Buchi UniversalExtractor E-800 Operation Manual
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Buchi UniversalExtractor E-800 Operation Manual

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Operation Manual

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Summary of Contents for Buchi UniversalExtractor E-800

  • Page 1 UniversalExtractor E-800 Operation Manual...
  • Page 2 CH-9230 Flawil 1 E-Mail: quality@buchi.com BUCHI reserves the right to make changes to the manual as deemed necessary in the light of experience, especially with respect to structure, illustrations and technical details. This manual is copyrighted. Information from it may neither be reproduced, distributed, or used for competitive purposes, nor made available to third parties.

  • Page 3: Table Of Contents

    2.6.6 Overfilled extraction beakers .................. 13 2.6.7 Spilled hazardous materials.................. 13 2.6.8 Solvent leakages during extraction process ............. 14 2.6.9 Incorrect function of the Analyte Protection Sensors.......... 14 2.6.10 Traces of dark extracts or residuals of extract foam.......... 14 Personal protective equipment .................... 14 Modifications........................ 14 Operation Manual UniversalExtractor E-800...
  • Page 4 3.2.5 Lower connections on the rear side................ 23 3.2.6 Installation board ...................... 24 Type plate.......................... 24 Scope of delivery ......................... 25 Technical data ........................ 25 3.5.1 UniversalExtractor E-800.................. 25 3.5.2 Ambient conditions .................... 26 3.5.3 Materials ........................ 27 Transport and storage ...................... 28 Transport .......................... 28 Storage .......................... 28 Lifting the instrument ...................... 28 Operation Manual UniversalExtractor E-800...
  • Page 5 Preparing the condenser ..................... 40 5.15 Preparing the tank bottle ..................... 42 5.16 Selecting a configuration ..................... 43 5.17 Disassembling the condenser circuit ...................  43 5.18 Mobile connection........................ 44 5.18.1 Requirements for local network settings.............. 44 5.18.2 Preparing the instrument for app using.............. 45 Operation Manual UniversalExtractor E-800...
  • Page 6 6.7.4 Changing the heating level of a solvent.............. 61 6.7.5 Changing the boiling point of a solvent.............. 62 6.7.6 Changing the enthalpy of a solvent ................ 62 6.7.7 Changing the molecular weight of a solvent ............. 63 6.7.8 Changing the density of a solvent................ 63 Operation Manual UniversalExtractor E-800...
  • Page 7 11.3 Spare parts and accessories .................... 81 11.3.1 Accessories ...................... 81 11.3.2 Spare parts ....................... 82 11.3.3 Conversion kits ...................... 84 11.3.4 Recirculating chiller.................... 84 11.3.5 Consumables...................... 85 11.3.6 Glass sample tubes and extraction thimbles ............ 85 11.3.7 Holder for extraction thimbles ................... 86 Operation Manual UniversalExtractor E-800...

  • Page 8: About This Document

    Indicates a danger that could result in damage to property. Symbols The following symbols are displayed in this operation manual or on the device: 1.2.1 Warning symbols Symbol Meaning General warning Hot surface Breakable items Hand injuries Flammable substances 8/88 Operation Manual UniversalExtractor E-800...

  • Page 9: Mark-Ups And Symbols

    Signal Signals are marked-up like this. Trademarks Product names and registered or unregistered trademarks that are used in this document are used only for identification and remain the property of the owner in each case. Operation Manual UniversalExtractor E-800 9/88...

  • Page 10: Safety

    The UniversalExtractor E-800 is designed for the extraction (solid-liquid extraction) of samples with known solvents or solvent mixtures and the reduction or drying of the extract. The UniversalExtractor E-800 can be used in laboratories for the following tasks: — Economic Continuous Extraction (without chamber heater) —...

  • Page 11: Location Of Warning Signs On The Product

    — Safety-related incidents that occur while using the device should be reported to the manufacturer (quality@buchi.com). BUCHI service technicians Service technicians authorized by BUCHI have attended special training courses and are authorized by BÜCHI Labortechnik AG to carry out special servicing and repair measures.

