21 Wiring Diagram w w w . p a r r i n s t . c o m...

  • Page 104: Fuse Diagram

    Drawings Figure 14-22 Fuse Diagram P a r r I n s t r u m e n t C o m p a n y...
  • Page 105 6400 Notes w w w . p a r r i n s t . c o m...

  • Page 106: Table

    Tables haPter Tables Table 15-1 Factory Default Settings Calorimeter Operations Program Information and Controls Operating Mode Determination Date XX/XX/XXXX Bomb Installed/EE 1/940.0 Time XX:XX Heater and Pump Volume Level Adjust Software and Hardware Info Operating Controls Settings Protect Method of Operation Dynamic User/Factory Settings Reporting Units...

  • Page 107: Table

    6400 Tables Determination Auto Sample ID Controls Fixed Fuse Correction ON 50.0 Automatic Sample ID Acid Correction Fixed HN03 8.0 Automatic Sample ID Number Fixed Sulfur Correction OFF 0.0 Automatic Sample ID Increment Net Heat/Dry Factors Net Heat & Dry Disable...

  • Page 108: Settings For Iso & Bsi Methods

    Tables Table 15-2 Settings for ISO & BSI Methods Page Line Setting Value Acid Correction (STD) Entered HNO Fixed Sulfur STD Thermochemical Corrections Acid Correction (DET) Entered HNO Fixed Sulfur DET Acid Multiplier 0.154 Sulfur Value is Percent Calculations Factors Sulfur Multiplier Use Offset Correction Offset Value...
  • Page 110 587M R03 02/11/14...

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