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Buchi UniversalExtractor E-800 Operation Manual
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Buchi UniversalExtractor E-800 Operation Manual

Buchi UniversalExtractor E-800 Operation Manual

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Operation Manual
UniversalExtractor E-800

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Summary of Contents for Buchi UniversalExtractor E-800

  • Page 1 Operation Manual UniversalExtractor E-800...
  • Page 2 CH-9230 Flawil 1 E-Mail: quality@buchi.com BUCHI reserves the right to make changes to the manual as deemed necessary in the light of experience, especially with respect to structure, illustrations and technical details. This manual is copyrighted. Information from it may neither be reproduced, distributed, or used for competitive purposes, nor made available to third parties.
  • Page 3 Upper connections on the rear side .................. 21 3.2.6 Lower connections on the rear side .................. 22 3.2.7 Installation board........................ 23 Type plate ............................ 24 Scope of delivery .......................... 24 Technical data ...........................  24 3.5.1 UniversalExtractor E-800 ..................... 24 3.5.2 Ambient conditions....................... 25 3.5.3 Materials .......................... 26 Operation Manual UniversalExtractor E-800...
  • Page 4 Installing two protection shields (extraction glass chamber universal only)...... 36 5.11.2 Installing one protection shield (Hot Extraction with beaker only)........ 37 5.12 Preparing the condenser ........................ 37 5.13 Preparing the tank bottle........................ 40 5.14 Disassembling the condenser circuit .................... 41 Operation Manual UniversalExtractor E-800...
  • Page 5 Changing the heating level of a solvent ................ 58 6.7.5 Changing the boiling point of a solvent ................ 58 6.7.6 Changing the enthalpy of a solvent.................. 59 6.7.7 Changing the molecular weight of a solvent ................ 59 6.7.8 Changing the density of a solvent.................. 60 Operation Manual UniversalExtractor E-800...
  • Page 6 Solvent table ............................ 76 11.3 Spare parts and accessories ...................... 77 11.3.1 Accessories.......................... 77 11.3.2 Spare parts .......................... 78 11.3.3 Recirculating chiller...................... 81 11.3.4 Consumables ........................ 81 11.3.5 Glass sample tubes and extraction thimbles ............... 81 11.3.6 Holder for extraction thimbles .................... 82 Operation Manual UniversalExtractor E-800...
  • Page 7 Indicates a danger that could result in damage to property. 1.2 Symbols The following symbols are displayed in this operation manual or on the device: 1.2.1 Warning symbols Symbol Meaning General warning Hot surface Breakable items Hand injuries Flammable substances Operation Manual UniversalExtractor E-800 7/84...
  • Page 8 Signals are marked-up like this. 1.3 Trademarks Product names and registered or unregistered trademarks that are used in this document are used only for identification and remain the property of the owner in each case. 8/84 Operation Manual UniversalExtractor E-800...
  • Page 9 2.1 Proper use The UniversalExtractor E-800 is designed for the extraction (solid-liquid extraction) of samples with known solvents or solvent mixtures and the reduction or drying of the extract. The UniversalExtractor E-800 can be used in laboratories for the following tasks: —...
  • Page 10 Safety-related incidents that occur while using the instrument should be reported to the manufacturer (quality@buchi.com). BUCHI service technicians Service technicians authorized by BUCHI have attended special training courses and are authorized by BÜCHI Labortechnik AG to carry out special servicing and repair measures.
  • Page 11 If faults occur: — Switch off the device immediately. — Unplug the power cord. — Inform the operator. — Cool the device before taking any further action. Do not continue to use devices that are damaged. Operation Manual UniversalExtractor E-800 11/84...
  • Page 12 Make sure that the decontamination agent is compatible with the materials used. See Chapter 3.5 “Technical data”, page 24 If you have any further questions, contact BUCHI Customer Service. 2.6.8 Solvent leakages during extraction process Solvent leaking systems can cause dangerous solvent vapors that lead to instrument damage or fire.
