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Product Overview Unpacking and System Setup Model 3321 Description of the APS ™ Aerodynamic Particle Sizer ® Spectrometer Spectrometer Spectrometer ™ Operations Operation and Service Manual Theory of Operation Appendixes Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
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M a n u a l H i s t o r y The following is a manual history of the Model 3321 Aerodynamic Particle Sizer ® Spectrometer (Part Number 1930092). Revision Date Preliminary March 1997 Preliminary 2 September 1997...
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TSI Incorporated. APS is a trademark of TSI Incorporated. Microsoft, Windows, are registered trademarks of Microsoft Corporation. ® Swagelok is a registered trademark of Swagelok Companies, Solon, Ohio. ® Model 3321 Aerodynamic Particle Sizer Spectrometer Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
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S a f e t y This section gives instructions to promote safe and proper handling of the Model 3321 Aerodynamic Particle Sizer ® Spectrometer. There are no user serviceable parts inside the instrument. Refer all repair and maintenance to a qualified technician. All maintenance and repair information in this manual is included for use by a qualified technician.
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L a b e l s The Model 3321 has eight labels as shown in Figure 1. 1. Laser Safety Information Label (back panel) 2. Serial Number Label (back panel) 3. Customer Service Label (back panel) 4. Danger High Voltage Label (Power Entry Module) 5.
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D e s c r i p t i o n o f C a u t i o n / W a r n i n g S y m b o l s The following symbols and an appropriate caution/warning statement are used throughout the manual and on the Model 3321 to draw attention to any steps that require you to take cautionary...
Submitting Comments ................ xiv CHAPTER 1 Product Overview ............1-1 Product Description ................1-1 Applications ..................1-2 How the 3321 Operates ..............1-2 System History .................. 1-4 CHAPTER 2 Unpacking and System Setup ........2-1 Packing List ..................2-1 Mounting the Sensor ................. 2-1 Ventilation Requirements ..............
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B—Beep ..................C-15 C—Clear Buffer and Sample Time ..........C-15 D—Dump ..................C-15 F—Fill Accumulators ..............C-15 G—Go ..................C-16 ® Model 3321 Aerodynamic Particle Sizer Spectrometer Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
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How to Input Commands and Troubleshoot the Results ....C-29 Input Guidelines ................C-29 Troubleshooting Input ..............C-29 APPENDIX D Model 3321 Specifications ........... D-1 Reader’s Comments Contents Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
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2-2 Install the Sensor on a Clean, Hard Surface and Provide Adequate Clearance for Ventilation ..........2-3 2-3 Serial Port Connector on the Back of the Model 3321 ....2-4 2-4 I/O Port of the Model 3321 APS™ Spectrometer ......2-5 3-1 Front Panel of the Model 3321 APS™...
A b o u t T h i s M a n u a l P u r p o s e This is an operation and service manual for the Model 3321 Aerodynamic Particle Sizer (APS ) Spectrometer.
(µm). It detects light-scattering intensity for particles from 0.3 to 20 µm. For setup and initial sampling, the Model 3321 can be operated without a computer. To save, interpret, or print data, however, it must be connected to a computer or some other data collection system.
H o w t h e 3 3 2 1 O p e r a t e s Aerodynamic diameter is the most important size parameter because it determines a particle’s airborne behavior. The Model 3321 is specifically engineered to perform aerodynamic size measurements in real time using low particle accelerations. ...
Previous time-of-flight spectrometers used two tightly focused laser beams, resulting in two distinct signals for each particle. As shown in Figure 1-2, the Model 3321 overlaps the two laser beams, producing one double-crested beam profile. Each particle creates a single, continuous signal that has two crests. Particles...
(3 2 -bit on ly), or W in dows 7 (3 2 or 6 4 -bit), Aerosol ® Instrument Manager software. The Model 3321 has several slight design and significant performance improvements over the 3320 for qualitative mass weighted distributions. The sample eduction nozzle has been redesigned to more effectively transport particles out of the detection region to the exhaust.
If any items are missing, notify TSI immediately. Table 2-1 Accessories Packing List Description Part No. Model 3321 Sensor 332100 ® Model 3321 Aerodynamic Particle Sizer Spectrometer 1930092 Manual ® Aerosol Instrument Manager Software 390059 ®...