  • Page 12: Protection Devices

    Use optimized extraction parameters, drying parameters and solvent amounts (e.g. from BUCHIs technical and application notes). 2.6.3 Mechanical damages If a device is damaged, sharp edges, moving parts or exposed electrical wires can cause injuries. Check device regularly for visible damage. 12/88 Operation Manual UniversalExtractor E-800...

  • Page 13: Glass Breakage

    Make sure that the personal protective equipment meets the requirements of the safety data sheets for the chemicals used. Make sure that the decontamination agent meets the requirements of the safety data sheets for the chemicals used. Operation Manual UniversalExtractor E-800 13/88...

  • Page 14: Solvent Leakages During Extraction Process

    Technical modifications to the device or accessories should only be carried out with the prior written approval of BÜCHI Labortechnik AG and only by authorized BUCHI technicians. BUCHI accepts no liability whatsoever for damage arising as a result of unauthorized modifications. 14/88...

  • Page 15: Product Description

    Büchi Labortechnik AG Product description | 3 Product description Description of function The UniversalExtractor E-800 is designed to carry out the following solid-liquid extraction methods: — Economic Continuous Extraction (without chamber heater). See Chapter 3.1.1 "Economic Continuous Extraction (with extraction glass chamber Economic Continues Extraction)", page 15...

  • Page 16: Soxhlet Extraction (With Extraction Glass Chamber Universal)

    — The magnetic valve is open, the solvent extracts the analyte and flows back into the beaker. Step 2 drying — The solvent is heated, vapor rises up to the condenser, condenses and flows into the tank bottle. — The analyte remains in the beaker. 16/88 Operation Manual UniversalExtractor E-800...

  • Page 17: Hot Extraction (With Extraction Glass Chamber Universal)

    — The magnetic valve is open, the solvent flows back into beaker, the solvent is not collected. Step 3 drying — The solvent is heated, vapor rises up to the condenser, condenses and flows into tank. — The analyte remains in the beaker. Operation Manual UniversalExtractor E-800 17/88...

  • Page 18: Soxhlet Warm Extraction (With Extraction Glass Chamber Universal)

    — The solvent is heated, vapor rises up around the sample to the condenser, condenses and flows into the tank bottle. — The analyte remains in the beaker. 3.1.7 Description of the analyte protection The Analyte Protection protects the analyte from overheating. 18/88 Operation Manual UniversalExtractor E-800...
  • Page 19 Extraction Extraction Presence of beaker Presence of solvent (Level check) Extraction step X X¹ X¹ X¹ X¹ X¹ Rinse step X¹ X¹ X¹ X¹ Dry step X¹ X¹ X¹ X¹ X¹ ¹ activation inert gas Operation Manual UniversalExtractor E-800 19/88...

  • Page 20: Configuration

    Protection shield Condenser rack Chamber rack Condenser tank bottle Installation board Tank bottle Heating plate Analyte protection sensor Beaker rack 10 Chamber heater 11 Inert gas connection 12 On/Off master switch (option) 13 Pro Interface 20/88 Operation Manual UniversalExtractor E-800...

  • Page 21: Front View (Without Chamber Heater)

    Front View (without chamber heater) Fig. 3: Front view Protection shield Condenser rack Chamber rack Condenser tank bottle Tank bottle Beaker rack Installation board Analyte protection sensor Heating plate 10 On/Off master switch 11 Pro Interface Operation Manual UniversalExtractor E-800 21/88...

  • Page 22: Rear View

    3.2.4 Upper connections on the rear side Fig. 5: Connections on the top Standard BUCHI communication port Standard BUCHI communication port (COM) (COM) LAN port Port for the cooling water valve 22/88 Operation Manual UniversalExtractor E-800...

  • Page 23: Lower Connections On The Rear Side

    Inert gas connection (option) (marked INERT) Coolant water out Exhaust (marked OUT) (marked EXHAUST) Coolant water in 10 Type plate (marked IN) 11 Coolant water solvent tank out 12 Solvent out (marked OUT) (marked TANK OUT (SOLVENT)) Operation Manual UniversalExtractor E-800 23/88...

  • Page 24: Installation Board

    Beaker rack Universal 10 Solvent collector tube 11 Sensor plugs 12 Attachment clip for tube 13 Lift Type plate The type plate identifies the instrument. The type plate is located at the rear of the instrument. 24/88 Operation Manual UniversalExtractor E-800...