  • Page 13 Unauthorized modifications can affect safety and lead to accidents. Use only genuine BUCHI accessories, spare parts and consumables. Carry out technical changes only with prior written approval from BUCHI. Only allow changes to be made by BUCHI service technicians. BUCHI accepts no liability for damage, faults and malfunctions resulting from unauthorized modifications.
  • Page 14 3 | Product description BÜCHI Labortechnik AG 3 Product description 3.1 Description of function The UniversalExtractor E-800 is designed to carry out the following solid-liquid extraction methods: — Hot Extraction (without chamber heater). See Chapter 3.1.1 “Hot Extraction (with Hot Extraction beaker)”, page 14 —...
  • Page 15 The magnetic valve is open, the solvent extracts the analyte and flows back into the beaker. Step 2 drying — The solvent is heated, vapor rises up to the condenser, condenses and flows into the tank bottle. — The analyte remains in the beaker. Operation Manual UniversalExtractor E-800 15/84...
  • Page 16 The magnetic valve is open, the solvent flows back into beaker, the solvent is not collected. Step 3 drying — The solvent is heated, vapor rises up to the condenser, condenses and flows into tank. — The analyte remains in the beaker. 16/84 Operation Manual UniversalExtractor E-800...
  • Page 17 Presence of beaker Presence of solvent (Level check) Extraction step - X¹ X¹ X¹ X¹ X¹ Rinse step X¹ X¹ X¹ X¹ Dry step X¹ X¹ X¹ X¹ X¹ ¹ activation inert gas Operation Manual UniversalExtractor E-800 17/84...
  • Page 18 Protection shield Condenser rack Chamber rack Condenser tank bottle Installation board Tank bottle Heating plate Analyte protection sensor Beaker rack 10 Chamber heater 11 Inert gas connection 12 On/Off master switch (option) 13 Pro Interface 18/84 Operation Manual UniversalExtractor E-800...
  • Page 19 3.2.2 Front View (without chamber heater) Fig. 3: Front view Protection shield Condenser rack Chamber rack Condenser tank bottle Tank bottle Beaker rack Installation board Analyte protection sensor Heating plate 10 On/Off master switch 11 Pro Interface Operation Manual UniversalExtractor E-800 19/84...
  • Page 20 3 | Product description BÜCHI Labortechnik AG 3.2.3 Front view (HE beaker) Fig. 4: Front view Protection shield Condenser rack Condenser tank bottle Tank bottle Beaker rack Installation board Heating plate On/Off master switch Pro Interface 20/84 Operation Manual UniversalExtractor E-800...
  • Page 21 3.2.5 Upper connections on the rear side Fig. 6: Connections on the top Standard BUCHI communication port Standard BUCHI communication port (COM) (COM) LAN port Port for the cooling water valve Operation Manual UniversalExtractor E-800 21/84...
  • Page 22 Fuse Inert gas connection (option) INERT (marked Coolant water out Exhaust EXHAUST (marked (marked Coolant water in 10 Type plate (marked 11 Coolant water solvent tank out 12 Solvent out TANK OUT (SOLVENT) (marked (marked 22/84 Operation Manual UniversalExtractor E-800...
  • Page 23 Chamber rack Universal FatExtractor E-500 only FatExtractor E-500 only Condenser rack Hot Extraction FatExtractor E-500 only Beaker rack Hot Extraction Beaker rack Universal 10 Solvent collector tube 11 Sensor plugs 12 Attachment clip for tube 13 Lift Operation Manual UniversalExtractor E-800 23/84...
  • Page 24 Pollution degree Dimensions (W x D x H) 638 x 595 x 613 mm (without glassware) Dimensions (W x D x H) 638 x 595 x 752 mm (with glassware Universal) Weight 44.8 kg (without glassware) 24/84 Operation Manual UniversalExtractor E-800...
  • Page 25 Max. altitude above sea level 2000 m Ambient temperature 5‒40 °C Maximum relative humidity 80% for temperatures up to 31 °C decreasing linearly to 50 % relative humidity at 40 °C Storage temperature max. 45 °C Operation Manual UniversalExtractor E-800 25/84...