[16.3 mm] 8.80 [223.5 mm] 3.28 [83.3 mm] Figure 2-1 Remove the Rubber Feet on the Base Plate to Mount the Model 3321 on Another Surface Ventilation Requirements The APS Sensor cabinet is designed to be cooled by room air ™...
P o w e r C o n n e c t i o n Connect the AC power cord (supplied) to the AC POWER IN connection on the back of the Model 3321 and then into an available power outlet. It is not necessary to select the correct voltage, the sensor accepts line voltage of 85 to 260 VAC, 50 to 60 Hz, 100 W max., single phase.
(Figure 2-3). Use the 4-meter cable provided. If you need a longer cable, use a standard IBM 9-pin, serial extension cable. Figure 2-3 Serial Port Connector on the Back of the Model 3321 APS™ Spectrometer I / O P o r t The APS spectrometer has a 15-pin, D-subminiature connector ™...
I/O Port of the Model 3321 APS™ Spectrometer B N C C o n n e c t o r s There are three BNC connectors on the Model 3321 for output of the following signals. Refer to Chapter 3 for a detailed description of each of the BNC connectors.
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D e s c r i p t i o n o f t h e A P S™ S p e c t r o m e t e r This chapter describes the front panel, back panel and internal components of the Model 3321 Aerodynamic Particle Sizer ® (APS ™)
Status LEDs Inlet Nozzle Control Knob LCD Display Figure 3-1 Front Panel of the Model 3321 APS™ Spectrometer The 320 × 240 pixel LCD display provides continuous real-time display of sample data. Sample data includes: Size distribution. Concentration. ...
Menu. Figure 3-2 Model 3321 Menu Layout Fine adjustment of the control knob (i.e., moving from one channel to the next) is best accomplished using the outer edge of the knob.
Inlet Nozzle The inlet nozzle on the top of the Model 3321 is designed so that aerosol can be sampled from a chamber or open air with good efficiency. Tubing can be attached to the inlet to sample when necessary. The inlet is .746 inches (18.9 mm) in diameter for use ®...
Power consumption and line voltage specifications can be found in Appendix Note: Make certain the line cord is plugged into a grounded power outlet. Position the Model 3321 so the power cord connector is easily accessible. DC Power Input The DC power connector is a quarter-turn quick-connect entry...
Pump Exhaust. Serial Port The Serial Port is a standard RS-232 serial connection that allows communications between the system computer and the Model 3321 spectrometer. Serial commands are sent to and from the ™ computer to provide instrument status and collect data information.
I/O Port This 15-pin, D-subminiature connector port provides three digital input and three digital output pins. It allows various signals to be sent to a data logger or control switches. Refer to Appendix C, "Using Serial Data Commands," for serial commands to control the I/O Port.
Laser PC board ❑ Filters ❑ Power PC board ❑ The only serviceable components of the Model 3321 APS ™ spectrometer are the filters, which require routine maintenance (refer to Appendix A). For a general description of these components, refer to Chapter 3, “Description of the APS...
PC-Board Optics Analog PC-Board Sheath Flow Pump Filters Detector PC-Board Power Supply Figure 3-6 Internal Diagram of the Model 3321 APS™ Spectrometer Description of the APS Spectrometer Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
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A P S™ S p e c t r o m e t e r O p e r a t i o n This chapter describes how to set up and operate the Model 3321 at the sensor using the control knob and LCD display. You can...
6. Return to the Menu to modify the sample time or set other parameters as necessary until you are satisfied that sampling is set up as desired. Model 3321 Aerodynamic Particle Sizer Spectrometer Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
Table 4-1 Description of Menu Items Function (see also Appendix C for serial commands Command related to Menu Items). Exit Exit the Menu and display graphical information. Sample Time [s] Set the total sample time. Can be set from 1 to 64,800 seconds (18 hours) in summed mode and from 1 to 300 seconds in average mode.
Exit Exit the Menu and display graphical information. C o l l e c t i n g D a t a After the Model 3321 APS spectrometer is set up and operating as ™ desired, use the computer and Aerosol Instrument Manager software to collect, save, interpret, and print sample data.
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C H A P T E R 5 T h e o r y o f O p e r a t i o n The Model 3321 is a time-of-flight spectrometer that measures the velocity of particles in an accelerating airflow through a nozzle.
