Related Manuals for Genevac Rocket 4D
Summary of Contents for Genevac Rocket 4D
- Page 1 Genevac Rocket ™ Evaporation System User Manual Original instructions Part number 04-7848 Issue 2-4 August 2014...
-
Page 3: Table Of Contents
System Information ........22 EC declaration of conformity......53 Warranty statement ........54 System Optimisation ......... 23 Returning equipment to Genevac ....54 Condenser ............ 23 Chiller warranty and service ......54 Delta T ............23 Model / serial number ........55 Coolant stabilisation ........ -
Page 4: Overview
Rocket 4D Evaporation System User Manual Overview 04-7848 Issue 2-4 August 2014... - Page 5 User Manual Rocket 4D Evaporation System Item Feature Function Main lid Automatically unlocks when safe to open. Manually lift to access the vacuum chamber and inner lid. Lid coupling Connect the feed line to the evaporation vessel when the main lid is closed (feed systems only).
-
Page 6: Safety
Do not place objects on top of the evaporator. Refer to the Genevac published list of acceptable solvents for solvent compatibility information. Clean up any solvent spillage immediately. -
Page 7: Combustible Solvents
To shutdown in an emergency, switch off the power socket at the wall and unplug (or simply unplug if there is no switch). All Genevac evaporators are designed to be safe, with respect to samples, when switched off in an emergency. The system will automatically vent and the rotor (evaporation vessel) will spin down slowly when power is removed. -
Page 8: Basics
Basics Power up Before switching on, check that power cables are connected (two to the rocket 4D and one to the re-circulating chiller) and all other cables and hoses are connected as shown in: Service connections. Switch on the Rocket4D power switch and switch on the chiller. -
Page 9: Controls
User Manual Rocket 4D Evaporation System Controls Menu screens interact with the controls for programming, selecting methods and operating the evaporator. Screen: Menus allow quick access to everyday functions for method selection and alteration, and an intuitive guide to advanced features. At-a-glance system status information is shown during the evaporation process. -
Page 10: Lcd Screen
Rocket 4D Evaporation System User Manual LCD screen Graphical and numerical information relating to system status and evaporation progress is shown during evaporation. Single Solvent Feed d (1 / 2) +38.8°C 33 mbar -1.0 °C +9.15 °C #00:43.01 time 1:00... -
Page 11: Opening The Lid
User Manual Rocket 4D Evaporation System Opening the lid Using the handle, manually lift the lid to the A lid stand provides safe storage for the lid fully open position. while samples are being loaded or unloaded. Note: The main lid cannot be opened when the power is switched off or when the evaporator is operating. -
Page 12: Baffles
Rocket 4D Evaporation System User Manual Baffles For feed enabled Rocket 4D evaporators, two types of baffle are supplied. To ensure even distribution of liquid around the evaporation vessel, it is important the correct baffle is used. Batch baffles Feed baffle... -
Page 13: Getting Started
Getting Started Batch mode Feed mode To start Rocket 4D in batch mode: To start Rocket 4D in feed mode (feed enabled systems only): Check / top-up the chamber water level. Load the evaporation vessel into the Check / top-up the chamber water level. -
Page 14: Starting The Evaporator
Rocket 4D Evaporation System User Manual Starting the evaporator Stopping When a method is selected and the start The evaporator stops automatically when button is pressed, the screen displays the the evaporation process is complete. method settings momentarily whilst the rotor spins up. -
Page 15: Evaporation Vessel
Tilt the evaporation vessel to elevate the lifting points to prepare the evaporation pouring spout above the liquid level before vessel for lifting out of the Rocket 4D. removing the stopper from the spout; then pour the contents from the vessel. -
Page 16: Draining The Condenser
Rocket 4D Evaporation System User Manual Draining the condenser In normal operation, draining is fully automatic and requires no user intervention. However, if manual draining is required, go to the Method Select menu, select the Drain Condenser option then press the start button... -
Page 17: Menu Overview
