Related Manuals for Genevac 04-6682
Summary of Contents for Genevac 04-6682
- Page 1 The Genevac Rocket™ Sample Holders User Manual Original instructions Part number 04-6682 Issue 2-14 February 2014...
-
Page 3: Table Of Contents
Contents Introduction ..........2 ASE Tube Puck ........30 Instructions ........... 31 Safety ............4 Flip-Flop..........32 Warnings and cautions ......4 Precautions ..........5 Spare parts ........... 33 Limitations of use ........5 Vial seals ..........33 Sample holder range ......6 Instructions ........... -
Page 4: Introduction
Rocket Sample Holders User Manual Introduction The sample holders described in this user manual are for use with the Genevac Rocket™ evaporator. SampleGenie GC vial system ASE tube Puck * Standard flask Flip-Flop - for use with ASE tube Puck With the selection of the appropriate sample holder, the Rocket evaporation system can be can be set up to dry samples completely or to concentrate samples to a small volume. - Page 5 Any imperfections (such as chips, scratches or labels applied to the flasks) are likely to cause leaks which will slow down the evaporation process. The advice and instructions contained within this manual will assist in the day to day use and maintenance of the Rocket sample holders. 04-6682 Issue 2-14 February 2014...
-
Page 6: Safety
User Manual Safety Warnings and cautions This symbol is used within this manual to highlight Warnings and Cautions. Warning: highlights a risk of material damage or personal injury Caution: highlights a risk of material damage. 04-6682 Issue 2-14 February 2014... -
Page 7: Precautions
Caution: Incorrect loading may result in damage to samples and to the Rocket evaporator. This user manual should be referred to in conjunction with the Genevac Rocket™ Evaporation System User manual. Only allow users who are familiar with all the issues outlined in this, and the Rocket user manual to use the Rocket sample holders. -
Page 8: Sample Holder Range
GC vial system Sample Genie ASE tube puck with collar and pad If your Rocket rotor looks like this: …it does not have flask-adapters and it is safe for use with the sample holders shown above: 04-6682 Issue 2-14 February 2014... -
Page 9: Older Sample Holders
Note: Sample holder components are not interchangeable between different sample holder types or versions. Do not attempt to exchange parts, e.g. do not attempt to fit a SampleGenie collar onto a SampleGenie 04-6682 Issue 2-14 February 2014... -
Page 10: Flask-Adapters - Removal
For instructions, refer to the Rocket User Manual. To avoid the risk of inadvertent use of non-compatible sample holders, Genevac recommend that all Rocket evaporators in a common location, should have the same rotor configuration with flask adapters removed and any early type sample holders should be upgraded to the later type. -
Page 11: Accessories
Rocket Sample Holders Accessories Seal removal tool A seal removal tool (Genevac part number: 04-8321) is supplied with SampleGenie . The tool can be used to remove the seal assembly from the SampleGenie flask without risk of damage to flask or seals. -
Page 12: Flask Rack
Flasks may also be placed in the flask rack to fill with samples. Flask splash cap Flasks should be sealed using flask splash caps (Genevac part number for set of six: 70-1265) before carrying in the rack. Flask splash cap... -
Page 13: Single Flask Holder
User Manual Rocket Sample Holders Single flask holder A single flask holder (Genevac part number: 04-6381) is available for use as a balance nest. Single flask holder 04-6682 Issue 2-14 February 2014... -
Page 14: Standard Flask
Spare parts Item Description Part number Quantity in set Complete assembly (excluding flask splash caps) 70-1321 Flask splash cap 70-1265 Standard flask 70-1170 Collar pad 70-1317 Collar 70-1319 04-6682 Issue 2-14 February 2014... -
Page 15: Instructions
Note: If rotor has flask-adapters, no not fit collar and collar pads to flasks. If rotor does not have flask adapters, flask collars and pads must be fitted to flasks. 04-6682 Issue 2-14 February 2014... -
Page 16: Gc Vial System
The evaporator can be set up to stop automatically with a small volume of solvent remaining in each vial. Note: GC vial system is for use in Rocket evaporators that do not have flask adapters fitted to the rotor. See: Limitations of use. 04-6682 Issue 2-14 February 2014... -
Page 17: Spare Parts
(perfluoroelastomer seals have a small notch for identification purposes). White viton seal Perfluoroelastomer seal Notch Note: Always check to make sure the sample holder seals are compatible for use with the solvent being evaporated. See: Acceptable solvents. 04-6682 Issue 2-14 February 2014... -
Page 18: Instructions
Place a vial seal on top of the vial with the sealing lip facing the vial and the flat side facing upwards. Vial seal (flat side up) Insert the GC vial and GC vial adapter into the neck of the GC flask. Make sure the vial locates squarely against the vial seal. 04-6682 Issue 2-14 February 2014... - Page 19 Repeat for the remaining flask assemblies and fill the flasks with samples. Balance the flasks to within 10 g. Insert the flask assemblies into the Rocket rotor. Note: The vial seal adapter should be removed from the flask when the sample holder is not in use. 04-6682 Issue 2-14 February 2014...
