Dionex ICS-1100 Manuals

Manuals and User Guides for Dionex ICS-1100. We have 2 Dionex ICS-1100 manuals available for free PDF download: Operator's Manual, Installation Instructions Manual

Dionex ICS-1100 Operator's Manual (168 pages)

Ion Chromatography System

Brand: Dionex | Category: Laboratory Equipment | Size: 2 MB

Printing History
2
Table of Contents
3
Introduction
11
Introduction to Ion Chromatography (IC)
11
Overview of the ICS-1100
14
About this Manual
15
Safety Messages and Notes
16
Safety and Regulatory Information
18
Safety Labels
18
Features
21
Operating Features
21
Front Panel
21
Top Cover
23
Component Panel
24
Right-Side Panel
27
Rear Panel
28
Flow Schematics
30
Chromeleon and Chromeleon Xpress
34
The Panel Tabset
34
Software Control Modes
35
System Wellness
35
System Component Details
36
Vacuum Degas Assembly (Optional)
36
Eluent Valve
38
Pump
38
Injection Valve
40
Auxiliary Valve (Optional)
42
Column Heater (Optional)
43
Suppressor
44
DS6 Heated Conductivity Cell
44
ER Controller
45
Operation and Maintenance
47
Operation Overview
47
Turning on the System Power
49
Connecting to Chromeleon
50
Set up the Eluent Reservoir
51
Prepare the Eluent
51
Degas the Eluent
52
Filter the Eluent
53
Fill the Reservoir
53
Set the Eluent Level
53
Connect the Reservoir
54
Check All Connections
54
Prime the Pump
55
Set System Operating Conditions
56
Equilibrate the System and Verify Operational Status
56
Prepare Samples
57
Collecting and Storing Samples
57
Pretreating Samples
58
Diluting Samples
58
Loading and Injecting Samples
59
Loading Samples with a Syringe
60
Loading Samples with a Vacuum Syringe
60
Loading Samples with an Autosampler
61
Injecting Samples
62
Processing Samples
62
Manual Sample Processing
62
Automatic (Batch) Sample Processing
63
Maintenance
65
Troubleshooting
67
Error Messages
67
Troubleshooting Error Messages
69
Column Heater Exceeds Safe Temperature
69
Column Heater Open Circuit
69
Column Heater Short Circuit
69
Degas Calibration Failed
70
Hardware Not Present
70
Leak Sensor Wet
70
Load/Inject Valve Error
71
Option Not Installed
71
Pressure Slope Calibration Error
71
Pump Motor Lost Control
72
Pump over Pressure
72
Pump Pressure Hardware Error
72
Pump Stopped Due to Lost USB Communication Error
73
Pump under Pressure
73
Second Valve Error
73
Suppressor Not Connected
74
Suppressor over Current
74
Suppressor over Power
75
Suppressor over Voltage
75
Suppressor Stopped for Zero Flow Rate
75
Liquid Leaks
76
Pump Difficult to Prime or Loses Prime
78
Pump Does Not Start
80
No Flow
80
Erratic Flow/Pressure Reading
81
Excessive System Backpressure
82
Peak "Ghosting
83
Nonreproducible Peak Height or Retention Time
84
Abnormal Retention Time or Selectivity
84
No Cell Response
85
High Cell Output
85
Baseline Noise or Drift
86
Vacuum Degas Assembly Does Not Run
87
Service
89
Diagnostic and Calibration Procedures
89
Chromeleon Wellness Panel Overview
90
Calibrating the Conductivity Cell
91
Calibrating the Flow Rate
93
Calibrating the Vacuum Degas Assembly
94
Isolating a Restriction in the Liquid Lines
94
Replacing Tubing and Fittings
97
Rebuilding the Injection Valve or Auxiliary Valve
98
Replacing an Auxiliary Valve Pod
100
Cleaning and Replacing the Pump Check Valves
102
Replacing a Pump Piston Seal and Piston Rinse Seal
104
Replacing a Pump Piston
108
Replacing the Waste Valve or Priming Valve O-Ring
109
Replacing the Conductivity Cell
111
Replacing the Suppressor
113
Replacing the Column Heater
115
Replacing the Column Heater Heat Exchanger
117
Replacing the Eluent Valve
118
Replacing the Leak Sensor
120
Priming the Pump
121
Priming the Eluent Lines with a Syringe
121
Priming with the Prime Button
123
Priming the Pump with Isopropyl Alcohol
124
Changing Main Power Fuses
125
A • Specifications
127
Electrical
127
Physical
127
Environmental
128
Front Panel
128
Analytical Pump and Fluidics
128
Eluent Regeneration
130
Detector Electronics
130
Conductivity Cell with Heat Exchanger
132
Injection Valve
132
Auxiliary Valve (Optional)
132
Vacuum Degas Assembly (Optional)
132
Column Heater (Optional)
133
Suppressors
134
Autosampler
135
System Software
135
B • TTL and Relay Control
139
TTL and Relay Connections
139
Selecting TTL Input Functions and Control Types
141
Controlling TTL and Relay Outputs
143
C • Reordering Information
145
D • Faq
149
How Do I Hook up an Autosampler
149
How Do I Print
149
Why Are the Retention Times Moving
149
How Do I Adjust Retention Times
149
When Should I Remake Standards
149
When Should I Remake Eluents
150
How Do I Start Chromeleon
150
How Do I Delete Data
150
How Do I Back up Data
150
How Do I Shut off the System
150
How Do I Store Columns
150
How Do I Know When a Column Is Dirty
150
How Do I Clean a Column
151
Why Is the Conductivity High
151
How Do I Configure and Operate the Auxiliary Valve
151
E • Glossary
153

Dionex ICS-1100 Installation Instructions Manual (52 pages)

Ion Chromatography System

Brand: Dionex | Category: Laboratory Equipment | Size: 1 MB

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