User Manual Rocket 4D Evaporation System Menu overview The menus allow quick access to everyday functions and to advanced features. Select <BACK> or press the stop button to return to a previous menu (some menus revert automatically after a short period). -
Page 18: Method Guide
User Manual Method guide The Rocket 4D can store up to ten individual methods which can be accessed from the Method Select menu. Factory loaded methods are described below (methods on your Rocket may differ if they have been over-written). -
Page 19: Method Select
User Manual Rocket 4D Evaporation System The second stage only then repeats as required to evaporate any remaining Method select solvent from the evaporation vessel. In the Method Select menu, turn the select control to highlight the desired method on the screen. -
Page 20: Acceptable Solvents
Rocket 4D Evaporation System User Manual Acceptable solvents The solvents listed in the following table will not damage the evaporator, providing appropriate methods are used. Contact your local Genevac representative for advice before using any solvent which is not listed. Solvent Recommended method Acceptable? ■... -
Page 21: Advanced Features
Log files and system appropriate folder. To transfer files from a information can also be downloaded from the data key to Rocket 4D, they must be in the evaporator. root of the \ROCKET\ folder. To Copy methods from a USB data key... -
Page 22: Log Files
Note: The evaporator creates a directory: \ROCKET\ARCHIVE in which to store the methods. Once files are transferred to the Note: Rocket 4D does not have a data key, they may then be transferred to real-time clock. When log files are viewed other evaporators. -
Page 23: Options Menu
Displays temperature in centigrade or Fahrenheit Waste full detect On / Off Enables operation of optional waste full detector Inert Gas Blanket Not applicable for Rocket 4D Inert Gas Purge Not applicable for Rocket 4D Change IGP Not applicable for Rocket 4D... -
Page 24: Reduce Odour
Rocket 4D Evaporation System User Manual Reduce odour Re-dissolve The Reduce Odour function adds a For feed enabled systems, the re-dissolve repeated vent and vacuum cycle to the end feature enables a measured amount of of a method to purge the evaporation fresh solvent to be fed into the evaporation chamber of residual solvent vapours. -
Page 25: System Optimisation
The Rocket 4D software monitors the from a re-circulating chiller which is temperature of coolant entering the remotely controlled by the Rocket 4D to condenser and compares it to the maintain optimum coolant temperature at all temperature of coolant leaving the times. -
Page 26: End Of Stage Trigger Point
Rocket 4D Evaporation System User Manual End of stage trigger point Final stage Once the evaporation process is under way, Once in the final drying stage, the screen the ∆T value peaks when solvent shows a vertical dashed line at the projected evaporation is most rapid. -
Page 27: Method Optimisation
Control Temp: range No heat or 30°C to 60°C (allows heat boost during re-dissolve) Special methods To further optimise the evaporator for specific applications, your local Genevac representative is able to provide special methods; these can be installed easily via a USB data key; for instructions, see: File Transfer. -
Page 28: Maintenance
Any maintenance or repair of this product, The following checks should be performed other than that specified within this user routinely: manual, must be carried out by Genevac or Before use an approved representative of Genevac, using only Genevac approved spare parts. -
Page 29: System Test
Fit the Inner lid. Go to the Method Select Menu and Note: The Rocket 4D System Test is a select the Batch Medium BP (or closest convenient method of checking the integrity equivalent) method. -
Page 30: Periodic Maintenance
Genevac strongly recommend implementing a schedule of planned maintenance. Changing parts in the field is complex and requires a high level of skill. Genevac offers a range of preventive maintenance, service and breakdown contracts designed to keep the equipment in good working order. -
Page 31: Outer Lid Seal
User Manual Rocket 4D Evaporation System Outer lid seal Inner lid seal A kit is available which includes all the parts Grasp the inner lid seal and pull away from required to replace the: the evaporation vessel to remove it, avoid dipping the lid seal into the contents of the ... -