-
Page 20: Samplegenie
Rocket Sample Holders User Manual SampleGenie Using SampleGenie samples can be dried directly into vials. Note: SampleGenie is for use in Rocket evaporators that do not have flask adapters fitted to the rotor. See: Limitations of use. 04-6682 Issue 2-14 February 2014... -
Page 21: Spare Parts
70-1661 Seal removal tool 04-8321 Please supply a sample of your vials, Genevac will supply vial adapters to match (size limits apply) Note: The SampleGenie flask includes non-wetted elastomer seals which are designed to tolerate the steam environment of the outer chamber only; they should not be exposed to solvents. -
Page 22: Vial Seal Assembly
A code on the base of the vial adapter, indicates its compatibility; only use the vial adapter with the SampleGenie set and vial type for which it was specified. For further information, contact your local Genevac representative. 04-6682 Issue 2-14 February 2014... -
Page 23: Vial Adapter Pad
Vial seated on vial adapter pad Note: Vial adapter pads must be used with larger vials (25 mm diameter or larger). 04-6682 Issue 2-14 February 2014... -
Page 24: Instructions
Insert the SampleGenie3 vial seal assembly into the neck of the flask and push until it locates against the shoulder of the flask. vial seal Note: Alternating the orientation of the seal with each use, will help prevent it becoming deformed. 04-6682 Issue 2-14 February 2014... - Page 25 Fill with samples, balancing each assembly to within 10 g. Load the SampleGenie3 assemblies into the Rocket rotor in a balanced configuration. Caution: Do not over-tighten. Over-tightening can result in breakage of the sample holder causing unrecoverable sample loss. 04-6682 Issue 2-14 February 2014...
- Page 26 User Manual Caution: Sharp, metallic tools can scratch the glass sealing face of the flask, causing leaks that may result in unrecoverable sample loss. Use the Genevac seal removal tool only for prizing the vial seal from the flask. 04-6682 Issue 2-14 February 2014...
-
Page 27: Retightening Before Restart
If there is a delay between preparing the sample holders and starting the evaporator, the vial adapters should be retightened. The vial adapters should also be retightened whenever the evaporator is stopped and restarted. 04-6682 Issue 2-14 February 2014... -
Page 28: Samplegenie
Spare parts are available for the legacy product; new systems are supplied with SampleGenie Note: The assembly shown is for use in Rocket evaporators that do not have flask adapters fitted to the rotor. 04-6682 Issue 2-14 February 2014... - Page 29 70-1317 Vial adapter pad 70-1323 Specify quantity when ordering Please supply a sample of your vials, Genevac will supply vial adapters to match (size limits apply) Caution: Do not fit a SampleGenie collar to a SampleGenie flask. 04-6682 Issue 2-14 February 2014...
