Page 2
CH-9230 Flawil 1 E-Mail: quality@buchi.com BUCHI reserves the right to make changes to the manual as deemed necessary in the light of experience, especially with respect to structure, illustrations and technical details. This manual is copyrighted. Information from it may neither be reproduced, distributed, or used for competitive purposes, nor made available to third parties.
Scope of delivery .......................... 17 Type plate ............................ 18 Technical data ........................... 18 3.7.1 ProxiMate™ ......................... 18 3.7.2 Ambient conditions....................... 19 3.7.3 Materials .......................... 19 Transport and storage........................ 20 Transport ............................ 20 Storage .............................. 20 Lifting the instrument ......................... 20 Operation Manual ProxiMate™...
Page 4
Software settings .......................... 23 5.6.1 Request a license for software or an application .............. 23 5.6.2 Import a license........................ 24 5.6.3 Calibrating a Baseline Correction Vector (BCV) .............. 24 5.6.4 Importing standardized reference data ................ 27 5.6.5 Changing the language of the instrument ................ 28 Operation Manual ProxiMate™...
Page 5
Import reference values via an Excel template .............. 66 6.11 Run AutoCal to create or update calibrations .................. 67 6.11.1 Open the calibration summary to find statistical information.......... 69 6.12 Importing and Exporting........................ 69 6.12.1 Exporting measurement data.................... 69 6.12.2 Importing application data.................... 72 6.12.3 Exporting application data.................... 72 Operation Manual ProxiMate™...
Page 6
Returning the instrument ........................ 94 Appendix ............................ 95 10.1 Measurement results ......................... 95 10.2 File explanations and folder locations.................... 95 10.3 Rules entering a formula........................ 96 10.4 Spare parts and accessories ...................... 97 10.4.1 Accessories.......................... 97 10.4.2 Spare parts .......................... 99 Operation Manual ProxiMate™...
Indicates a danger that could result in damage to property. 1.2 Symbols The following symbols are displayed in this operation manual or on the device: 1.2.1 Warning symbols Symbol Meaning General warning Breakable items Hot surface Dangerous electrical voltage Instrument damage Operation Manual ProxiMate™ 7/100...
Signal Signals are marked-up like this. 1.3 Trademarks Product names and registered or unregistered trademarks that are used in this document are used only for identification and remain the property of the owner in each case. 8/100 Operation Manual ProxiMate™...
Safety-related incidents that occur while using the instrument should be reported to the manufacturer (quality@buchi.com). BUCHI service technicians Service technicians authorized by BUCHI have attended special training courses and are authorized by BÜCHI Labortechnik AG to carry out special servicing and repair measures.
Unauthorized modifications can affect safety and lead to accidents. Use only genuine BUCHI accessories, spare parts and consumables. Carry out technical changes only with prior written approval from BUCHI. Only allow changes to be made by BUCHI service technicians. 10/100...
Page 11
Büchi Labortechnik AG Safety | 2 BUCHI accepts no liability for damage, faults and malfunctions resulting from unauthorized modifications. Operation Manual ProxiMate™ 11/100...
3.2 Sample presentation options The choice of sample presentation of ProxiMate™ is optimised for the type of sample under analysis and for the working environment where the instrument is used. ProxiMate™ can be configured with a choice of sample presentation options: up view and down view configurations.
As plastics have their own NIR spectra, changes in type of dish can influence the measurement output leading to perceived measurement shifts. Use of the down view mode prevents this from occurring. Additionally ProxiMate™ down view also allows the use of large volume sample dishes. These are particularly useful with samples that are inhomogeneous, as the measurement is averaged over a much larger sample area.
The On/Off master switch does not interrupt the electric power supply. See Chapter 5.4 "Establishing electrical connections", page 22 Status On/Off master switch Status Description No light The instrument is not switched on. Steady light The instrument is on Flashing light The instrument shuts down 14/100 Operation Manual ProxiMate™...