  • Page 25: Scope Of Delivery

    Pollution degree Dimensions (W x D x H) 638 x 595 x 613 mm (without glassware) Dimensions (W x D x H) 638 x 595 x 752 mm (with glassware Universal) Weight 44.8 kg (without glassware) Operation Manual UniversalExtractor E-800 25/88...

  • Page 26: Universalextractor E-800

    Max. altitude above sea level 2000 m Ambient temperature 5‒40 °C Maximum relative humidity 80% for temperatures up to 31 °C decreasing linearly to 50 % relative hu- midity at 40 °C Storage temperature max. 45 °C 26/88 Operation Manual UniversalExtractor E-800...

  • Page 27: Materials

    Steel 1.4301/304 with powder coating Exhaust Aluminium coated Protection shield PMMA GS Glass ware Borosilikat 3.3 Sealings glassware PTFE (with FKM core) Tank bottle Borosilikat 3.3 Tank bottle valve PTFE / FFKM Sealing solvent connection PTFE Tubing Operation Manual UniversalExtractor E-800 27/88...

  • Page 28: Transport And Storage

    The instrument should be transported by two persons at the same time. Lift the instrument at the points indicated. NOTICE Dragging the instrument can damage the feet of the instrument. Lift the instrument when positioning or re-locating. 28/88 Operation Manual UniversalExtractor E-800...
  • Page 29 Büchi Labortechnik AG Transport and storage | 4 Fig. 9: Lifting the instrument Lift the instrument – this requires two persons each lifting at the points indicated on the left and right side of the instrument. Operation Manual UniversalExtractor E-800 29/88...

  • Page 30: Installation

    1. Provide the mains voltage and frequency specified on the type plate of the instrument. 2. Be designed for the load imposed by the instruments connected. 3. Be equipped with suitable fuses and electrical safety features. 4. Be equipped with a proper grounding. 30/88 Operation Manual UniversalExtractor E-800...

  • Page 31: Securing Against Earthquakes

    Risk of property damage and diminished performance due to use of unsuitable power cables. The power supply cables supplied with the product by BUCHI precisely match the requirements of the device. If other power cables that do not meet those requirements are used, the device may be damaged and/or its performance diminished.

  • Page 32: Connecting The Solvent Tubes To The Condenser Tank Bottle

    Attach a solvent connection nut with seals to the connection marked IN (SOLVENT) . Attach the inlet tube onto the connection marked OUT . Attach the drain tube onto the connection marked IN (SOLVENT) . 32/88 Operation Manual UniversalExtractor E-800...

  • Page 33: Connecting The Coolant Tubes To The Condenser Tank Bottle

    Connecting inert gas (option) 5.8.1 Connecting inert gas to the instrument (option) Precondition: R Make sure that the instrument is not connected to the power supply. Attach the inert gas tube onto the connection marked INERT. Operation Manual UniversalExtractor E-800 33/88...

  • Page 34: Connecting Inert Gas To The Extraction Glas Chamber (Option)

    Connect the inert gas tube. Preparing the extraction glass chamber Economic Continuous Extraction NOTICE! Make sure that the small gap of the sealing shows in the direction of the extraction glass chamber. Attach the sealing to the extraction glass chamber. 34/88 Operation Manual UniversalExtractor E-800...

  • Page 35: Installing The Extraction Glass Chamber Economic Continuous Extraction

    Push the chamber rack in the instrument. 5.11 Preparing the extraction glass chamber universal NOTICE Risk of broken parts by using tools Using tools for preparing the instrument can break parts. Tighten all parts with your hands. Operation Manual UniversalExtractor E-800 35/88...

  • Page 36: Installing The Extraction Glass Chamber Universal

    The extraction glass chamber universal is pre- pared. 5.12 Installing the extraction glass chamber universal NOTICE An incorrect assembled extraction glass chamber can cause glass breakage. Install the extraction glass chamber according to following instructions. 36/88 Operation Manual UniversalExtractor E-800...
  • Page 37 Pull the chamber rack. Precondition: R Start with the extraction glass chamber on the left side. R Make sure that the BUCHI Logo points to the front. Put the extraction glass chamber in the chamber rack. Turn the extraction glass chamber 45°...

