Dionex UltiMate 3000 Series Manuals

Manuals and User Guides for Dionex UltiMate 3000 Series. We have 9 Dionex UltiMate 3000 Series manuals available for free PDF download: Operating Instructions Manual, User Manual

Dionex UltiMate 3000 Series, UltiMate SR-3000 Manual

Brand: Dionex | Category: Laboratory Equipment | Size: 0 MB

Dionex UltiMate 3000 Series Operating Instructions Manual (236 pages)

SD, RS, and BM Pumps

Brand: Dionex | Category: Water Pump | Size: 2 MB

Declaration of Conformity
3
Table of Contents
9
1 Introduction

15
2 Overview

25
- Unit Description
  25
- Pump Configurations
  26
- Operating Principle
  29
- Front Panel Elements
  30
- Rear Panel
  31
  - Power Switch
    32
  - Fuse Cartridge
    32
  - USB Connector
    32
  - Digital I/O
    33
  - Solvent Rack
    33
- Fluid Connections
  34
- Rear Seal Wash System
  35
- Mixing System and Inline-Filter
  36
- Purge Unit
  37
- Leak Sensor
  37
- Vacuum Degasser
  38
- Pulse Damper
  38
- Chromeleon Software
  39
- Wellness, Predictive Performance and Diagnostics
  40
3 Installation

41
4 Preparation for Operation (Startup)

59
- Overview of Actions
  59
- General Precautions for Connecting Capillaries
  61
- Solvent Reservoirs
  62
  - General Notes
    62
  - Connecting the Solvent Reservoirs
    63
    
    All Pumps Except ISO-3100BM
    63
    
    Iso-3100Bm
    64
- Setting up the Rear Seal Wash System
  65
- Connecting Drain Tubing
  67
- Purging the Pump
  68
  - Purging the Pump Manually
    69
  - Purging the Pump by Using the Autosampler
    71
- Equilibrating the System
  72
5 Operation and Maintenance

75
- Power-Up
  75
- Status Screens
  76
- Operation with Chromeleon
  78
  - Connecting to Chromeleon
    78
  - Direct Control
    79
  - Automated Control
    82
- Function Keys and Menus on the Pump Display
  84
  - Showing the Function Keys
    84
  - Pump Menus
    86
    
    General Menu Layout and Structure
    87
    
    Main Menu
    88
    
    Control Menu
    89
    
    Preferences Menu
    89
    
    Diagnostics Menu
    90
    
    Configuration Menu
    90
- Information for Operating the Pump
  91
- Special Chromeleon Functions
  105
- Shutting down the Pump
  111
- Routine and Preventive Maintenance
  113
6 Troubleshooting

117
- Overview
  117
- Pump Block Status Indicator
  118
- Messages on the Pump Display
  119
- Chromeleon Diagnostics Messages
  126
- Operating Problems
  128
- Checking the Compression Values
  135
7 Service

137
- General Notes
  137
- Eliminating Leakage
  138
- Rear Seal Wash System
  139
  - Inspecting the Rear Seal Wash System for Leakage
    139
  - Replacing the Peristaltic Tubing
    140
  - Replacing the Detector
    141
  - Cleaning the Detector
    141
- Replacing the Check Valve Cartridges
  142
- Pistons and Piston Seals
  144
- Mixing System
  160
  - Capillary Mixer
    160
  - Static Mixer
    161
    
    Replacing the Static Mixer
    161
    
    Checking the Static Mixer for Permeability
    162
- Inline Filter
  163
- Replacing the Purge Valve Knob
  167
- Testing the Pump for Leakage
  168
- Vacuum Degasser (Rinsing the Degassing Channels)
  171
- Replacing the Main Power Fuses
  172
- Updating the Pump Firmware
  173
8 Pump-Specific Information

175
- Iso-3100
  176
  - Iso-3100Sd
    176
    
    Interior Components
    176
    
    Flow Schematic
    177
    
    Operating Principle (Schematics)
    178
  - Iso-3100Bm
    179
    
    Interior Components
    179
    
    Flow Path
    180
  - Operating Principle (Schematics)
    181
- Lpg-3400
  182
  - Interior Components
    182
  - Flow Path
    183
  - Operating Principle (Schematics)
    185
- Dgp-3600
  186
  - Interior Components
    186
  - Flow Path
    187
  - Operating Principle (Schematics)
    189
- Hpg-3200
  190
  - Interior Components
    190
  - Flow Path
    191
  - Operating Principle (Schematics)
    192
- Hpg-3400
  193
9 Optimizing the Pump for Specific Applications