USB socket USB socket Cable gland for network connection Advanced IP module The instrument connections are lo- cated behind the Advanced IP mod- ule. See Chapter 3.4.3 "Connections (IP module removed)", page 16 Cable gland for mains lead Cooler Operation Manual ProxiMate™ 15/100...
Büchi Labortechnik AG 3 | Product description 3.4.3 Connections (IP module removed) Fig. 3: Connections on the rear side Not available Network Audio Disabled USB ports Display port Do not use 16/100 Operation Manual ProxiMate™...
Fig. 4: Location of the type plate Type plate 3.5 Scope of delivery NOTE The scope of delivery depends of the configuration of the purchase order. Accessories are delivered as per the purchase order, order confirmation, and delivery note. Operation Manual ProxiMate™ 17/100...
The instrument should be transported by two persons at the same time. Lift the instrument at the points indicated. Fig. 6: Lifting the instrument Lift the instrument – this requires two persons lifting at the points indicated on the bottom of the instrument. 20/100 Operation Manual ProxiMate™...
Make sure that the power supply can be disconnected at any time in an emergency. 5.3 Securing against earthquakes Fig. 7: Securing against earthquakes Cooler Cord Loop a cord around the cooler and attach it to a fixed point. Operation Manual ProxiMate™ 21/100...
5.5 Installing a USB device NOTE Make sure that the USB socket is covered either with the cover lid or the protection cover. Open one of the cover lids for the USB socket. Plug USB device in the USB socket. 22/100 Operation Manual ProxiMate™...
The instrument is in administrator mode. [License Request] Tap the button. ð The display shows a dialog box with the license request menu. [Edit] Tap the button. ð The display shows a dialog with an alphanumeric input box. Operation Manual ProxiMate™ 23/100...
Confirm with Open the location and save the license request file to a USB stick or something similar. Send the license request file and a short explanation to registration@buchi.com. ð You will receive a license file in return. 5.6.2 Import a license Navigation path ➔...
Page 25
The display shows the Sample Presentation menu. [Default] Select [OK] Confirm with Fig. 8: Positioning plate with two openings for up and down view Measurement of the external white reference in up view mode Fig. 9: Thin spacer ring for up view Operation Manual ProxiMate™ 25/100...
Page 26
In case of a dual view instrument, repeat the calibration for the up view mode. Define calibration settings for liquid samples [Measurement View] Tap on ð The display shows the Measurement View menu. [Up] Select for calibration for liquid measurements. [OK] Confirm with 26/100 Operation Manual ProxiMate™...
Restart the NIRWise software after successful BCV calibration. 5.6.4 Importing standardized reference data NOTE The location of the destination folder is fixed. See Chapter 10.2 "File explanations and folder locations", page 95 Navigation path ➔ ➔ [Import External Refer- ence Data] Operation Manual ProxiMate™ 27/100...
The control panel shows a dialog box with selectable languages. Select a language. [OK] Tap the button ð The dialog box closes. ð The control panel shows a dialog box. [OK] Tap the button to confirm the dialog box. Restart the software. 28/100 Operation Manual ProxiMate™...
The function bar shows available functions according to the current operation. The functions on the function bar are executed by tapping the relevant function buttons. Symbol Description Meaning [Back] The display reverts to the previous view. Operation Manual ProxiMate™ 29/100...
Page 30
Shows information about the instru- [Information] ment and the installed Licenses. [Full page ] The report fits on full page. The report fits to width scrolling. [Width scrolling] [Go to windows] The instrument changes to the win- dows® surface. 30/100 Operation Manual ProxiMate™...
The tested sample is in the specifications. By tapping the symbol the instrument carries out a measurement. Target value is the expected parameter for the product. The target value is defined in the Application. 32/100 Operation Manual ProxiMate™...
Page 33
A barcode reader can be connected to the instrument. When the barcode reader is configured the user can use this label to identify the sample under analysis. As an alternative insert a barcode manually Navigation path ➔ Operation Manual ProxiMate™ 33/100...
Page 34
Tap the button next to the ð The display shows a dialog with an alphanumeric input box. Enter an order number or code. [OK] Tap the button ð The order is saved. ð The dialog box closes. 34/100 Operation Manual ProxiMate™...