  • Page 26 Steel 1.4301/304 with powder coating Exhaust Aluminium coated Protection shield PMMA GS Glass ware Borosilikat 3.3 Sealings glassware PTFE (with FKM core) Tank bottle Borosilikat 3.3 Tank bottle valve PTFE / FFKM Sealing solvent connection PTFE Tubing 26/84 Operation Manual UniversalExtractor E-800...
  • Page 27 The instrument should be transported by two persons at the same time. Lift the instrument at the points indicated. NOTICE Dragging the instrument can damage the feet of the instrument. Lift the instrument when positioning or re-locating. Operation Manual UniversalExtractor E-800 27/84...
  • Page 28 4 | Transport and storage BÜCHI Labortechnik AG Fig. 10: Lifting the instrument Lift the instrument – this requires two persons each lifting at the points indicated on the left and right side of the instrument. 28/84 Operation Manual UniversalExtractor E-800...
  • Page 29 Provide the mains voltage and frequency specified on the type plate of the instrument. Be designed for the load imposed by the instruments connected. Be equipped with suitable fuses and electrical safety features. Be equipped with a proper grounding. Operation Manual UniversalExtractor E-800 29/84...
  • Page 30 Risk of instrument damage because of not suitable power supply cables. Not suitable power supply cables can cause bad performance or an instrument damage Use only BUCHI power supply cables. Make sure that all connected devices are grounded. Make sure that the power plug is freely accessible at all times.
  • Page 31 Attach a solvent connection nut with seals to the connection marked Attach a solvent connection nut with seals to the IN (SOLVENT) connection marked Attach the inlet tube onto the connection marked Attach the drain tube onto the connection IN (SOLVENT) marked Operation Manual UniversalExtractor E-800 31/84...
  • Page 32 5.8 Connecting inert gas (option) 5.8.1 Connecting inert gas to the instrument (option) Precondition: Make sure that the instrument is not connected to the power supply. Attach the inert gas tube onto the connection INERT marked 32/84 Operation Manual UniversalExtractor E-800...
  • Page 33 Connect the inert gas tube. 5.9 Preparing the extraction glass chamber universal NOTICE Risk of broken parts by using tools Using tools for preparing the instrument can break parts. Tighten all parts with your hands. Operation Manual UniversalExtractor E-800 33/84...
  • Page 34 Install the extraction glass chamber according to following instructions. Precondition: The configuration is set to Universal. See Selecting a configuration Prepare the extraction glass chamber universal. See Chapter 5.9 “Preparing the extraction glass chamber universal”, page 33 34/84 Operation Manual UniversalExtractor E-800...
  • Page 35 Pull the chamber rack. Precondition: Start with the extraction glass chamber on the left side. Make sure that the BUCHI Logo points to the front. Put the extraction glass chamber in the chamber rack. Turn the extraction glass chamber 45°...
  • Page 36 Make sure, that both protections shields fit together. Hold both protection shields on both sides at the point indicated. Put the rear protection shield on both sides into the rear slot at the same time. 36/84 Operation Manual UniversalExtractor E-800...
  • Page 37 Put the protection shield on both sides into the front slot at the same time. 5.12 Preparing the condenser NOTICE Risk of broken parts by using tools Using tools for preparing the instrument can break parts. Tighten all parts with your hands. Operation Manual UniversalExtractor E-800 37/84...
  • Page 38 Put the sealing on the bottom of the condenser. Attach the solvent connection nut with the seal to the condenser. Connect the solvent collector tube. NOTICE! Do not use force to carry out this action step. Put the condenser in the condenser rack. 38/84 Operation Manual UniversalExtractor E-800...
  • Page 39 Secure the condenser with the flange lock. Turn the condenser. Connect the solvent collector tube to the installation board Attach the tubes with the attachment clip to the installation board. Connect the condensers. Establish a condenser circuit. Operation Manual UniversalExtractor E-800 39/84...
  • Page 40 Using tools for preparing the instrument can break parts. Tighten all parts with your hands. Switch the On/Off master switch to Off. Put the bottle cap on the bottle. Put the tank bottle in the instrument. Attach the joint clip. 40/84 Operation Manual UniversalExtractor E-800...