197
10 Technical Information

201
11 Accessories, Consumables, and Spare Parts

205
- Standard Accessories
  205
- Optional Accessories
  211
- Consumables and Spare Parts
  213
12 Reference Information

221
- Chemical Resistance of PEEK
  221
- Solvent Miscibility
  224
- Properties of Common Solvents
  225
- Safety Information about Flammable Solvents
  226
13 Appendix

229
- Digital I/O (Pin Assignment)
  229
- Solvent Rack (Pin Assignment)
  230
14 Index

231

Dionex UltiMate 3000 Series Operating Instructions Manual (114 pages)

Fluorescence Detectors

Brand: Dionex | Category: Security Sensors | Size: 1 MB

Declaration of Conformity
3
Table of Contents
5
Introduction
9
How to Use this Manual
9
Safety Information
10
Symbols on the Instrument and in the Manual
10
General Safety Precautions
11
Consignes Générales de Sécurité
12
Intended Use
14
Federal Communications Commission (FCC) Note
15
Overview
17
Unit Description
17
Operating Principle
18
Configurations
20
Interior Components
21
Front Panel Elements
22
Rear Panel
23
Power Switch
23
Fuse Cartridge
24
USB Port
24
Analog Outputs (Optional)
24
Fluid Connections
25
Flow Cells
25
Lamp
26
Leak Sensor
26
Detector Control
27
Direct Control
27
Automated Control
27
System Wellness, Predictive Performance, and Diagnostics
28
Installation
29
Facility Requirements
29
Unpacking
29
Positioning the Detector in the Ultimate 3000 System
30
Connecting the Detector
31
General Information
31
Connecting the USB Cable
31
Connecting the Power Cord
32
Connecting the Analog Outputs (Optional)
33
Installing the DAC Module
33
Connecting an Analog Output to an Evaluation Device
34
Configuring the Analog Outputs
34
Setting up the Detector in Chromeleon
35
Loading the USB Driver for the Detector
35
Installing the Detector
37
Configuring the Detector
37
Initial Installation
37
Virtual Mode
38
Module Address
38
Device Name
39
DAC Board
39
Changing the Configuration Properties
40
Preparation for Operation (Startup)
41
Overview
41
Connecting the Drain System
41
Installing the Flow Cell
42
Equilibrating the System
44
General Guidelines for Detector Operation
46
Mobile Phases
46
Mobile Phase Delivery System
47
Flow Cells
47
Operation and Maintenance
49
Power-Up
49
Detector Display
49
Menus on the Detector Display
51
Detector Menus
52
General Menu Layout and Structure
53
Main Menu
55
Configuration Menu
56
Diagnostics Menu
57
Service Menu
57
Chromeleon Software
58
Connecting to Chromeleon
58
Direct Control
59
Automated Control
61
Smartstartup and Smartshutdown
65
Operational Settings
66
Detecting Liquid Leaks in the Detector
66
Adjusting the Screen Brightness or Contrast
66
Operational Modes of the Detector
67
Single-Channel Mode
67
Multi-Channel Mode (FLD-3400RS Only)
67
Zero Order Mode
67
Spectra Scanning
68
Optimizing Detector Performance
70
Determining the Optimum Excitation and Emission Wavelength
70
Sensitivity (Detector Sensitivity)
73
Filter Wheel Setting (FLD-3400RS Only)
75
Response Time and Data Collection Rate
76
Multi-Channel Performance
77
Flow Cell Temperature
78
Lamp Mode
78
Baseline Behavior
79
Monitoring System Functions
80
Wavelength Calibration and Verification
80
Wavelength Calibration
81
Recording the Flow Cell Temperature
81
Predictive Performance
82
Operational Qualification and Performance Qualification
82
Shutting down the Detector
82
Routine and Preventive Maintenance Intervals
84
Troubleshooting
85
Overview
85
Messages on the Detector Display
86
Operating Problems
89
Service
93
General Notes
93
Lamp
94
Flow Cell
95
Flushing the Flow Cell
95
Replacing the Flow Cell
95
Removing the Flow Cell
96
Installing the Flow Cell
97
Drying the Leak Sensor
98
Replacing the Main Power Fuses
99
Updating the Detector Firmware
100
Technical Information
103
Accessories, Consumables, and Spare Parts
105
Standard Accessories
105
Optional Accessories
106
Consumables and Spare Parts
107
Appendix: Common Mobile Phases
109
Index
111