Filters allow the user to narrow the selection of sample to those that fulfill specific criteria. Navigation path ➔ ➔ [History] [History] Navigate to the menu via the navigation path. Tap button filter. ð The display shows a dialog box with the selectable filters. Operation Manual ProxiMate™ 35/100...
Page 36
The display shows the filtered measurements. Deselect filter Navigation path ➔ ➔ [History] [History] Navigate to the menu via the navigation path. Tap the button filter. ð The display shows a dialog box with the selectable filters. 36/100 Operation Manual ProxiMate™...
Page 37
Application Time and date Order Sample ID Include in calibration dataset (Auto- Cal) Tap the button of the selected filter. [OK] Tap the button ð The dialog box closes. ð The display shows all available measurements. Operation Manual ProxiMate™ 37/100...
[Remote host] Open program TeamViewer The Software opens for remote support. (administrator only) [Restore Backup] Contact BUCHI Customer Service. [Cleaning Mode] Procedure See Chapter 7.7 "Cleaning the dis- play", page 91 (all users) [Operational View / Procedure The data is displayed depends on the...
The display shows a dialog with an alphanumeric input box. Enter the password. [OK] Tap the button ð The dialog box closes. ð The instrument is in administrator mode. ð The status bar shows the icon administrator. Operation Manual ProxiMate™ 41/100...
Tap the application you wish to copy. ð The display highlights the application in green. [Copy] Tap the function on the function bar. ð The display shows a dialog with an alphanumeric input box. Enter a name for the application. 42/100 Operation Manual ProxiMate™...
Down The application uses the down view lamp. Radiation is directed onto and collected from the upper surface of the sample. The radiation does not interact with the sample cup. Proceedings: Navigation path ➔ Operation Manual ProxiMate™ 43/100...
The display highlights the application in green. [Measurement mode] Tap the action ð The display shows a dialog box with the selectable values. Select a value. [OK] Tap the button ð The dialog box closes. ð The setting is saved. 44/100 Operation Manual ProxiMate™...
Tap the name of the application that you wish to edit. ð The display highlights the application in green. [Description] Tap the action ð The display shows a dialog with an alphanumeric input box. Enter a description for the application. Operation Manual ProxiMate™ 45/100...
Tap the name of the application that you wish to edit. ð The display highlights the application in green. [Measurement duration] Tap the action ð The display shows a dialog box with a numeric input box. 46/100 Operation Manual ProxiMate™...
The instrument is in administrator mode. See Chapter 6.5 "Log in administrator mode", page 41 [Application] Navigate to the menu via the navigation path. [Edit] Tap the function on the function bar. ð [Edit] The display highlights the function in green. Operation Manual ProxiMate™ 47/100...
Tap the name of the application you wish to remove. ð The display highlights the application in green. [Remove] Tap the function on the function bar. Confirm the secure question. ð The display shows a dialog with the two deleting modes. Select the deleting mode. 48/100 Operation Manual ProxiMate™...
The display highlights the application in green. Tap the name of the property that you wish to edit. ð The display shows the view Property . [Name] Tap the action ð The display shows a dialog with an alphanumeric input box. Operation Manual ProxiMate™ 49/100...
Tap the name of the property that you wish to edit. ð The display shows the view Property . [Sort order] Tap the action ð The display shows a dialog box with a numeric input box. 50/100 Operation Manual ProxiMate™...
Tolerance Max. see Chap- ter 6.8.23 "Changing the Toler- ance maximum of a property", page 64 Limit Min. see Chapter 6.8.22 "Changing the Limit minimum of a property", page 63 Limit Max. seeChapter 6.8.21 "Changing the Limit maximum of a property", page 63 Operation Manual ProxiMate™ 51/100...
Page 52
Tolerance Max. see Chap- ter 6.8.23 "Changing the Toler- ance maximum of a property", page 64 Limit Min. seeChapter 6.8.22 "Changing the Limit minimum of a property", page 63 Limit Max. see Chapter 6.8.21 "Changing the Limit maximum of a property", page 63 52/100 Operation Manual ProxiMate™...