Filter Filter Total-Flow Pump Figure 5-1 Aerosol Flow Through the Model 3321 APS Spectrometer ™ After passing through the orifice, the sheath flow is reunited with the sample flow at the accelerating orifice nozzle. This flow confines the sample particles to the center stream and accelerates the airflow around the particles.
Sample flow is filtered before and after each of the two pumps. The filter upstream of the pump protects the pump from contamination. The filter downstream of the pump prevents contamination of the flow as the pump vanes wear. O p t i c s P a t h The first component in the optics path, see Figure 5-2, is the laser diode.
This signal, referred to as a double crested signal, consists of a pair of peaks. Model 3321 Aerodynamic Particle Sizer Spectrometer Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
Figure 5-3 Typical Example of a Double Crested Signal Each peak represents the presence of the particle in the center of the individual laser beams and can range in amplitude 0–10 volts. The signal is gained and buffered into two channels. One channel is for very small particles and has a high gain.
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An A/D converter is then used to give the digital value of each of the side-scatter-intensity pulse heights. Model 3321 Aerodynamic Particle Sizer Spectrometer Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
The high gain value is checked for an over range in the A/D digital value, which indicates a large particle. If it is over range, the digital value from the low gain A/D is output to the digital module. If it is not over range, the digital value from the high gain A/D is output.
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Event 2. The APS spectrometer can be configured to record data in two ™ different modes: uncorrelated and correlated. Model 3321 Aerodynamic Particle Sizer Spectrometer Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
Coincidence typically increases proportionally with particle concentration. In the case of the Model 3321 APS ™ spectrometer; however, although coincidence is still a problem at high concentrations, the particles are not mis-classified.
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A P P E N D I X A M a i n t e n a n c e Most components of the APS spectrometer are solid state and ™ require no maintenance. This section provides information about the maintenance procedures that are required and includes a suggested maintenance schedule.
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Replace the outer inlet in the nozzle mount. Note that there is an alignment pin that matches a slot in the side of the outer Model 3321 Aerodynamic Particle Sizer Spectrometer Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
inlet. Rotate the outer inlet until the inlet seats on the alignment pin. Replace the cover on the instrument. Tighten the six screws holding the cover in place. Replace the outer inlet retaining ring and tighten firmly. Insert the power cord into the power entry connector on the back of the instrument.
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Note: The outer nozzle is very delicate. Take great care in cleaning or blowing compressed air through the nozzle. Blow clean, compressed air backwards through the outer nozzle to remove any debris. Model 3321 Aerodynamic Particle Sizer Spectrometer Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
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The finish on the outside of the nozzle should be flat black. Remove any coating on the outer nozzle with a clean, lint-free, soft cloth and clean water. Check that the nozzle is clear by holding it up to a light and checking for a clear view through the nozzle orifice.
Tilt the printed circuit board upward and remove the large ribbon cable connector from the center front of the board. Model 3321 Aerodynamic Particle Sizer Spectrometer Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
Check that the flows are correct. R e p l a c i n g t h e E P R O M Normally the EPROM will not be replaced, however, early shipments of the Model 3321 APS spectrometer may not have all ™...
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It is important that they go in the correct sockets. Locate the EPROM sockets from Figure A-1. Model 3321 Aerodynamic Particle Sizer Spectrometer Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
Figure A-1 Location of EPROM Chips on APS™ Spectrometer Digital PC-Board Use the EPROM removal tool provided with the new EPROM chips to remove one of the old chips. Remove the new EPROM with the same seven-digit part number from its static protection bag Install the new chip into the vacant socket by aligning the notch on the top center of the chip with the notch shown on the silkscreen.
The calibration process requires special equipment and tools. Therefore, it is recommended you return the instrument to the factory for calibration. A-10 Model 3321 Aerodynamic Particle Sizer Spectrometer Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
A P P E N D I X B T r o u b l e s h o o t i n g This appendix lists potential problems and their solutions. Note: If none of the solutions provided corrects the problem, call your TSI representative for advice.
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Check for good contact between the power cord and the wall outlet. Check for power at the outlet. Serial Communications not working See Table C-4, “Troubleshooting Serial Commands.” Model 3321 Aerodynamic Particle Sizer Spectrometer Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
P i n C o n n e c t o r s The Model 3321 has a single 9-pin, D-subminiature connector port on the back panel labeled SERIAL PORT (See Figure 3-3 and Figure C-1). This communication port is configured at the factory to work with RS-232 type devices.