Dionex UltiMate 3000 Series Operating Instructions Manual (120 pages)

Column Compartments

Brand: Dionex | Category: Laboratory Equipment | Size: 1 MB

Declaration of Conformity
3
Table of Contents
5
Introduction
9
Operating Instructions
9
Safety Information
10
Symbols on the TCC and in the Manual
10
General Safety Precautions
11
Consignes Générales de Sécurité
13
Intended Use
16
Federal Communications Commission (FCC) Note
16
Overview
17
Unit Description
17
Operating Principle
19
TCC Configurations
20
Front Panel Elements
21
Rear Panel
22
Power Switch
23
Fuse Cartridge
23
USB Connector
23
Digital I/O Ports
23
Interior Components
24
Gas and Humidity Sensors
25
Column Switching Valve
25
Column Identification System (Column ID)
27
Pre-Column Heater
27
Post-Column Cooler
28
Chromeleon Software
29
Direct Control
29
System Wellness, Predictive Performance, and Diagnostics
29
Installation
31
Facility Requirements
31
Unpacking
31
Positioning the TCC in the Ultimate 3000 System
32
Connecting the TCC
34
General Information
34
Connecting the USB Cable
34
Connecting the Power Cord
34
Connecting the Digital I/O
35
Setting up the TCC in Chromeleon
37
Loading the USB Driver for the TCC
37
Installing the TCC
39
Configuring the TCC
40
Initial Installation
40
Changing the Basic Configuration or Selecting Advanced Settings
42
Configuration Page
43
Preparation for Operation (Startup)
45
Overview of Actions
45
General Precautions for Connecting Capillaries
46
Opening the Column Chamber
47
Inspecting the Valve Drainage
48
Installing a Pre-Column Heater
48
Installing a Separation Column
49
Installing the Post-Column Cooler Insert
51
Connecting the Components to the Column Switching Valve
52
Connections on a 2-Position, 6-Port Column Switching Valve
53
Connections on a 2-Position, 10-Port Column Switching Valve
54
Connections on a 6-Position, 7-Port Column Switching Valve
55
Connecting the Drain System
55
Equilibrating the System
56
Operation and Maintenance
59
Power-Up
59
Status Screen
60
Operation with Chromeleon
61
Connecting to Chromeleon
61
Direct Control
62
Automated Control
65
Display Screens (Function Keys and Menus)
67
Showing the Function Keys
67
TCC Menus
68
General Menu Layout and Structure
69
Main Menu
70
Control Menu
71
Information Menu
72
Configuration Menu
73
Operational Settings
74
Selecting the Column
74
Turning on Column Thermostatting
75
Activating Column Identification (Column ID)
76
Adjusting the Sensitivity of the Gas and Humidity Sensors
77
Turning on Post-Column Thermostatting
78
Adjusting the Screen Brightness or Contrast
79
Selecting the Status Screen
79
Smartstartup and Smartshutdown
80
Special Chromeleon Functions
81
Predictive Performance
81
Diagnostics Tests
82
Recording the Temperature Signals
83
Operational Qualification und Performance Qualification
83
Shutting down the TCC
83
Routine and Preventive Maintenance
85
Troubleshooting
87
Overview
87
Messages on the TCC Display
88
Chromeleon Diagnostics Messages
91
Operating Problems
93
Service
95
General Notes
95
Removing Gases and Humidity from the Column Chamber
96
Column Switching Valve
97
Inspecting the Column Switching Valve for Leakage
98
Replacing the Valve Pod
99
Troubleshooting Tip
101
Replacing the Valve Stator
103
Rotor Seal and Stator Face Seal
104
Replacing the Rotor Seal
105
Replacing the Rotor Seal and Stator Face Seal
105
Replacing the Main Power Fuses
106
Updating the TCC Firmware
107
Technical Information
109
Accessories, Consumables, and Spare Parts
111
Standard Accessories
111
Optional Accessories
113
Consumables and Spare Parts
114
Index
117