-
Page 30: Vial Adapters
SampleGenie set and vial type for which it was specified. For further information, contact your local Genevac representative. Vial adapter pad Vial adapters for vials of 25 mm diameter and larger (including 20 ml scintillation vials) have a vial adapter pad which clips into a recess in the base of the vial adapter well;... -
Page 31: Instructions
Screw the vial adapter onto the flask. Repeat for the remaining SampleGenie assemblies. Fill with samples, balancing each assembly to within 10 g. Load the SampleGenie assemblies into the Rocket rotor in a balanced configuration. 04-6682 Issue 2-14 February 2014... -
Page 32: Ase Tube Puck
Each ASE tube puck, accepts three ASE tubes or Flip-Flops, allowing a total capacity of 18 tubes in the evaporator. Puck seals Spare parts Description Part number Quantity in set ASE tube puck – complete assembly 70-1282 Puck seal 70-1287 04-6682 Issue 2-14 February 2014... -
Page 33: Instructions
If necessary, release the clamp and rest on the base of the puck. agitate the tubes to reseat the puck assembly O-rings; then re-clamp. Load the puck assemblies into the Rocket rotor. Press down the clamping lever. 04-6682 Issue 2-14 February 2014... -
Page 34: Flip-Flop
Rocket Sample Holders User Manual Flip-Flop The Flip-Flop sample holder format simplifies the process for concentrating the sample ® extract from a Dionex ASE system* by eliminating the need to transfer samples by a separate process. 04-6682 Issue 2-14 February 2014... -
Page 35: Spare Parts
White viton seal Perfluoroelastomer seal Notch Note: Always check to make sure the sample holder seals are compatible for use with the solvent being evaporated. See: Acceptable solvents. 04-6682 Issue 2-14 February 2014... -
Page 36: Instructions
Caution: Follow the instructions carefully. The vial cover and funnel must be tightened correctly. If the assembly is too tight, the vial cover may be damaged; too loose, the seal may leak and cause damage to the samples. 04-6682 Issue 2-14 February 2014... -
Page 37: Loading Sample Holders
A set of six blanking plug must be balanced to within 10 g. Avoid the can be ordered using Genevac part number cumulative imbalance by distributing any 04-5865/S. minor weight variations evenly around the rotor. -
Page 38: Cleaning And Maintenance
The following page provides additional instructions for the cleaning of specific sample holder types. Caution: Do not quench or submerge sample holders in any cleaning solvents (including water). 04-6682 Issue 2-14 February 2014... -
Page 39: Flask Assembly Cleaning
A small hole is provided on the side of the funnel so a narrow tool (such as a paper clip) may be inserted to remove the tube seal. Insert a narrow tool here to remove the tube seal 04-6682 Issue 2-14 February 2014... -
Page 40: General Maintenance
Leave the Flip-Flop disassembled when not in use. Flip-Flop maintenance Do not leave the Flip-Flop funnel to soak in any cleaning solvent (including water) Use only high quality vials. Genevac recommend 60 ml ASE collection vials from I-Chem or Dionex. 04-6682 Issue 2-14 February 2014... -
Page 41: General Routine Checks
General routine checks Check the condition of all sample holders before each use; if there is any structural damage (if any part of a sample holder is bent or deformed) do not use it. Contact Genevac Service for evaluation. Replace any defective seals or O-rings at the first sign of wear. -
Page 42: Troubleshooting
Twist sample holder to break remove from rotor holder seal Sample leaks from Flip-Flop Vial cover / funnel not Tighten vial cover to funnel, screwed together tightly refer to Flip-Flop enough Vial seal worn Replace vial seal 04-6682 Issue 2-14 February 2014... -
Page 43: Technical Data
Vial seals - SG White vitonor perfluoroelastomer Vial seals - SG PTFE sealWhite silicon rubber ASE tube puck Capacity 3 x ASE tubes per puck Vial seals White vitonor perfluoroelastomer Tube seals White Viton or perfluoroelastomer 04-6682 Issue 2-14 February 2014... -
Page 44: Acceptable Solvents
Limitations apply to GC vial system , SampleGenie , and Flip-Flop with perfluoroelastomer seals and to SampleGenie Consult your Genevac representative for advice before using Rocket sample holders with any solvents that are not listed. 04-6682 Issue 2-14 February 2014... -
Page 45: Colour Variation Of Surface Finish
Where this occurs it does not affect the performance or integrity of the component or assembly. Patents Genevac products are protected by the following patents and patent applications: 0905450.3 PCT/GB2010/050523... -
Page 46: Amendment Control
Layout and clarification review. Standard flasks may be cleaned in dishwasher with spindle tray. 2-13 Specify do not quench or soak in any solvent including water. 15-Nov-13 2-14 Colour variation of surface finish added. Original instructions 18-Feb-14 statement added. 04-6682 Issue 2-14 February 2014... -
Page 48: Useful Information
Genevac Limited. applications@genevac.com If you need to contact Genevac for assistance, use either the telephone or Web site: fax Hotlines shown. Alternatively, email or visit our web site.
Need help?
Do you have a question about the 04-6682 and is the answer not in the manual?
Questions and answers