B a u d R a t e The baud-rate setting is the rate of communication in terms of bits per second (baud). The Model 3321 uses a baud rate setting of 9600, 19,200 or 38,400. For proper communications, make sure that all software used with the instrument is set at the appropriate rate.
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The four types of commands are: Set commands, which set all the operating parameters for the spectrometer ™ Action commands, which control mechanical components of the spectrometer ™ Read (polled) commands, in which the APS spectrometer ™ sends data in response to a specific request from the computer Unpolled commands, in which the APS spectrometer...
S e t C o m m a n d s Set commands allow you to set up operating parameters for the Model 3321. If a set command is sent with no parameter, the current parameter is echoed. Note: Some of the commands directly affect or are affected by other commands.
To label the calibration done on December 25th of the APS spectrometer with serial number 104: SCLS/N 104 Calibrated December 25, 1997 Model 3321 Aerodynamic Particle Sizer Spectrometer Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
SCE—Set Calibration Environment SCE lets you set the temperature and pressure. SCEp,t where: p = absolute pressure at calibration (in millibars). t = absolute temperature at calibration (in degrees K). SCE with no parameters echoes the current values of p and t, which are saved in EEPROM and loaded into RAM when the instrument is powered up.
To set the outputs for I/O connector pins 11, 12, and 13 to 0 volts: To set the outputs for I/O connector pins 11, 12, and 13 to 5 volts: Model 3321 Aerodynamic Particle Sizer Spectrometer Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
SF—Set Front Panel Enable SF lets you disable the front panel of the Model 3321 to prevent clearing sample averages that are being read by an external computer. where: x = 0 or 1: 0 = front panel disabled 1 = front panel enabled When the front panel is disabled, it has “view only”...
❑ Front panel LED may flash if laser is not able to operate at set power. This indicates that the laser has degraded and may need to be replaced. C-10 Model 3321 Aerodynamic Particle Sizer Spectrometer Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
SMA—Set Mode for Analog Output SMA sets the mode and range for the analog output BNC on the back panel SMAx where: x = 0 to 6 0 = total concentration 1/cc 10 volts. 1 = total concentration 10/cc 10 volts. 2 = total concentration 100/cc 10 volts.
Note: The value of t is saved in EEPROM and loaded when the instrument is powered up. C-12 Model 3321 Aerodynamic Particle Sizer Spectrometer Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
Examples: To set the sample mode to averaging and the sample time to 240 seconds: SMT0,240 To set the sample mode to summing and the sample time to 12 hours: SMT1,43200 To set the sample mode to correlated data (paired) and the sample time to 60 minutes: SMT2,3600 Note: Baud rate must be set to 38,400 for correlated mode.
A c t i o n C o m m a n d s Action commands control mechanical components of the Model 3321. If you enter an action command without a parameter, the mechanical state is echoed back. A—Perform APD Autocal Performs an automatic calibration of the Avalanche Photodetector if autocal is enable by the SMC command, see SMC.
B—Beep Bx,y where: x = no value, 0, 1, >1. no value for x returns 1 if beep is active, 0 if not. A 0 turns beep off; a 1 turns beep on. >1 is number of beeps. y = duration of beep in approximately 62.5 ms steps (for a 1-second beep, y = 16).
Q—Quick Concentration Report Produces a concentration report. This is a 3310 command. A LF is appended after the terminating CR. C-16 Model 3321 Aerodynamic Particle Sizer Spectrometer Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
R e a d C o m m a n d s ( P o l l e d ) Read commands are polled, which means the Model 3321 sends data in response to a specific request from the computer R—Read Accumulator...
Reads bins 400 to 1023 Reads bins 0 to 1023 RF—Read Flags RF returns a four-character hexadecimal value representing the state of the Model 3321. The values for the 10 flags are as follows: 0000 0000 0000 0001 Laser fault...
Reads the accumulated on-time of the instrument (in hours). The time is updated once an hour and stored in EEROM. Example Response Indicates the Model 3321 has been on for approximately 72 hours. RPI—Read Inlet Pressure Reads the current absolute inlet pressure in millibars. Example Response 1013.3...
