User Manuals: Dionex ICS-2100 Chromatography Equipment

Manuals and User Guides for Dionex ICS-2100 Chromatography Equipment. We have 2 Dionex ICS-2100 Chromatography Equipment manuals available for free PDF download: Operator's Manual, Installation Instructions Manual

Dionex ICS-2100 Operator's Manual (288 pages)

Dionex Ion Chromatography System

Brand: Dionex | Category: Analytical Instruments | Size: 4 MB

Table of Contents

3
- 1 Introduction
  
  13
  - Introduction to Ion Chromatography (IC)
    13
  - Overview of the ICS-2100
    16
  - About this Manual
    17
    
    Safety Messages and Notes
    18
  - Safety and Regulatory Information
    20
    
    Safety Labels
    20
- 2 Features
  
  23
  - Operating Features
    23
    
    Front Panel
    23
    
    Top Cover
    28
    
    Component Panel
    30
    
    Rear Panel
    33
  - Flow Schematics
    35
  - Chromeleon and Chromeleon Xpress
    42
    
    The Panel Tabset
    42
    
    Software Control Modes
    43
    
    System Wellness
    43
  - System Component Details
    44
    
    Vacuum Degas Assembly (Optional)
    44
    
    Eluent Valve
    46
    
    Pump
    46
    
    Eluent Generator
    49
    
    Auxiliary Power Supply (Optional)
    54
    
    Injection Valve
    54
    
    Auxiliary Valve (Optional)
    56
    
    Column Heater
    57
    
    DS6 Heated Conductivity Cell
    58
    
    Suppressor
    58
- 3 Operation and Maintenance
  
  61
  - Operation Overview
    61
  - Turning on the System Power
    63
  - Connecting to Chromeleon
    64
  - Set up the Eluent Reservoir
    66
    
    Fill the Reservoir
    66
    
    Filter the Deionized Water
    66
    
    Set the Eluent Level
    66
    
    Connect the Reservoir
    68
  - Check All Connections
    69
  - Prime the Pump
    69
  - Set System Operating Conditions
    70
  - Equilibrate the System and Verify Operational Status
    71
  - Prepare Samples
    72
    
    Collecting and Storing Samples
    72
    
    Diluting Samples
    73
    
    Pretreating Samples
    73
  - Loading and Injecting Samples
    74
    
    Loading Samples with a Syringe
    75
    
    Loading Samples with a Vacuum Syringe
    76
    
    Loading Samples with an Autosampler
    76
    
    Injecting Samples
    77
  - Processing Samples
    77
    
    Manual Sample Processing
    77
    
    Automatic (Batch) Sample Processing
    78
  - Maintenance
    80
- 4 Troubleshooting
  
  83
  - Error Messages
    83
Ics-2100 Ion Chromatography System

84
- Auxiliary Power Supply Disconnected
  86
- Auxiliary Power Supply over Current
  86
- Troubleshooting Error Messages
  86
- Auxiliary Power Supply over Voltage
  87
- Auxiliary Power Supply Stopped for Zero Flow
  87
- Column Heater Exceeds Safe Temperature
  87
- Column Heater Open Circuit
  88
- Column Heater Short Circuit
  88
- CR-TC over Current
  88
- CR-TC Stopped for Zero Flow Rate
  89
- Degas Calibration Failed
  89
- EGC Board Not Present
  89
- Calibration Error
  90
- Disconnected Error
  90
- Invalid Concentration
  90
- Invalid Concentration Vs. Flow Rate
  90
- Invalid Flow Rate
  91
- Over Current
  91
- Over Voltage
  91
- Hardware Not Present
  92
- Leak Sensor Wet
  92
- Load/Inject Valve Error
  92
- Option Not Installed
  93
- Pressure Slope Calibration Error
  93
- Pump Motor Lost Control
  93
- Pump over Pressure
  94
- Pump Pressure Hardware Error
  94
- Pump Stopped Due to Lost USB Communication Error
  94
- Pump under Pressure
  95
- Second Valve Error
  95
- Suppressor Not Connected
  96
- Suppressor over Current
  96
- Suppressor over Power
  97
- Suppressor over Voltage
  97
- Suppressor Stopped for Zero Flow Rate
  97
  - Liquid Leaks
    98
  - Pump Difficult to Prime or Loses Prime
    100
  - No Flow
    102
  - Pump Does Not Start
    102
  - Erratic Flow/Pressure Reading
    103
  - Excessive System Backpressure
    104
  - Peak "Ghosting
    105
  - Abnormal Retention Time or Selectivity
    106
  - No Cell Response
    106
  - Nonreproducible Peak Height or Retention Time
    106
  - High Cell Output
    107
  - Baseline Noise or Drift
    108
  - Vacuum Degas Assembly Does Not Run
    109
- 5 Service
  