  • Page 38: Installing The Protection Shields

    Push the chamber rack in the instrument. 5.13 Installing the protection shields 5.13.1 Installing two protection shields (extraction glass chamber universal only) Make sure, that both protections shields fit together. 38/88 Operation Manual UniversalExtractor E-800...

  • Page 39: Installing One Protection Shield (Extraction Glass Chamber Ece Only)

    Put the front protection shield on both sides into the front slot at the same time. 5.13.2 Installing one protection shield (extraction glass chamber ECE only) Hold the protection shield on both sides at the point indicated. Operation Manual UniversalExtractor E-800 39/88...

  • Page 40: Preparing The Condenser

    NOTICE! Make sure that the small gap of the sealing show in the direction of the condenser. Put the sealing on the bottom of the condenser. Attach the solvent connection nut with the seal to the condenser. 40/88 Operation Manual UniversalExtractor E-800...
  • Page 41 NOTICE! Do not use force to carry out this action step. Put the condenser in the condenser rack. Secure the condenser with the flange lock. Turn the condenser. Connect the solvent collector tube to the installation board Operation Manual UniversalExtractor E-800 41/88...

  • Page 42: Preparing The Tank Bottle

    5.15 Preparing the tank bottle NOTICE Risk of broken parts by using tools Using tools for preparing the instrument can break parts. Tighten all parts with your hands. Switch the On/Off master switch to Off. 42/88 Operation Manual UniversalExtractor E-800...

  • Page 43: Selecting A Configuration

    ð The display shows a dialog with the selectable configurations. Tap the configuration according to the installed glass setup. ð The configuration is selected. ð The dialog box closes. 5.17 Disassembling the condenser circuit Disconnect the indicated condenser connection. Operation Manual UniversalExtractor E-800 43/88...

  • Page 44: Mobile Connection

    Disconnect the solvent collector tube from the installation board. 5.18 Mobile connection 5.18.1 Requirements for local network settings The following port has to be enabled in the firewall settings on the internet gateway: — TCP (HTTPS) traffics through remote port 443 44/88 Operation Manual UniversalExtractor E-800...

  • Page 45: 5.18.2 Preparing The Instrument For App Using

    Büchi Labortechnik AG Installation | 5 In order to use the BUCHI Cloud a DNS server must be configured on the instrument. NOTE If there is no DNS server available enter the IP address for the BUCHI Cloud connection manually.

  • Page 46: Operating The Interface Pro

    Function bar The function bar shows available functions according to the current operation. The functions on the function bar are executed by tapping the relevant function buttons. 46/88 Operation Manual UniversalExtractor E-800...

  • Page 47: Menu Bar

    — For saving the individual [Setup] menu settings for the extraction positions — For saving extraction [Method] menu methods — Editing and activating — Change settings [Configuration] menu — Service menu — System information Operation Manual UniversalExtractor E-800 47/88...
  • Page 48 On the home menu the following control buttons are available: Button Meaning Skips the actual step at the selected position. Skips the actual step for all positions. Aborts extraction on the selected extraction position. Editing the running method. 48/88 Operation Manual UniversalExtractor E-800...

  • Page 49: Setup Menu

    [Network] Enter value The following parameters can be edited: Device name/DHCP/MAC address/ System IP address/Subnet mask/ Gateway [Delete app connec- Confirmation question Resets external connections to the tion] instrument. [Demo Mode] On/Off Simulate an extraction. Operation Manual UniversalExtractor E-800 49/88...
  • Page 50 Tap up or down. ð Display shows the actual current consumption. — Beeper On/Off — Chiller On/Off (option) Submenu System Information The submenu [System information] contains details of the connected devices and information on network connection diagnosis. 50/88 Operation Manual UniversalExtractor E-800...

  • Page 51: Solvent Menu

    The status bar shows actual information about the instrument (e.g. extraction method, LAN connection, etc.). Selecting a method for an extraction position NOTE Combination of solvents with far apart boiling points. Do not use solvents with boiling point differences higher than 20 °C. Operation Manual UniversalExtractor E-800 51/88...