Dionex UltiMate 3000 Series Operating Instructions Manual (114 pages)

Column Compartment

Brand: Dionex | Category: Laboratory Equipment | Size: 1 MB

Declaration of Conformity
3
Table of Contents
5
Introduction
9
How to Use this Manual
9
Safety Information
10
Symbols on the Instrument and in the Manual
10
General Safety Precautions
11
Consignes Générales de Sécurité
13
Intended Use
16
Federal Communications Commission (FCC) Note
16
Overview
17
Unit Description
17
Operating Principle
18
TCC Configurations
19
Overview
19
Column Switching Valve
20
Front Panel Elements
22
Rear Panel
23
Power Switch
24
Fuse Holder
24
USB Connector
24
Digital I/O Ports
24
Interior Components
25
Gas and Humidity Sensors
26
Column Identification System (Column ID)
26
Pre-Column Heater
27
Chromeleon Software
28
Direct Control
28
System Wellness, Predictive Performance, and Diagnostics
28
Installation
29
Facility Requirements
29
Unpacking
29
Positioning the TCC in the Ultimate 3000 System
31
Connecting the TCC
33
General Information
33
Connecting the USB Cable
33
Connecting the Power Cord
33
Connecting the Digital I/O
34
Setting up the TCC in Chromeleon
36
Loading the USB Driver for the TCC
36
Installing the TCC
38
Configuring the TCC
39
Initial Installation
39
Changing the Basic Configuration or Selecting Advanced Settings
42
Configuration Page
43
Preparation for Operation (Startup)
45
Overview of Actions
45
Opening the Front Panel Door
46
General Precautions for Connecting Capillaries
47
Installing the Valve Pod
48
Troubleshooting Tip
50
Installing a Separation Column
51
Connecting the Capillaries to the Column Switching Valve
53
Connections on a 2-Position, 6-Port Column Switching Valve
54
Connections on a 2-Position, 10-Port Column Switching Valve
55
Connections on a 6-Position, 7-Port Column Switching Valve
56
Connecting the Drain System
56
Equilibrating the System
57
Operation and Maintenance
59
Power-Up
59
Status Screen
60
Operation with Chromeleon
61
Connecting to Chromeleon
61
Direct Control
62
Automated Control
65
Display Screens (Function Keys and Menus)
67
Showing the Function Keys
67
Switching Valves
67
TCC Menus
68
General Menu Layout and Structure
68
Main Menu
70
Control Menu
71
Information Menu
72
Configuration Menu
73
Operational Settings
74
Selecting the Column
74
Turning on Column Thermostatting
75
Activating Column Identification (Column ID)
76
Adjusting the Sensitivity of the Gas and Humidity Sensors
77
Adjusting the Screen Brightness or Contrast
78
Smartstartup and Smartshutdown
78
Special Chromeleon Functions
79
Predictive Performance
79
TCC Diagnostics
80
Recording the Temperature Signal
81
Operational Qualification und Performance Qualification
81
Shutting down the TCC
81
Routine and Preventive Maintenance
83
Troubleshooting
85
Overview
85
Messages on the TCC Display
86
Chromeleon Diagnostics Messages
89
Operating Problems
90
Service
93
General Notes
93
Column Switching Valve
94
Inspecting the Column Switching Valve for Leakage
95
Replacing the Valve Pod
96
Replacing the Valve Stator
99
Rotor Seal and Stator Face Seal
100
Replacing the Rotor Seal
101
Replacing the Rotor Seal and Stator Face Seal
101
Replacing the Main Power Fuses
102
Updating the TCC Firmware
103
Technical Information
105
Accessories, Spare Parts, and Consumables
107
Standard Accessories
107
Optional Accessories
108
Consumables and Spare Parts
109
Index
111

Dionex UltiMate 3000 Series Operating Instructions Manual (114 pages)