  111
  - Diagnostic and Calibration Procedures
    111
    
    Chromeleon Wellness Panel Overview
    112
    
    Diagnostic and Calibration Touch Screen Overview
    114
    
    Calibrating the Conductivity Cell
    115
    
    Calibrating the Flow Rate
    118
    
    Calibrating the Vacuum Degas Assembly
    120
  - Isolating a Restriction in the Liquid Lines
    121
  - Replacing Tubing and Fittings
    125
  - Rebuilding the Injection Valve or Auxiliary Valve
    126
  - Replacing an Auxiliary Valve Pod
    128
  - Cleaning and Replacing the Pump Check Valves
    130
  - Replacing a Pump Piston Seal and Piston Rinse Seal
    132
  - Replacing a Pump Piston
    136
  - Replacing the Waste Valve or Priming Valve O-Ring
    137
  - Replacing the Conductivity Cell
    139
  - Replacing the Suppressor
    142
  - Replacing the Column Heater
    143
  - Replacing the Column Heater Heat Exchanger
    146
  - Replacing the Eluent Valve
    147
  - Replacing the Leak Sensor
    149
  - Priming the Pump
    150
    
    Priming the Eluent Lines with a Syringe
    150
    
    Priming with the Prime Button
    152
  - Priming the Pump with Isopropyl Alcohol
    153
  - Changing Main Power Fuses
    154
  - Replacing an Elugen Cartridge
    155
    
    Elugen Cartridge
    155
    
    Replacing a KOH, Lioh, MSA, or Naoh
    155
    
    Replacing a K2CO3 Cartridge
    163
  - Replacing the CR-TC
    177
  - Replacing the EPM Electrolytic Ph Modifier
    181
    
    Recording the EPM Serial Number in Chromeleon
    182
    
    Plumbing the EPM for Hydrating and Conditioning
    183
    
    Hydrating and Conditioning the EPM
    185
  - Replacing the EGC CO3 Mixer
    186
    
    Installing the New EGC CO3 Mixer
    186
    
    Filling the EGC CO3 Mixer with Deionized Water
    187
    
    Filling the EGC CO3 Mixer with Eluent
    190
  - Replacing the EGC Holder and Degas Assembly
    197
    
    Disconnecting and Removing the Elugen Cartridge
    197
    
    In the New EGC Holder
    200
    
    In the New EGC Holder
    202
    
    Installing the New EGC Holder Without a CR-TC
    204
    
    Or EPM
    204
    
    Reinstalling the Elugen Cartridge
    205
- A • Specifications
  
  207
  - Electrical
    207
  - Physical
    207
    
    A.1 Electrical
    207
    
    A.2 Physical
    207
  - Environmental
    208
  - Front Panel
    208
  - Analytical Pump and Fluidics
    208
    
    A.3 Environmental
    208
    
    A.4 Front Panel
    208
    
    A.5 Analytical Pump and Fluidics
    208
  - Eluent Generation
    210
  - A.6 Eluent Generation
    210
  - Detector Electronics
    212
  - A.7 Detector Electronics
    212
  - Conductivity Cell with Heat Exchanger
    212
  - Injection Valve
    214
  - Auxiliary Valve (Optional)
    214
  - A.9 Injection Valve
    214
  - Vacuum Degas Assembly
    214
  - Column Heater
    214
  - Auxiliary Power Supply (Optional)
    214
  - Suppressors
    215
  - Autosampler
    216
  - System Software
    216
- B • Touch Screen Operation
  
  219
  - Using the Touch Screen
    219
  - Using the Touch Screen with Chromeleon
    222
  - Overview of ICS-2100 Touch Screen
    223
  - Home Page
    224
    