  • Page 52: Editing A Method

    Tap the function [OK] on the function bar. ð The display shows the view Method Tap the function [Save] on the function bar. ð The method is saved. 6.6.2 Changing the name of a method Navigation path ➔ 52/88 Operation Manual UniversalExtractor E-800...

  • Page 53: Setting The Solvent Of A Method

    Activating the checkbox enables the inert gas during the extraction steps. [Inert gas Rinse] Activating the checkbox enables the inert gas during the rinse step. [Inert gas Drying] Activating the checkbox enables the inert gas during the drying step. Operation Manual UniversalExtractor E-800 53/88...

  • Page 54: Setting The Extraction Time Of A Method

    — If the extraction time and a number of extraction cycles is set, the extraction will finish once both settings are fulfilled. The number of extraction cycles is selectable from 0 to 5940. Navigation path ➔ Navigate to the [Method] menu via the navigation path. 54/88 Operation Manual UniversalExtractor E-800...

  • Page 55: Setting The Extraction Heating Level Of A Method

    ð The heating level is saved. 6.6.8 Setting the chamber heater (Soxhlet Warm, Hot and Twisselmann Extraction) The heating steps are selectable from 0 to 10. Navigation path ➔ Navigate to the [Method] menu via the navigation path. Operation Manual UniversalExtractor E-800 55/88...

  • Page 56: Setting The Soxhlet Valve Open Time Of A Method (Soxhlet And Soxhlet Warm Extraction)

    The sample structure is easily releasing the solvent. [max] The extraction glass chamber universal LSV is used. The sample structure is slowly releasing the solvent. Navigation path ➔ Navigate to the [Method] menu via the navigation path. 56/88 Operation Manual UniversalExtractor E-800...

  • Page 57: Setting The Rinse Time Of A Method (Soxhlet, Soxhlet Warm, Hot And Twisselmann Extraction)

    Change the rinse heating level to compensate ambient conditions. WARNING Setting the heating level too high The consequences are device damage, serious injuries or death. Use the pre-set heating levels. Adjust the heating level to compensate the ambient conditions. Operation Manual UniversalExtractor E-800 57/88...

  • Page 58: 6.6.12 Setting The Number Of Dry Steps

    Incorrect drying step settings can damage the analyte and the beaker. Use the analyte protection for the first drying step. Change the default setting to the optimized parameters of your application. See "Technical Note: Heating guide for UniversalExtractor E-800 ". Obey all safety precautions. See Chapter 2.6 "Residual risks", page 12 Checkbox...

  • Page 59: 6.6.14 Setting The Time For A Dry Step

    Enter the value in the numeric input box. Tap the function [OK] on the function bar. ð The dialog box closes. Tap the function [Save] on the function bar. ð The time for the drying step is saved. Operation Manual UniversalExtractor E-800 59/88...

  • Page 60: 6.6.15 Setting The Heating Level For A Dry Step

    Changing the name of a solvent (own created solvents only) Navigation path ➔ Navigate to the [Solvent] menu via the navigation path. Tap the name of the solvent you wish to edit. ð The display highlights the selection in green. 60/88 Operation Manual UniversalExtractor E-800...

  • Page 61: Changing The Chamber Heating Level (Option)

    Tap the action [Manually]. ð The display highlights the action [Heating level] in white. Tap the action [Heating level]. ð The display shows a dialog box with a numeric input box. Enter a heating level for the solvent. Operation Manual UniversalExtractor E-800 61/88...

  • Page 62: Changing The Boiling Point Of A Solvent

    ð The display shows a dialog box with a numeric input box. Enter the enthalpy for the solvent. Tap the function [OK] on the function bar. ð The value for the enthalpy is saved. ð The dialog box closes. 62/88 Operation Manual UniversalExtractor E-800...

  • Page 63: Changing The Molecular Weight Of A Solvent

    ð The display shows a dialog box with a numeric input box. Enter the density for the solvent. Tap the function [OK] on the function bar. ð The value for the density is saved. ð The dialog box closes. Operation Manual UniversalExtractor E-800 63/88...