Thermostatted Column Compartments

Brand: Dionex | Category: Laboratory Equipment | Size: 1 MB

Declaration of Conformity
3
Table of Contents
5
Introduction
9
How to Use this Manual
9
Safety Information
10
Symbols on the Instrument and in the Manual
10
General Safety Precautions
11
Consignes Générales de Sécurité
13
Intended Use
16
Federal Communications Commission (FCC) Note
16
Overview
17
Unit Description
17
Operating Principle
18
TCC Configurations
19
Overview
19
Biocompatible TCC Version
20
Column Switching Valve
21
TCC Interior Components
23
Front Panel Elements
24
Rear Panel
25
Power Switch
26
Fuse Holder
26
USB Connector
26
Digital I/O Ports
26
Gas and Humidity Sensors
27
Column Identification System (Column ID)
27
Eluent Preconditioner
28
Chromeleon Software
29
Direct Control
29
System Wellness, Predictive Performance, and Diagnostics
29
Installation
31
Facility Requirements
31
Unpacking
31
Positioning the TCC in the Ultimate 3000 System
32
Connecting the TCC
34
General Information
34
Connecting the USB Cable
34
Connecting the Power Cord
34
Connecting the Digital I/O
35
Setting up the TCC in Chromeleon
37
Loading the USB Driver for the TCC
37
Installing the TCC
39
Configuring the TCC
40
Initial Installation
40
Changing the Basic Configuration or Selecting Advanced Settings
43
Configuration Page
44
Preparation for Operation (Startup)
47
Overview of Actions
47
Opening the Front Panel Door
48
General Precautions for Connecting Capillaries
49
Installing a Separation Column
50
Connecting the Capillaries to the Column Switching Valve
52
Connections on a 2-Position, 6-Port Column Switching Valve
52
Connections on a 2-Position, 10-Port Column Switching Valve
53
Connections on a 6-Position, 7-Port Column Switching Valve
54
Connecting the Drain Tubing
55
Equilibrating the System
57
Operation and Maintenance
59
Power-Up
59
Status Screen
60
Operation with Chromeleon
61
Connecting to Chromeleon
61
Direct Control
62
Automated Control
65
Display Screens (Function Keys and Menus)
67
Showing the Function Keys
67
Switching Valves
67
TCC Menus
68
General Menu Layout and Structure
68
Main Menu
70
Control Menu
71
Information Menu
72
Configuration Menu
73
Operational Settings
74
Selecting the Column
74
Turning on Column Thermostatting
75
Activating Column Identification (Column ID)
76
Adjusting the Sensitivity of the Gas and Humidity Sensors
77
Adjusting the Screen Brightness or Contrast
78
Smartstartup and Smartshutdown
78
Special Chromeleon Functions
79
Predictive Performance
79
TCC Diagnostics
80
Recording the Temperature Signal
81
Operational Qualification und Performance Qualification
81
Shutting down the TCC
82
Routine and Preventive Maintenance
84
Troubleshooting
85
Overview
85
Messages on the Front Panel Display
86
Chromeleon Diagnostics Messages
89
Operating Problems
90
Service
93
General Notes
93
Column Switching Valve
94
Inspecting the Column Switching Valve for Leakage
95
Replacing the Valve Pod
96
Replacing the Valve Stator
99
Rotor Seal and Stator Face Seal
100
Replacing the Rotor Seal
100
Replacing the Rotor Seal and Stator Face Seal
101
Replacing the Main Power Fuses
102
Technical Information
103
Accessories, Spare Parts, and Consumables
105
Standard Accessories
105
Optional Accessories
108
Consumables and Spare Parts
109
Index
111

Dionex UltiMate 3000 Series Operating Instructions Manual (102 pages)