  • Page 41 Disconnect the indicated condenser connection. Make sure, that there is no coolant in the condenser circuit. Disconnect the other condenser connections. Remove the flange lock. Pull the condenser out of the condenser rack. Disconnect the solvent collector tube. Operation Manual UniversalExtractor E-800 41/84...
  • Page 42 5 | Installation BÜCHI Labortechnik AG Disconnect the solvent collector tube from the installation board. 42/84 Operation Manual UniversalExtractor E-800...
  • Page 43 The function bar shows available functions according to the current operation. The functions on the function bar are executed by tapping the relevant function buttons. Symbol Description Meaning [Back] The display reverts to the previous view. Operation Manual UniversalExtractor E-800 43/84...
  • Page 44 For saving extraction menu methods — Editing and activating — [Configuration] Change settings menu — Service menu — System information — Solvent library [Solvent] menu See Chapter 11.2 “Solvent table”, page 76 — Editing and saving solvents 44/84 Operation Manual UniversalExtractor E-800...
  • Page 45 The setup menu allows saving different methods for different extraction positions. See Chapter 6.5 “Selecting a method for an extraction position”, page 48 6.3.3 Method menu [Method] menu allows saving methods. See Chapter 6.6 “Editing a method”, page 49 Operation Manual UniversalExtractor E-800 45/84...
  • Page 46 [Demo Mode] On/Off Simulate an extraction. Submenu Service WARNING Incorrect use of the actor settings. Incorrect use of the actors settings can cause instrument damages and injuries. Carry out the actor setting as described. 46/84 Operation Manual UniversalExtractor E-800...
  • Page 47 Action Option Explanation View The following information on the Ex- [Extraction unit] traction Unit is available: — Serial number — Firmware version — Operating hours — Board temperature — Code Operation Manual UniversalExtractor E-800 47/84...
  • Page 48 ð The display shows a dialog with an alphanumeric input box. Enter a name for the set-up. [Save] Tap the function on the function bar. ð The name is saved. ð The dialog box closes. 48/84 Operation Manual UniversalExtractor E-800...
  • Page 49 [Solvent] Tap the action ð The display shows a dialog with the selectable solvents. Tap the solvent you wish to use. [OK] Tap the function on the function bar. ð The dialog box closes. Operation Manual UniversalExtractor E-800 49/84...
  • Page 50 Tap the name of the method that you wish to edit. ð The display shows the view Method . [Edit] Tap the function on the function bar. [Inert gas] Tap the action 50/84 Operation Manual UniversalExtractor E-800...
  • Page 51 Enter the value in the numeric input box. [OK] Tap the function on the function bar. ð The dialog box closes. [Save] Tap the function on the function bar. ð The number of extraction cycles is saved. Operation Manual UniversalExtractor E-800 51/84...
  • Page 52 Enter the value in the numeric input box. [OK] Tap the function on the function bar. ð The dialog box closes. [Save] Tap the function on the function bar. ð The drying heating level is saved. 52/84 Operation Manual UniversalExtractor E-800...
  • Page 53 6.6.10 Setting the rinse time of a method (Hot Extraction with beaker, Soxhlet, Soxhlet Warm, Hot Extraction with chamber heater and Twisselmann Extraction) Enter the duration of the rinse step in minutes. — at least 0 minutes — maximum 5940 minutes / 99 hours Operation Manual UniversalExtractor E-800 53/84...
  • Page 54 Change the rinse heating level to compensate ambient conditions. WARNING Setting the heating level too high The consequences are device damage, serious injuries or death. Use the pre-set heating levels. Adjust the heating level to compensate the ambient conditions. 54/84 Operation Manual UniversalExtractor E-800...
  • Page 55 Incorrect drying step settings can damage the analyte and the beaker. Use the analyte protection for the first drying step. Change the default setting to the optimized parameters of your application. See Technical Note: Heating guide for UniversalExtractor E-800 . Obey all safety precautions. See Chapter 2.6 “Residual risks”, page 11 Checkbox...
  • Page 56 The consequences are device damage, serious injuries or death. Use the pre-set heating levels. Adjust the heating level to compensate the ambient conditions. Navigation path ➔ [Method] Navigate to the menu via the navigation path. 56/84 Operation Manual UniversalExtractor E-800...