Page 32: Inner Lid Feed Seal
This indicates an O-ring in the lid coupling must be replaced. Remove the inner lid from the Rocket 4D and place it on a suitable work surface. Using long nose pliers, nip the seal on one side of Anti-overfill tube the central tube and pull it out. -
Page 33: Rotary Joint Seals
User Manual Rocket 4D Evaporation System Rotary joint seals Withdraw the PTFE inner liner and two Description Part number Rotary joint seal kit 70-1515/S O-rings from the rotary joint cap. Tools required: Spanner – open 14 mm Spanner – open 17 mm ... -
Page 34: Feed System
Rocket 4D Evaporation System User Manual Feed system Hoses Check the product solution and rinse solvent For descriptions of hose fittings, see Hose feed hoses are undamaged (no sharp bends, connection method in Unpacking and no kinks or constrictions that could affect Setting-up. -
Page 35: Re-Circulating Coolant
User Manual Rocket 4D Evaporation System Re-circulating coolant Draining the re-circulating coolant Use the sight gauge to check the coolant Identify the coolant hose connections to the level. If necessary, open the top cover and evaporator and to the chiller. - Page 36 Rocket 4D Evaporation System User Manual Evaporator and chiller positioned at the same height: Switch off the chiller. Disconnect the quick-release connector for the coolant feed hose the chiller. Evaporator positioned Elevate the end of the hose and allow a...
-
Page 37: Unpacking And Setting Up
Lifting hand-holds Note: Rocket 4D has high friction rubber feet which are designed to prevent movement on the bench; to facilitate moving, it has a skid plate at the back. To manoeuvre the Rocket into position, lift the front and slide it on a skid plate. -
Page 38: Installation Site
Rocket 4D Evaporation System User Manual Installation site Chiller The Rocket 4D must be installed on a level The evaporator is supplied with a and sturdy work surface with provision for: re-circulating chiller. A 75 mm air gap between the... -
Page 39: Hose Connections
User Manual Rocket 4D Evaporation System Hose connections Batch system This overview shows the hose connections for a Rocket 4d Batch system; refer to the installation instructions of the following pages. Vacuum hose Waste solvent container Vacuum pump exhaust adapter... - Page 40 Rocket 4D Evaporation System User Manual Feed system This overview shows the hose connections for a Rocket 4D Feed system. For details, refer to the installation instructions on the following pages. Rinse valve hose Waste solvent container (not supplied) Vacuum hose...
- Page 41 User Manual Rocket 4D Evaporation System Hose connection method Rotary joint feed hose The connection method is similar for both Feed systems only: Connect the pre-cut 6 mm and 8 mm OD PTFE hoses that are length of 6 mm OD PTFE hose to the outlet used.
- Page 42 Rocket 4D Evaporation System User Manual Exhaust hose Feed hoses Connect an 8 mm OD PTFE hose to the Feed systems only: Connect 6 mm OD exhaust outlet. PTFE hoses to the inlet (bottom connector) of the feed valve and to the rinse valve.
- Page 43 Make sure the chiller feed connects to the sufficient capacity to handle solvent Rocket 4D feed, and the chiller return throughput. connects to the Rocket 4D return. To prevent drain failure or the possibility of...
- Page 44 Using the Klein Flange connectors and three to position “1” (as shown). metre vacuum pipe, connect the vacuum pump to the Rocket 4D vacuum inlet. Push the exhaust adapter firmly into the pump exhaust outlet and twist it so the outlet faces the desired direction.
-
Page 45: Electrical Connections
Electrical connections The illustration on this page shows the electrical connections. Connect the vacuum pump to the Rocket 4D via the pump control cable supplied, do not connect the vacuum pump directly to the mains power supply outlet. Power inlet connector 2... - Page 46 Using the pump control cable, connect the Connect the control cable female connector vacuum pump to the pump power outlet to the Rocket 4D socket located under the connector on the Rocket 4D. evaporator control panel. Connect the control cable male connector to the socket located on the front of the chiller, below the control panel.