  • Page 64: Performing An Extraction

    Instead of glass sample tube with frit it is possible to insert a thimble. Put the holder for the glass sample tube with frit into the extraction chamber. Put the glass sample tube with frit into the holder in the extraction chamber. 64/88 Operation Manual UniversalExtractor E-800...

  • Page 65: Adjusting The Optical Sensor (Soxhlet, Soxhlet Warm And Hot Extraction)

    Select different methods for each extrac- See Chapter 7.2.2 "Selecting different tion position. methods for each extraction position", page 66 Select a programmed setup. See Chapter 7.2.3 "Selecting a pro- grammed setup", page 66 Operation Manual UniversalExtractor E-800 65/88...

  • Page 66: Selecting A Method For All Extraction Positions

    Selecting the extraction positions The extraction positions can show the following status: Status Meaning The extraction position is activated. The extraction position will be heated. The extraction position is not activated. The extraction position will not be heated. 66/88 Operation Manual UniversalExtractor E-800...

  • Page 67: Starting An Extraction

    — For Soxhlet, Soxhlet Warm and Hot Extraction. See Chapter 7.1.3 "Adjusting the optical sensor (Soxhlet, Soxhlet Warm and Hot Extraction)", page 65 — For Twisselmann Extraction . See Chapter 7.1.2 "Adjusting the optical sensor (Twisselmann and Continuous Extraction only)", page 65 Operation Manual UniversalExtractor E-800 67/88...

  • Page 68: Task During Performing An Extraction

    A beaker is placed under the position. An extraction glass chamber is installed at the position. The lift is in the lower position. Insert the nozzle of the dispenser into the condenser. Add solvent with a dispenser. 68/88 Operation Manual UniversalExtractor E-800...
  • Page 69 A not correctly installed condenser can cause skin burns or a building fire A beaker is placed under the position. An extraction glass chamber is installed at the position. The lift is in the lower position. Put a funnel on the condenser. Add solvent through the funnel. Operation Manual UniversalExtractor E-800 69/88...

  • Page 70: Ending An Extraction

    Exporting extraction parameters without cloud connection Precondition: R The App is installed on a mobile device. R An extraction is finished. Tap the button [QR Code] on the function bar. ð The display shows a QR code. 70/88 Operation Manual UniversalExtractor E-800...

  • Page 71: Exporting Extraction Parameters With Cloud Connection

    R The App is installed on a mobile device. R An extraction is finished. R The instrument is connected via LAN cable. See Chapter 5.18 "Mobile connection", page 44 The extraction parameters are automatically transferred to the App. Operation Manual UniversalExtractor E-800 71/88...

  • Page 72: Cleaning And Servicing

    Make sure that the cleaning agent meets the requirements of the safety data sheets for the chemicals used. Make sure that the cleaning agent is compatible with the materials used. See Chapter 3.5 "Technical data", page 25 If you have any further questions, contact BUCHI Customer Service. Component Action Frequency Solvent tank Empty the solvent tank.

  • Page 73: Removing The Tank Bottle

    Heating plate Wipe down the heating plate with a Weekly damp cloth. If heavily soiled, use ethanol or a mild detergent. If cracked or broken, contact BUCHI customer service. Hoses and hose con- Check the hoses and hose connections Weekly nections for defects (cracks, brittle areas).

  • Page 74: Draining Solvent From The Instrument

    Open the tank valves Navigation path ➔ ➔ [Service] ➔ [Actors] ➔ [Valves] Navigate to [Valves] via the navigation path. ð The display shows the view Valves Select the position of the tank valve you wish to open. 74/88 Operation Manual UniversalExtractor E-800...

  • Page 75: Switch Of The Pump

    Wait until all solvent is in the tank bottle. Close the tank valve. 8.3.3 Switch of the pump Navigation path ➔ ➔ [Service] ➔ [Actors] Navigate to [Actors] via the navigation path. ð The display shows the view Actors Disable the action [Pump]. Operation Manual UniversalExtractor E-800 75/88...

  • Page 76: Help With Faults

    Add solvent. See Chapter "Adding solvent through the condenser with a funnel", page 69 Loss of solvent Seals wrong, deformed or Exchange the seals. damaged Incorrect positioning of the Contact BUCHI Customer beaker/ glassware and seals Service. 76/88 Operation Manual UniversalExtractor E-800...