Page 53
The instrument is in administrator mode. See Chapter 6.5 "Log in administrator mode", page 41 [Application] Navigate to the menu via the navigation path. [Edit] Tap the function on the function bar. ð [Edit] The display highlights the function in green. Operation Manual ProxiMate™ 53/100...
The display shows a dialog box with the selectable values. Select a value. [OK] Tap the button ð The dialog box closes. ð The setting is saved. ð The value for the Initial Wavelength Range is saved. 54/100 Operation Manual ProxiMate™...
6.8.8 Changing the Calibration Base (Calibration model only) The following settings are available: Type Explanation The property value is expressed neglecting the presence of [Dry Basis] water in the sample. The water contribution is subtracted from the calculation. Operation Manual ProxiMate™ 55/100...
The amount of water is expressed as a percentage of the total weight. The property value is expressed including the presence of [As Is] water in the sample. The water contribution is included in the calculation. Proceedings: 56/100 Operation Manual ProxiMate™...
The display shows the view Property . [Formula] Tap the action ð The display shows a dialog with an alphanumeric input box. Enter the formula. [OK] Tap the button ð The dialog box closes. ð The formula is saved. Operation Manual ProxiMate™ 57/100...
Tap the name of the property that you wish to edit. ð The display shows the view Property . [Illuminant] Tap the action ð The display shows a dialog box with a numeric input box. Enter the value in the numeric input box. 58/100 Operation Manual ProxiMate™...
[Edit] Tap the function on the function bar. ð [Edit] The display highlights the function in green. Tap the name of the application that you wish to edit. ð The display highlights the application in green. Operation Manual ProxiMate™ 59/100...
ð The alphanumeric input box shows the available special characters. Navigation path ➔ Precondition: The instrument is in administrator mode. See Chapter 6.5 "Log in administrator mode", page 41 [Application] Navigate to the menu via the navigation path. 60/100 Operation Manual ProxiMate™...
The value for the Bias is saved. 6.8.18 Changing the Slope of a property The slope is a factor that is used to correct proportional systematic differences between the result of a measurement and the reference value. Proceedings: Navigation path ➔ Operation Manual ProxiMate™ 61/100...
Tap the button ð The dialog box closes. ð The value for the Mahalanobis is saved. 6.8.20 Changing the Target of a property Sets the target value, relative to which the tolerances are considered. Proceedings: Navigation path ➔ 62/100 Operation Manual ProxiMate™...
[OK] Tap the button ð The dialog box closes. ð The value for the Limit is saved. 6.8.22 Changing the Limit minimum of a property Sets the lower limit for the property. Proceedings: Navigation path ➔ Operation Manual ProxiMate™ 63/100...
ð The value for the Tolerance is saved. 6.8.24 Changing the Tolerance minimum of a property Tolerance is a difference from the target value. Sets the lower tolerance relative to the target. Proceedings: Navigation path ➔ 64/100 Operation Manual ProxiMate™...
ð The property is deleted. 6.10 Enter reference values Navigation path ➔ ➔ [History] Function bar symbols used in this section: [Edit] Allows the selected item to be edited. Operation Manual ProxiMate™ 65/100...
Dataset] Precondition: The instrument is in administrator mode. Samples have been measured with ProxiMate™ and are properly and uniquely labeled. The reference values of the samples have been determined by a primary method. [History] Navigate to the menu via the navigation path.
Open the template with Excel, enter the reference values. Safe the template with the reference values. Copy the template to a USB or to the ProxiMate. Navigate to the History menu via the navigation path. [Import] Tap the function on the function bar.
Page 68
Values of statistic parameters of IDs of last n (default = five) mea- new calibration surements Parameter values according to ac- Parameter values as predicted by tual calibration new calibration [Accept] [Reject] Button Button 68/100 Operation Manual ProxiMate™...
At least one measurement is available in the History menu. Navigate to the History menu via the navigation path. Navigate to the measurement you wish to export and tap it. ð The display highlights the measurement in green. Operation Manual ProxiMate™ 69/100...