Example Response 3.96 RQT—Read Total Flow Reads the total flow rate in liters per minute (L/min). Example Response 5.02 C-20 Model 3321 Aerodynamic Particle Sizer Spectrometer Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
Response 298.2 Indicates the internal temperature is 298.2 K or 25.0° C. RTD—Read Temperature of Detector (APD) Reads the APD and optics temperature of the Model 3321. Example Response 306.6 Indicates the APD and optics temperature is 306.6 K or 33.4° C.
RV—Read Firmware Version Reads the current version level of the Model 3321 firmware. Example Response Model 3321 APS Firmware Version 1.12 13-Dec- 2001 U n p o l l e d C o m m a n d s Using unpolled commands instructs the Model 3321 to automatically output data records at specific intervals.
UA—Generate Accumulator Report Record (Report Record A) Enables and disables reporting of Record A in unpolled operation. where: x = 1 Enables A Record x = 0 Disables A Record UA will echo current setting 0 or 1. See Record A in the “Unpolled Record Formats”...
UY will echo current setting 0 or 1. See Record Y in the “Unpolled Record Formats” section of this chapter. C-24 Model 3321 Aerodynamic Particle Sizer Spectrometer Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
= 4 digit hex value for status flags (see RF command) stime = sample time not corrected for dead time dtime = dead time (ms for 3321, µs for 3320) evt1 = number of single hump events evt3 = number of 3+ hump events...
= 4 digit hex value for status flags (see RF command) stime = sample time not corrected for dead time dtime = dead time (ms for 3321, µs for 3320) evt1 = number of single hump events C-26...
= 4 digit hex value for status flags (see RF command) stime = sample time not corrected for dead time dtime = dead time (ms for 3321, µs for 3320) evt1 = number of single hump events evt3 = number of 3+ hump events...
= 4 digit hex value for status flags (see RF command) stime = sample time not corrected for dead time dtime = dead time (ms for 3321, µs for 3320) evt1 = number of single hump events evt3 = number of 3+ hump events...
tpumpv = total pump voltage itemp = inlet temperature in degrees C (ex. 25.5) btemp = internal box temperature in degrees C (ex. 31.5) dtemp = detector temperature for APD and optics in degrees C (ex: 25.5) = APD operating voltage in volts H o w t o I n p u t C o m m a n d s a n d T r o u b l e s h o o t t h e R e s u l t s Use the following information as a guide to inputting software...
Incorrect baud rate Software must be set at 9600, 19200, or 38400 baud to match instrument setting. Also check computer hardware. RS232 chip on the Model 3321 Contact TSI. Refer to "Contacting Customer Service." Model 3321 is locked up Remove power from the Model 3321, then apply power to the instrument.
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S p e c i f i c a t i o n s The following specifications—which are subject to change—list the most important features of the Model 3321. Table D-1 ® Specifications of the Model 3321 Aerodynamic Particle Sizer (APS ) Spectrometer ™ Measurement technique .......
(internal to power supply -- not accessible by operator) ......~T 6.3A SB/250V TSI and TSI logo are registered trademarks of TSI Incorporated. Model 3321 Aerodynamic Particle Sizer Spectrometer Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
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I n d e x analog module (continued) side-scatter circuit, 5-6 AC power connector, 3-5 Analog Out, 3-7 accumulator (TOF) data record (A), C-25 analog PC board, 3-8 action commands, C-4, C-14 APD module, 5-4 beep, C-15 applications, 1-2 clear buffer and sample time, C-15 APS.
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Hi Conc, 3-4 read sheath flow, C-20 Laser, 3-4 read temperature in box, C-21 Particle, 3-4 read temperature of detector, C-21 Index-2 Model 3321 Aerodynamic Particle Sizer Spectrometer Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
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read commands (continued) set commands (continued) read temperature of inlet, C-21 set laser power, C-10 read total Delta P, C-20 set mode and sample time, C-12 read total flow, C-20 set mode for analog output, C-11 read firmware version, C-22 set mode for automatic calibration of APD, C-12 read flags, C-18 set pumps, C-13...
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2-2 view information, 3-3 W–X–Y–Z warning, v warning labels location, vi warranty, iii Index-4 Model 3321 Aerodynamic Particle Sizer Spectrometer Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
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Please help us improve our manuals by completing and returning this questionnaire to the address listed in the “About This Manual” chapter. Feel free to attach a separate sheet of comments. ® Manual Title Model 3321 Aerodynamic Particle Sizer Spectrometer P/N 1930092 Rev.
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