Dionex ICS-900 Ion Chromatography System Manuals

Dionex ICS-900 Ion Chromatography System Manuals

Manuals and User Guides for Dionex ICS-900 Ion Chromatography System. We have 1 Dionex ICS-900 Ion Chromatography System manual available for free PDF download: Operator's Manual

Dionex ICS-900 Operator's Manual

Dionex ICS-900 Operator's Manual (142 pages)

Ion Chromatography System

Brand: Dionex | Category: Laboratory Equipment | Size: 7 MB

Table of Contents

Table of Contents

3
- 1 Introduction
  
  9
  - Overview of the ICS-900
    9
  - The ICS-900 Operator's Manual
    10
    
    Overview
    10
  - Safety and Regulatory Information
    11
    
    Safety Messages and Notes
    11
    
    Safety Symbols
    13
    
    Declaration of Conformity
    14
- 2 Description
  
  15
  - Operating Features
    15
    
    Front Door and Top Cover
    15
    
    Component Mounting Panel
    17
    
    Rear Panel
    19
  - Fluid Schematic
    22
  - System Component Details
    24
    
    Pump
    24
    
    Pressure Transducer
    25
    
    Injection Valve with Sample Loop
    26
    
    MMS 300 Micromembrane Suppressor
    27
    
    Displacement Chemical Regeneration (DCR)
    28
    
    Conductivity Cell and DS5 Detection Stabilizer
    29
  - Chromeleon and Chromeleon Xpress Software
    31
    
    The Panel Tabset
    31
    
    Software Control Modes
    32
    
    System Wellness and Predictive Performance
    33
- 3 Operation and Maintenance
  
  35
  - Operation Overview
    35
  - Turning on the ICS-900 Power
    36
  - Connecting to Chromeleon or Chromeleon Xpress
    36
  - Preparing the Eluent
    37
  - Preparing the Regenerant
    38
  - Priming the Pump
    40
  - Equilibrating the System
    43
  - Verifying Operational Status
    43
  - Configuring Standby Mode
    44
  - Preparing Samples
    45
    
    Collecting and Storing
    45
    
    Pretreating
    45
    
    Diluting
    46
  - Processing Samples
    47
    
    Overview
    47
    
    Manually Processing Samples
    48
    
    Automatically Processing Samples (Batch Processing)
    50
    
    Loading and Injecting Samples with an Autosampler
    52
    
    Loading and Injecting Samples with a Syringe
    54
    
    Example Chromeleon Commands for Loading and Injecting Samples
    56
  - Maintenance
    57
- 4 Troubleshooting
  
  59
  - Alarms and Error Conditions
    59
Ics-900 Operator's Manual

60
- Flow Rate Calibration Error
  61
- Load/Inject Valve Error
  61
- Module Data Buffer Overflow. Data May Have Been Lost
  62
- Pump Motor Lost Control
  62
- Pump Pressure Hardware Error
  62
- Pump Pressure Slope Calibration Error
  63
- Remaining Eluent below 200 Ml
  63
- The System Pressure Has Exceeded the High Pressure Limit
  64
- The System Pressure Is below the Low Pressure Limit
  64
- To Troubleshoot
  64
  - Liquid Leaks
    65
  - Pump Difficult to Prime or Loses Prime
    66
  - Pump Does Not Start
    67
  - No Flow
    67
  - Erratic Flow/Pressure Reading
    67
  - Excessive System Backpressure
    68
  - Peak "Ghosting
    68
  - Nonreproducible Peak Height or Retention Time
    69
  - Abnormal Retention Time or Selectivity
    69
  - No Detector Response
    70
  - High Detector Output
    70
  - Baseline Noise or Drift
    71
- 5 Service
  
  73
  - Diagnostics and Calibrations
    73
    
    Opening the Wellness Panel
    73
    
    Wellness Panel Features
    75
    
    Calibrating the Pressure Transducer
    77
    
    Calibrating the Cell
    78
    
    Calibrating the Flow Rate
    80
  - Replacing Tubing and Fittings
    81
  - Isolating a Restriction in the Liquid Plumbing
    82
  - Eluent in
    83
  - Cleaning Eluent Bottles
    84
  - Changing the Sample Loop
    84
  - Cleaning and Replacing Pump Check Valves
    85
  - Replacing a Pump Piston Seal and Backup Seal
    88
  - Replacing a Pump Piston
    94
  - Replacing the Waste Valve Seal
    95
  - Rebuilding the Injection Valve
    96
  - Replacing the Conductivity Cell
    98
    
    Eluent out
    98
  - Replacing the Suppressor
    99
  - Changing the Main Power Fuses
    100
- A • Specifications
  
  101
  - Electrical
    101
  - Physical
    101
  - Environmental
    101
  - Front and Rear Panel Leds
    102
  - Pump
    102
  - Injection Valve
    103
  - Suppressors
    103
  - A.6 Injection Valve
    103
  - Column Heater/Thermostat
    104
  - Conductivity Detector and Flow Cell
    104
  - Autosampler
    105
  - System Software
    106
- B • Reordering Information
  
  107
- C • TTL and Relay Control
  
  109
- D • Faq
  
  121
  - How Do I Connect to an Autosampler
    121
  - How Often Should I Perform Calibrations
    121
  - Why Are the Retention Times Moving
    121
  - How Do I Adjust Retention Times
    122
  - When Should I Remake Standards
    122
  - When Should I Remake Eluents
    122
  - How Do I Start Chromeleon or Chromeleon Xpress
    122
  - How Do I Back up Data
    122
  - How Do I Delete Data
    122
  - How Do I Shut off the System
    123
  - How Do I Store Columns
    123
  - How Do I Know When a Column Is Dirty
    123
  - How Do I Clean a Column
    123
  - Why Is the Conductivity High
    123
- E • Introduction to Ion Chromatography (IC)
  
  125
- F • Glossary
  
  127
- Index
  
  133

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