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ICS-90
Dionex ICS-90 Manuals
Manuals and User Guides for Dionex ICS-90. We have
2
Dionex ICS-90 manuals available for free PDF download: Operator's Manual, Installation Instructions Manual
Dionex ICS-90 Operator's Manual (138 pages)
ION CHROMATOGRAPHY SYSTEM
Brand:
Dionex
| Category:
Laboratory Equipment
| Size: 2 MB
Table of Contents
Table of Contents
3
1 Introduction
9
Introduction to Ion Chromatography (IC)
9
Overview of the ICS-90
11
About this Manual
12
Safety Messages and Notes
13
Safety Labels
15
2 Description
17
Operating Features
18
Front Door and Top Cover
18
Rear Panel
20
Component Mounting Panel
23
Fluid Schematic
28
Displacement Chemical Regeneration (DCR)
29
The Chromeleon Interface
31
The Chromeleon Browser
31
The ICS-90 Control Panels
32
3 Operation and Maintenance
35
Preparing the Eluent
35
Preparing the Regenerant
35
Pressurizing the Eluent Reservoir
36
Preparing Samples
37
Collecting and Storing
37
Pretreating
38
Diluting
38
Operation
39
Starting up the ICS-90
39
Starting up Chromeleon
40
Preparing the ICS-90 for Operation
41
Manual Sample Processing
42
Automatic Sample Processing
43
Sample Injection
44
Maintenance
47
4 Troubleshooting
49
Alarms and Error Conditions
49
Liquid Leaks
52
Pump Difficult to Prime or Loses Prime
53
Pump Does Not Start
54
No Flow
54
Erratic Flow
54
Excessive System Backpressure
54
Peak "Ghosting
55
Nonreproducible Peak Height or Retention Time
56
Abnormal Retention Time or Selectivity
56
No DS5 Response
57
High DS5 Output
57
Baseline Noise or Drift
58
5 Service
59
Diagnostics and Calibrations
59
Calibrating the Pressure Transducer
62
Calibrating the Cell
64
Replacing Tubing and Fittings
66
Changing the Sample Loop
67
Isolating a Restriction in the Liquid Plumbing
68
Cleaning and Replacing Pump Check Valves
68
Replacing a Pump Piston Seal
70
Replacing a Pump Piston
73
Replacing the Waste Valve O-Ring
75
Rebuilding the Injection Valve
76
Installing a New DS5 Detection Stabilizer
77
Installing a New Suppressor
78
Changing the Main Power Fuses
79
A • Specifications
81
Electrical
81
Physical
81
A.1 Electrical
81
Environmental
82
Front Panel
82
A.3 Environmental
82
Rear Panel
83
Pump
83
Pulse Damper
83
A.5 Rear Panel
83
Detector
84
DS5 Detection Stabilizer
84
Injection Valve
84
Delay Volume
84
A.8 Detector
84
B • Installation
85
Facility Requirements
85
B.1 Facility Requirements
85
Unpacking the ICS-90 System
86
Unpacking the ICS-90
86
Removing the Pump Shipping Screw
87
Unpacking the Computer (North America Only
88
Unpacking the Computer (Outside North America
88
Installing Chromeleon
89
Turn on the Computer
89
B.3 Installing Chromeleon
89
Connecting the ICS-90 to the Computer
90
Connecting the Power Cord
92
Turning on the ICS-90 Power
93
Setting up Chromeleon
94
Installing the Chromeleon Software License
94
B.7 Setting up Chromeleon
94
Creating a Timebase
96
B.7.2 Creating a Timebase
96
Connecting the ICS-90 to a Chromeleon Control Panel
98
In the Browser, Open the Dionex Templates\Panels\Dionex_Ic\Ics
99
System Panels Folder and Double-Click One of the Following ICS
99
Control Panels
99
Be Used)
99
ICS-90_System_As40
99
Verifying Chromeleon Communication
101
Connecting the Waste Lines
102
Connecting the Gas Source
103
Setting up the Eluent and Regenerant Reservoirs
104
Installing and Plumbing the Columns and Suppressor
106
Pressurizing the Eluent Reservoir
109
Priming the Pump
110
Setting the Pump Flow Rate
112
Record the Measured Flow Rate in Chromeleon
115
Equilibrating the System
116
Verifying Operational Status
116
Connecting the AS40 Automated Sampler (Optional
117
Operating the ICS-90
118
Installation Troubleshooting
118
C • Reordering Information
119
D • Faq
121
How Do I Hook up an AS40 Automated Sampler
121
How Do I Print
121
How Often Should I Perform Calibrations
121
Why Are the Retention Times Moving
121
How Do I Adjust Retention Times
121
D.1 How Do I Hook up an AS40 Automated Sampler?
121
D.6 When Should I Remake Standards?
122
D.13 How Do I Know When a Column Is Dirty?
123
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Dionex ICS-90 Installation Instructions Manual (40 pages)
Ion Chromatography System
Brand:
Dionex
| Category:
Laboratory Equipment
| Size: 0 MB
Table of Contents
Table of Contents
3
Facility Requirements
5
Unpacking the ICS-90 System
6
Unpacking the ICS-90
6
Removing the Pump Shipping Screw
7
Installing the ICS-90 System
9
Installing the Chromatography Software
9
Installing the Software
9
Installing the Software License
11
Starting the Chromeleon Server Monitor
14
Connecting the ICS-90 to the Computer
15
Connecting the Power Cord
17
Turning on the ICS-90 Power
18
Setting up the Chromatography Software
19
Creating a Timebase
19
Connecting to the Control Panel
22
Verifying Communication with the ICS-90
24
Connecting the Waste Lines
25
Connecting the Gas Source
26
Setting up the Eluent and Regenerant Reservoirs
27
Installing and Plumbing the Columns and Suppressor
29
Pressurizing the Eluent Reservoir
32
Priming the Pump
33
Setting the Pump Flow Rate (ICS-90 Only)
34
Setting the Flow Rate
34
Recording the Measured Flow Rate
37
Setting the Pump Flow Rate (ICS-90A Only)
38
Equilibrating the System
38
Verifying Operational Status
39
Connecting the AS40 Automated Sampler (Optional)
39
Operating the ICS-90
40
Installation Troubleshooting
40
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