Page 70
Tap on all other samples that you wish to export. ð A ll selected samples are highlighted in green. [Export] Tap the function on the function bar. ð The display shows the Export menu. Select the file format which you wish to export. 70/100 Operation Manual ProxiMate™...
Page 71
[Go to windows] The instrument changes to the windows® surface. Navigate to the Tools menu via the navigation path. [Go To Windows] Tap the button. ð The display switches to the desktop of the in-built computer. Operation Manual ProxiMate™ 71/100...
The display shows a dialog with the properties of the application you wish to export. All properties are highlighted in green. Tap the properties you do not want to export. ð The disabled properties are highlighted in white. 72/100 Operation Manual ProxiMate™...
To export the report as excel file, tap the button. ð The display shows a dialog box confirming the successful export. 6.13.2 Create a report of multiple samples of the same application Navigation path ➔ ➔ [History] Operation Manual ProxiMate™ 73/100...
➔ ➔ [History] Function bar symbols used in this section: Generates on-screen report [Report] Activates multiple selection [Multiple selection] of measurements. [Select all] Selects all measurements in the list. NOTICE! only available if multiple selection is activated 74/100 Operation Manual ProxiMate™...
The display switches to the desktop of the in-built computer. Open the Data folder on the desktop. Navigate to the subfolders Exports and then Data . Find the exported file labelled with the application name and the date and time stamp of the export. Operation Manual ProxiMate™ 75/100...
➔ Precondition: The instrument is prepared. See Chapter 6.14.1 "Preparing the instrument", page 76 [Application] Navigate to the menu via the navigation path. Tap the application you wish to use. ð The display highlights the application in green. 76/100 Operation Manual ProxiMate™...
6.14.4 Shutting down the instrument Navigation path ➔ [Start] Navigate to the menu via the navigation path. [Switch off] Tap the function on the function bar. Answer to the confirmation question. ð The instrument is shutting down. Operation Manual ProxiMate™ 77/100...
Do not carry out any servicing and cleaning operations that involve opening the housing. Use only genuine BUCHI spare parts in order to ensure correct operation and preserve the warranty. Carry out the service and cleaning operations described in this section to extend the lifetime of the instrument.
Touch the lamp on the indicated areas. 7.2.1 Changing the down view lamp Disconnect the power supply to the instrument. Wait 15 min. for lamp to cool. Open the cover lid on the top of the instrument. Operation Manual ProxiMate™ 79/100...
Page 80
Büchi Labortechnik AG 7 | Cleaning and servicing Remove the seal and the cover lid. Press the ferrule. Turn the ferrule 1/4 turn counterclockwise. Remove the defective lamp from the lamp socket. Disconnect the defective lamp. 80/100 Operation Manual ProxiMate™...
Page 81
Put the connected new lamp in the lamp socket. Make sure that the screw indicated is in the groove of the lamp socket. Put ferrule and spring on the lamp socket. Press the ferrule. Turn the ferrule 1/4 turn clockwise. Operation Manual ProxiMate™ 81/100...
Replacement", page 86 Carry out a baseline correction vector calibration. See Calibrating a Baseline Correction Vector (BCV) 7.2.2 Changing the up view lamp Disconnect the power supply to the instrument. Wait 15 min. for lamp to cool. 82/100 Operation Manual ProxiMate™...
Page 83
Make sure that the instrument cannot tip over during the lamp replacement procedure. Open the cover lid on the bottom of the instrument. Remove the seal and the cover lid. Press the ferrule. Turn the ferrule 1/4 turn counterclockwise. Operation Manual ProxiMate™ 83/100...
Page 84
Remove the defective lamp from the lamp socket. Disconnect the defective lamp. Connect the new lamp. Put the connected replacement lamp in the lamp socket. Make sure that the indicated screw is in the groove of the lamp socket. 84/100 Operation Manual ProxiMate™...