  • Page 77: Draining Solvent From Extraction Glass Chamber Universal

    Navigate to [Valves] via the navigation path. ð The display shows the view Valves Select the position of the Soxhlet valve you wish to open. Open the Soxhlet valve. Wait until the extraction glass chamber is empty. Close Soxhlet valve. Operation Manual UniversalExtractor E-800 77/88...

  • Page 78: Taking Out Of Service And Disposal

    When disposing, observe the disposal regulations of the materials used. Materials used see Chapter 3.5 "Technical data", page 25 10.3 Returning the instrument Before returning the instrument, contact the BÜCHI Labortechnik AG Service Department. https://www.buchi.com/contact 78/88 Operation Manual UniversalExtractor E-800...

  • Page 79: Appendix

    Water out Connection Condenser CW OUT Condenser Condenser Flow meter (inside instrument) Condenser Condenser Connection CW Tank OUT Condenser solvent tank CW IN Condenser Connection solvent tank CW Tank IN CW OUT Fig. 13: Condenser circuit Operation Manual UniversalExtractor E-800 79/88...

  • Page 80: 11.1.2 Solvent Collector Schematic

    °C) [g/mL] mol] mol] 2-Propanol (Iso- 39.85 60.1 0.78 propanol, iPrOH) Acetone (Propanon, 56.05 29.1 58.08 0.791 AcMe) Acetonitril (MeCN) 81.65 29.75 41.05 0.78 Benzene 80.09 30.72 78.11 0.8765 Butanon 79.59 31.3 72.11 0.805 (Methylethylketon, AcEt) 80/88 Operation Manual UniversalExtractor E-800...

  • Page 81: Spare Parts And Accessories

    0.86 11.3 Spare parts and accessories Use only genuine BUCHI consumables and spare parts in order to ensure correct, safe and reliable operation of the system. NOTE Any modifications of spare parts or assemblies are only allowed with the prior written permission of BUCHI.

  • Page 82: 11.3.2 Spare Parts

    Allows for turning the instrument for easier access. 11.3.2 Spare parts Order no. Image Extraction glass chamber universal 11062501 Extraction chamber universal inert 11064849 Extraction chamber universal LSV 11062502 Extraction chamber universal LSV inert 11064850 82/88 Operation Manual UniversalExtractor E-800...
  • Page 83 11070136 Soxhlet assembly cpl. 11067065 One part constiting of magnetic valve and level sensor for extraction glass chamber Soxhlet Set of seals E-800, PTFE, 2 pcs. 11067483 Membrane with anchor for magnetic valve unit 037534 Operation Manual UniversalExtractor E-800 83/88...

  • Page 84: 11.3.3 Conversion Kits

    6 pcs. Set of draining tubes ECE, FEP 11067479 11.3.3 Conversion kits The UniversalExtractor E-800 can be converted into another configuration with an easy change of glass assembly. Order no. Conversion kit from Soxhlet / Universal to ECE 11068488...

  • Page 85: 11.3.5 Consumables

    11067814 Working volume: 116 mL Filling volume: 144 mL Extraction thimbles 25 x 100 mm, 25 pcs. 018105 Working volume: 44 mL Extraction thimbles 33 x 94 mm, 25 pcs. 11058983 Working volume: 64 mL Operation Manual UniversalExtractor E-800 85/88...

  • Page 86: Holder For Extraction Thimbles

    11068485 Holders for thimbles d43, stainless steel, 6 pcs. 11068486 Set of holders for glass sample tubes with frit, PTFE, 3 pcs. 11067485 Set of holders for LSV glass sample tubes, PTFE, 3 pcs. 11067486 86/88 Operation Manual UniversalExtractor E-800...
  • Page 88 T +971 4 313 2860 T +52 55 9001 5386 F +66 2 862 08 54 F +971 4 313 2861 latinoamerica@buchi.com bacc@buchi.com middleeast@buchi.com www.buchi.com/es-es www.buchi.com/th-th www.buchi.com We are represented by more than 100 distribution partners worldwide. Find your local representative at: www.buchi.com...

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