Flow Managers and Thermostatted Column Compartments

Brand: Dionex | Category: Analytical Instruments | Size: 2 MB

Introduction
7
Symbols on the Instrument and in the Manual
8
General Safety Precautions
9
Consignes Générales de Sécurité
11
Intended Use
14
Overview
15
Theory of Operation (Ultiflow)
17
Supported Configurations
18
Biocompatible Flow Managers
19
General Flow Manager Design
23
Column Switching Valve
24
Flow Splitter
25
Front Panel Display and Controls
26
Rear Panel Connectors
27
Leak Sensors
28
System Wellness
29
Installation
31
Positioning the Flow Manager in the Ultimate 3000 System
32
Connecting the Flow Manager
33
Digital I/O
34
Preparing the Flow Manager
35
Installing a Separation Column
37
Connecting the Capillaries to the Column Switching Valve
41
Installing a Trap Column
42
Connecting the Flow Splitter
43
Manual Injection Port
45
User Interface
47
Soft Key Menus
48
Menu Structure and Layout
49
Main Menu
51
Control Menu
52
Information Menu
53
Configuration Menu
54
Software Control by Chromeleon
55
Assigning the Flow Splitter
62
Operating the Flow Manager with Chromeleon
63
Column Identification System (Column ID)
64
Splitter Identification System (Splitter ID)
65
Diagnostics
66
Troubleshooting
67
Error Messages
68
Chromeleon Diagnostics Messages
72
Routine Maintenance
75
Maintenance Intervals
77
Flow Control Valve
78
Replacing the Fuses
79
Drying the Fluid Leak Sensor
80
Column Switching Valve
85
Shutting down the Flow Manager
87
Technical Information
89
Accessories, Consumables and Spare Parts
91
Consumables, Spare Parts, and Optional Accessories
92
Technical Appendix - Pin Assignment
97
Index
99

Dionex UltiMate 3000 Series Operating Instructions Manual (62 pages)

Brand: Dionex | Category: Laboratory Equipment | Size: 0 MB

Table of Contents
5
Introduction
7
How to Use this Manual
7
Safety Information
8
Symbols on the Instrument and in the Manual
8
General Safety Precautions
9
Consignes Générales de Sécurité
10
Intended Use
13
Federal Communications Commission (FCC) Note
13
Overview
15
Unit Description
15
SRD Configurations
15
Front Panel Elements
16
Rear Panel
17
Fluid Connections
18
Leak Sensor
19
Wellness
19
Installation
21
Facility Requirements
21
Unpacking
21
Positioning the SRD in the Ultimate 3000 System
23
Connecting the SRD
25
Connecting the SRD to an Ultimate 3000 System Pump
25
Connecting the SRD to the Main Power Supply (Optional)
25
Preparation for Operation (Startup)
27
Overview
27
Connecting Drain Tubing
27
Solvent Reservoirs
28
General Notes
28
Connecting the Solvent Reservoirs
29
Connecting the Solvent Lines from the Pump to the Degasser
31
Operation and Maintenance
33
Choosing the Solvents
33
General Notes for Degasser Operation
35
Operational Settings
36
Turning the Degasser on or off (from the Ultimate 3000 System Pump)
36
Turning the Degasser on and off from the Pump Display
36
Turning the Degasser on and off in Chromeleon
37
Turning the Degasser on or off (Stand-Alone Operation)
38
Special Chromeleon Functions
39
Leak and Vacuum Monitoring
39
SRD Diagnostics
39
Shutting down the SRD
40
Routine and Preventive Maintenance
41
Troubleshooting
43
Overview
43
Messages on the Pump Display
44
Chromeleon Diagnostics Message
44
Operating Problems
45
Service
49
General Notes
49
Rinsing the Degassing Channels
50
Eliminating Leakage in the Solvent Rack
51
Technical Information
53
Accessories, Consumables, and Spare Parts
55
Standard Accessories
55
Optional Accessories
57
Consumables and Spare Parts
57
Pin Assignment
59
15-Pin D-Sub Port
59
DC Input
59
Index
61

Dionex UltiMate 3000 Series Operating Instructions Manual (22 pages)

Solvent Rack

Brand: Dionex | Category: Laboratory Equipment | Size: 0 MB

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Laboratory Equipment Measuring Instruments Analytical Instruments Security Sensors Water Pump

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Dionex UltiMate 3000 Series Manuals

Table of Contents

Table of Contents

1 Introduction

2 Overview

3 Installation

4 Preparation for Operation (Startup)

5 Operation and Maintenance

6 Troubleshooting

7 Service

8 Pump-Specific Information

9 Optimizing the Pump for Specific Applications

10 Technical Information

11 Accessories, Consumables, and Spare Parts

12 Reference Information

13 Appendix

14 Index

Table of Contents

Table of Contents

Table of Contents

Table of Contents

Table of Contents

Table of Contents

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