Page 85
Cleaning and servicing | 7 Put ferrule and spring on the lamp socket. Press the ferrule. Turn the ferrule 1/4 turn clockwise. Put the seal and the cover lid on the instrument. Attach the cover lid with the tool provided. Operation Manual ProxiMate™ 85/100...
Select which lamp was replaced (up view lamp or down view lamp). Confirm the secure question with 7.3 Checking the desiccant cartridge Color Describtion Pink used cartridge (replacement required) Blue unused cartridge Open the cover lid for the desiccant cartridge. 86/100 Operation Manual ProxiMate™...
Page 87
Remove the cover lid and the seal. Check the color of the window of the desiccant cartridge. If necessary change the desiccant cartridge. See Chapter 7.4 "Changing the desiccant cartridge", page 88 Put seal and cover lid on the instrument. Operation Manual ProxiMate™ 87/100...
Büchi Labortechnik AG 7 | Cleaning and servicing Color Describtion Attach the cover lid. 7.4 Changing the desiccant cartridge Open the cover lid for the desiccant cartridge. Remove the cover lid and the seal. 88/100 Operation Manual ProxiMate™...
Page 89
Büchi Labortechnik AG Cleaning and servicing | 7 Remove the used desiccant cartridge. Put a new desiccant cartridge in the instrument. Put seal and cover lid on the instrument. Attach the cover lid. Operation Manual ProxiMate™ 89/100...
[Extended System Test] Navigate to the action via the navigation path. ð The display shows the dialog Extended System Test . [Advanced System Test] Select check box [Start] Tap the button ð The instrument starts the test. 90/100 Operation Manual ProxiMate™...
The display shows a dialog box with a numeric input box. Wipe down the display with a damp cloth. Enter the displayed secure code. [OK] Tap the button ð The dialog box closes. ð The touch function of the display is unlocked. Operation Manual ProxiMate™ 91/100...
The internal reference '{0}' Service. might not be moving properly. 1007 The current system tempera- Move the Instrument to a location where the ambient ture ({0} °C) is outside the ex- temperature meets pected range ({1}..{2} °C). specification. 92/100 Operation Manual ProxiMate™...
Page 93
Reattempt data backup. backup. Error: '{0}'. Contact BUCHI Customer Service. 2502 A critical error occured during Restart the instrument. Reattempt test. test run. Test run has been Contact BUCHI Customer canceled. For more details Service. see log file. Operation Manual ProxiMate™ 93/100...
When disposing, observe the disposal regulations of the materials used. Materials used see Chapter 3.7 "Technical data", page 18. 9.3 Returning the instrument Before returning the instrument, contact the BÜCHI Labortechnik AG Service Department. https://www.buchi.com/contact 94/100 Operation Manual ProxiMate™...
Cosine of x Cos(x) Absolute value of a double-precision float- Abs(x) ing-point number x Rounds double-precision floating-point Round(x) value x to the nearest integer value Rounds double-precision floating-point Round(x,decimal) value x to a specified number of decimal places 96/100 Operation Manual ProxiMate™...
Büchi Labortechnik AG Appendix | 10 10.4 Spare parts and accessories Use only genuine BUCHI consumables and spare parts in order to ensure correct, safe and reliable operation of the system. NOTE Any modifications of spare parts or assemblies are only allowed with the prior written permission of BUCHI.
Page 98
11055998 Protection cover USB-WiFi stick 11066582 Light shield (down view) 11067281 Performance test standards kit (7 pcs.) 11067545 Recertification of performance test standards kit 11070905 NIRWise PLUS Chemometrics suite 11068025 Set Network cable RJ45 5m 11068780 98/100 Operation Manual ProxiMate™...
Büchi Labortechnik AG Appendix | 10 10.4.2 Spare parts Order no. Image Spare lamp 11065441 Desiccant cartridge 11065467 Shelf life in original packaging is 12 months Replacement Window HPSC 046246 Operation Manual ProxiMate™ 99/100...
Page 100
We are represented by more than 100 distribution partners worldwide. Find your local representative at: www.buchi.com...
Need help?
Do you have a question about the ProxiMate and is the answer not in the manual?
Questions and answers