  • Page 57 Additional solvents can be added by following the instructions in Chapter 2 “Safety”, page 9. The user defined solvents have no predefined heating level. The heating level must be chosen when creating a method. Please refer to BUCHI's application notes. 6.7.1 Creating a new solvent Navigation path ➔...
  • Page 58 [Boiling point] Tap the action [OK] Tap the function on the function bar. ð The control panel shows a dialog box with a numeric input box. Enter the boiling point for the solvent. 58/84 Operation Manual UniversalExtractor E-800...
  • Page 59 The display shows a dialog box with a numeric input box. Enter the mol weight for the solvent. [OK] Tap the function on the function bar. ð The value for the mol weight is saved. ð The dialog box closes. Operation Manual UniversalExtractor E-800 59/84...
  • Page 60 The display shows a dialog box with a numeric input box. Enter the density for the solvent. [OK] Tap the function on the function bar. ð The value for the density is saved. ð The dialog box closes. 60/84 Operation Manual UniversalExtractor E-800...
  • Page 61 Instead of glass sample tube with frit it is possible to insert a thimble. Put the holder for the glass sample tube with frit into the extraction chamber. Put the glass sample tube with frit into the holder in the extraction chamber. Operation Manual UniversalExtractor E-800 61/84...
  • Page 62 Select different methods for each extrac- See Chapter 7.2.2 “Selecting different tion position. methods for each extraction position”, page 63 Select a programmed setup. See Chapter 7.2.3 “Selecting a pro- grammed setup”, page 63 62/84 Operation Manual UniversalExtractor E-800...
  • Page 63 The extraction position will be heated. The extraction position is not activated. The extraction position will not be heated. The extraction for this extraction position is aborted. The extraction position is not heated anymore. Navigation path ➔ Operation Manual UniversalExtractor E-800 63/84...
  • Page 64 Place the beakers on the corresponding positions directly on the heating plate. Close the protection shield. [Home] Navigate to the menu via the navigation path. [Down] Tap the function on the function bar. ð The lift moves down. 64/84 Operation Manual UniversalExtractor E-800...
  • Page 65 A not correctly installed condenser can cause skin burns or a building fire A beaker is placed under the position. An extraction glass chamber is installed at the position. The lift is in the lower position. Operation Manual UniversalExtractor E-800 65/84...
  • Page 66 A not correctly installed condenser can cause skin burns or a building fire A beaker is placed under the position. An extraction glass chamber is installed at the position. The lift is in the lower position. 66/84 Operation Manual UniversalExtractor E-800...
  • Page 67 If necessary remove solvent from the extraction glass chamber. See Chapter 8.3 “Draining solvent from the instrument”, page 71 Switch off the connected recirculating chiller or close the water tap. Empty the solvent tank. See Chapter 8.2 “Removing the tank bottle”, page 70 Operation Manual UniversalExtractor E-800 67/84...
  • Page 68 7 | Performing an extraction BÜCHI Labortechnik AG 7.6 Shutting down the instrument Navigation path ➔ Precondition: The extraction process has ended. Switch the On/Off master switch to Off. 68/84 Operation Manual UniversalExtractor E-800...
  • Page 69 Do not carry out any servicing and cleaning operations that involve opening the housing. Use only genuine BUCHI spare parts in order to ensure correct operation and preserve the warranty. Carry out the service and cleaning operations described in this section to extend the lifetime of the instrument.
  • Page 70 Switch the On/Off master switch to On. Interface Wipe down the display with a damp Monthly cloth. 8.2 Removing the tank bottle Switch the On/Off master switch to Off. Remove the joint clip. Push the solvent tank up. 70/84 Operation Manual UniversalExtractor E-800...
  • Page 71 Close the tank valve. 8.3.3 Switch of the pump Navigation path ➔ ➔ [Service] ➔ [Actors] [Actors] Navigate to via the navigation path. ð The display shows the view Actors . [Pump] Disable the action Operation Manual UniversalExtractor E-800 71/84...