-
Page 47: Vacuum Chamber Water Reservoir
Refer to the Julabo chiller user manual and set the chiller to remote control mode. Connector for waste solvent full detector As waste solvent can be handled in various ways, no waste solvent full detection system is supplied with Rocket 4D. 04-7848 Issue 2-4 August 2014... -
Page 48: Priming The Cooling System
Rocket 4D Evaporation System User Manual Priming the cooling system To prime the cooling system, follow the instructions in the chiller operating manual. Note: The following additional steps may be required if the Rocket is positioned a significant height above the chiller. -
Page 49: Troubleshooting
If the Rocket 4D detects a safety critical error, it will stop safely and show details of When the evaporation vessel is stationary, the problem on the screen. If a non-critical... -
Page 50: Error Rectification
Instructions for rectification are given where user rectification may be possible. If error codes occur that are not listed, or if the suggested rectification does not resolve the problem, contact your Genevac distributor for further advice. Non-critical errors clear automatically. To clear other error messages, once the cause has been established and rectified, press the stop button. -
Page 51: Fuses
Antisurge (T) Ceramic - Siba 70-065-65-16 04-3766 1¼” x ¼” Antisurge (T) Ceramic - Siba 70-065-65-16 04-3766 Caution: Fuses should only be replaced by suitably trained personnel. If a fuse blows repeatedly, contact Genevac service for assistance. 04-7848 Issue 2-4 August 2014... -
Page 52: Other Troubleshooting
Check the feed hose connections for leaks (look for air bubbles in the feed hoses). Check the feed hoses for kinks or other obstructions. Contact your local Genevac representative for details and availability of spare parts. 04-7848 Issue 2-4 August 2014... -
Page 53: Options
Your local Genevac representative will be Infinity Trolley is a modular trolley system, happy to offer advice or information on the designed to be used with any Genevac full range of sample holders and evaporation system. The lower shelf can be... -
Page 54: Technical Data
The system must be connected to mains power supply outlets by three separate mains power cables (two to the Rocket 4D and one to the re-circulating chiller). Refer to the Julabo User Manual for chiller power requirements. Power cables supplied are 2 m in length and appropriate to the region to which the unit is delivered. -
Page 55: Ec Declaration Of Conformity
Signed: Name: G Broadbent Position: Research and Development Manager Date: July 2014 Being the person appointed by Genevac Ltd to sign on their behalf. *Where option F is feed system (N is option not fitted). 04-7848 Issue 2-4 August 2014... -
Page 56: Warranty Statement
This warranty is any shipping costs incurred. subject to the following provisions: Genevac will not accept any delivery of The system must be sited, installed and equipment which is not accompanied by... -
Page 57: Model / Serial Number
Spout seal kit 70-1515/S Rotary joint seal kit Accessories 70-1186 Lid holder (stainless steel, for inner lid) 70-1151 Pouring stand Patents Genevac products are protected by the following patents or patent applications: 3948/KOLPN/2009 0702503.4 12/294,363 200780014821.9 PCT/GB2010/050523 6682631 2436075 2332865... -
Page 58: Amendment Control
Rotary joint PTFE liners added to consumable parts list. Rotary joint added to Maintenance. Specifications updated. Infinity trolley option introduced. Illustrations updated. Troubleshooting reviewed. R&D amendments. Rocket 4D Declaration of Conformity issued. Emergency shutdown instruction added. Acceptable Solvents updated. Pre-heat evaporator for DMF- instruction added. -
Page 60: Useful Information
Useful information Genevac Limited Read these instructions before operating The Sovereign Centre the Rocket 4D evaporation system and Farthing Road keep them near the system for easy Ipswich reference. Your attention is drawn in IP1 5AP particular to the Safety section.
Need help?
Do you have a question about the Rocket 4D and is the answer not in the manual?
Questions and answers