    B.4 Home
    224
    
    Home Page Pump Controls
    224
    
    Home Page Column Heater
    226
    
    Home Page EGC Controls
    226
    
    Home Page Detector Controls
    227
    
    Home Page Injection Valve Controls
    227
    
    B.4.6 Other Home Page Controls
    228
    
    Other Home Page Controls
    228
  - Plot Page
    229
  - B.5 Plot
    229
  - Status Page
    230
    
    B.6 Status
    230
    
    Viewing Other Status Parameters
    232
    
    Status Parameter Details
    233
  - Pump Page
    235
    
    B.7 Pump
    235
    
    The Pressure Unit
    235
    
    Setting Degas Operating Parameters (Optional)
    236
    
    Controlling the Eluent Valve
    237
  - Eluent Generator Page
    238
    
    B.8 Eluent Generator
    238
    
    EGC Serial Number
    238
    
    Setting the Eluent Concentration
    239
    
    Controlling the Eluent Generator Power
    240
    
    Monitoring the Elugen Cartridge Life
    240
    
    Controlling the CR-TC Power
    241
  - Suppressor Page
    242
  - B.9 Suppressor
    242
  - Detector Page
    243
    
    Selecting the Conductivity Polarity
    244
    
    Setting the Data Rise Time
    244
    
    Setting Analog out Options
    245
  - Information Page
    246
  - Module Setup Page
    247
  - Input/Output Page
    248
  - Diagnostic and Calibration
    248
- C • TTL and Relay Control
  
  251
- D • Reordering Information
  
  263
- E • Faq
  
  267
  - How Do I Hook up an Autosampler
    267
  - How Do I Print
    267
  - Why Are the Retention Times Moving
    267
  - How Do I Adjust Retention Times
    267
  - When Should I Remake Standards
    267
  - When Should I Replace the Eluent Generator Cartridge
    268
  - How Do I Start Chromeleon
    268
  - How Do I Delete Data
    268
  - How Do I Back up Data
    268
  - How Do I Shut off the System
    268
  - How Do I Store Columns
    268
  - How Do I Know When a Column Is Dirty
    269
  - How Do I Clean a Column
    269
  - Why Is the Conductivity High
    269
  - How Do I Configure and Operate the Auxiliary Valve
    269
- F • Glossary
  
  271

Dionex ICS-2100 Installation Instructions Manual (110 pages)

Ion Chromatography System

Brand: Dionex | Category: Laboratory Equipment | Size: 2 MB

Dionex Categories

Laboratory Equipment Measuring Instruments Analytical Instruments Security Sensors Water Pump

More Dionex Manuals

User Manuals: Dionex ICS-2100 Chromatography Equipment

Dionex ICS-2100 Operator's Manual (288 pages)

Table of Contents

Table of Contents

1 Introduction

2 Features

3 Operation and Maintenance

4 Troubleshooting

Ics-2100 Ion Chromatography System

5 Service

A • Specifications

B • Touch Screen Operation

C • TTL and Relay Control

D • Reordering Information

E • Faq

F • Glossary

Dionex ICS-2100 Installation Instructions Manual (110 pages)

Table of Contents

1 Facility Requirements

2 Unpacking the IC System

3 Connecting an Autosampler (Optional)

4 Unpacking the PC

5 Installing Chromeleon

6 Installing the Chromeleon Software License Dongle

7 Installing the Software License

8 Starting the Chromeleon Server

9 Connecting to the Chromeleon PC

10 Connecting the Power Cord

11 Installing the ICS-2100 Device Driver

12 Setting up Chromeleon

13 Installing and Plumbing the Columns and Suppressor

14 Connecting the Waste Lines

15 Setting up the Eluent Reservoir

16 Entering the Eluent Level

17 Priming the Pump

18 Setting up the Eluent Generator

19 Equilibrating the System

20 Verifying Operational Status

21 Connecting the Analog Output (Optional)

22 Pressurizing the Eluent Reservoir (Optional)

23 Connecting the Pump Continuous Seal Wash (Optional)

24 Sample Processing Overview

25 Troubleshooting the USB Configuration Error

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