  • Page 72 Add solvent. See Chapter “Adding solvent through the condenser with a funnel”, page 66 Loss of solvent Seals wrong, deformed or Exchange the seals. damaged Incorrect positioning of the Contact BUCHI Customer beaker/ glassware and seals Service. 72/84 Operation Manual UniversalExtractor E-800...
  • Page 73 ð The display shows the view Valves . Select the position of the Soxhlet valve you wish to open. Open the Soxhlet valve. Wait until the extraction glass chamber is empty. Close Soxhlet valve. Operation Manual UniversalExtractor E-800 73/84...
  • Page 74 When disposing, observe the disposal regulations of the materials used. For the used materials see Chapter 3.5 “Technical data”, page 24 or the material labeling on the parts. 10.3 Returning the instrument Before returning the instrument, contact the BÜCHI Labortechnik AG Service Department. https://www.buchi.com/contact 74/84 Operation Manual UniversalExtractor E-800...
  • Page 75 Water out Connection Condenser CW OUT Condenser Condenser Flow meter (inside instrument) Condenser Condenser Connection CW Tank OUT Condenser solvent tank CW IN Condenser Connection solvent tank CW Tank IN CW OUT Fig. 14: Condenser circuit Operation Manual UniversalExtractor E-800 75/84...
  • Page 76 Acetonitril (MeCN) 81.65 29.75 41.05 0.78 Benzene 80.09 30.72 78.11 0.8765 Butanon (Methylethylke- 79.59 31.3 72.11 0.805 ton, AcEt) Chloroform 29.24 119.38 1.48 (Trichloromethane) Cyclohexane 80.73 29.97 84.16 0.78 Dichloromethane (DCM) 40 28.06 84.93 1.33 76/84 Operation Manual UniversalExtractor E-800...
  • Page 77 106.17 0.86 11.3 Spare parts and accessories Use only genuine BUCHI consumables and spare parts in order to ensure correct, safe and reliable operation of the system. NOTE Any modifications of spare parts or assemblies are only allowed with the prior written permission of BUCHI.
  • Page 78 Cooling water valve, 24 VAC 031356 Valve opens cooling water feed during distillation. Turning disk 11067985 Allows for turning the instrument for easier access. 11.3.2 Spare parts Order no. Image Extraction glass chamber universal 11062501 78/84 Operation Manual UniversalExtractor E-800...
  • Page 79 Extraction chamber universal LSV inert 11064850 Set of beakers HE, 2 pcs. 11067475 Set of beakers, 2 pcs. 11067474 Set of beakers LSV, 2 pcs. 11067714 Condenser E-800 cpl. 11067064 Condenser flange E-800 11067818 Condenser tank bottle 11065966 Operation Manual UniversalExtractor E-800 79/84...
  • Page 80 Protection shield bottom, cpl. 11067831 Set of gliding elements including magnets, 10 11067827 pcs. Reflectorfoil analyte protection, 6 pcs. 11068522 Silicone hose D6/9 L=3 m 048355 Set of draining tube, FEP, Universal configu- 11067477 ration, 6 pcs. 80/84 Operation Manual UniversalExtractor E-800...
  • Page 81 Glass sample tubes with frit LSV, long, 6 pcs. 11067816 The glass sample tubes with 150 mm length fit perfectly into the Universal LSV glass extraction chamber. Working volume: 180 mL Filling volume: 216 mL Operation Manual UniversalExtractor E-800 81/84...
  • Page 82 Working volume: 182 mL 11.3.6 Holder for extraction thimbles Order no. Holders for thimbles d25, PTFE, 3 pcs. 11067488 Holders for thimbles d33, PTFE, 3 pcs. 11067490 Holders for thimbles d43, PTFE, 3 pcs. 11067491 82/84 Operation Manual UniversalExtractor E-800...
  • Page 83 11068485 Holders for thimbles d43, stainless steel, 6 pcs. 11068486 Set of holders for glass sample tubes with frit, PTFE, 3 pcs. 11067485 Set of holders for LSV glass sample tubes, PTFE, 3 pcs. 11067486 Operation Manual UniversalExtractor E-800 83/84...
  • Page 84 11593959 | D en We are represented by more than 100 distribution partners worldwide. Find your local representative at: www.buchi.com...