Drawell DW-TY-9900 Operation Manual
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Drawell DW-TY-9900 Operation Manual

Inductively coupled plasma atomic emission spectrometer
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COMPANY NAME
DW-TY-9900 Inductively Coupled Plasma Atomic Emission
Spectrometer
Operation manual
DRAWELL INTERNATIONAL TECHNOLOGY LIMITED
Chongqing Center : Suite 2605,Building No.11,Shiyou Road No.1, Yuzhong District, Chongqing, China.
Tel: 0086-023-63268643
Shanghai Office : Suite 1101,Lane561 XiuChuan Rd.,PuDong New Area,Shanghai,China
Tel: 0086-021-50966080
Homepage : www.drawell.com.cn
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  • Page 1 COMPANY NAME DW-TY-9900 Inductively Coupled Plasma Atomic Emission Spectrometer Operation manual DRAWELL INTERNATIONAL TECHNOLOGY LIMITED Chongqing Center : Suite 2605,Building No.11,Shiyou Road No.1, Yuzhong District, Chongqing, China. Tel: 0086-023-63268643 Shanghai Office : Suite 1101,Lane561 XiuChuan Rd.,PuDong New Area,Shanghai,China Tel: 0086-021-50966080...

  • Page 2: Table Of Contents

    Chapter 1 DW-TY-9900 Inductively Coupled Plasma Atomic Emission Spectrometer (ICP-AES) Overview............................1 1.1 The Main Structure of ICP-AES....................1 1.2 Brief Description of the Main Working Principle of ICP-AES............1 1.3 Application..........................1 1.4 Instrument Composition and Working Principle................1 1.5 The Main Features........................2 1.6 The Main Specifications......................2 Chapter 2 Working Environment and Facility Requirements............3...

  • Page 3: Chapter 1 Dw-Ty-9900 Inductively Coupled Plasma Atomic Emission Spectrometer (Icp-Aes) Overview

    1.3 Application As a large precision inorganic analytical instrument, DW-TY-9900 ICP Spectrometer is widely used 1. Steel and its alloys include carbon steel, cast iron, alloy steel, high purity steel, ferroalloy, etc.

  • Page 4: The Main Features

    channel. Atomic is ionized by energy of outsiders, but the atoms are in unstable state, and from the high-level transition to the ground state, atoms will release tremendous energy, this energy is a certain wavelength of electromagnetic radiation and is sent out. Different elements have different spectral characteristics.

  • Page 5: Chapter 2 Working Environment And Facility Requirements

    Chapter 2 Working Environment and Facility Requirements 2.1 Working Environment 2.1.1 Room The effective space of the room is about 12-15 square meters, which is suitable for keeping the temperature. There are reagent cabinets with standard liquid, reagent racks, computer tables and chairs, etc., and 1-2 air conditioners are installed.

  • Page 6: Power Supply And Auxiliary Material Configuration

    Therefore, the quality of the power supply must be guaranteed. 2.2.2 Power Requirements DW-TY-9900 ICP-AES needs AC single-phase 220V/50Hz power supply. If the voltage fluctuation is greater than ±1V, it needs to be equipped with 10KVA precision purification AC regulated power supply(output accuracy ≤...

  • Page 7: Grounding Requirements

    ф110PVC elbow tee, with an axial fan to lead the exhaust gas to the outdoors. 2.3 Other Requirements for Laboratory A) DW-TY-9900 ICP-AES is floor-mounted and mobile and comes with its own operating table. The user only needs to prepare reagent racks and cabinets for spiked liquids and reagents and a computer table.

  • Page 8: Chapter 3 Installation

    The power supply to the DW-TY-9900 ICP-AES room should first be connected to a 60A circuit breaker, and then respectively connected t0 32A, 20A circuit breakers, and 10A circuit breakers to supply...
  • Page 9 Exhaust ducts: When using DW-TY-9900 ICP-AES for analysis and testing, the exhaust gas is mainly argon, but there are also some metal vapors and various gaseous substances generated.
  • Page 10 Fig. 3-3 Schematic diagram of installation of exhaust equipment Exhaust volume: the size of the exhaust air volume, it is advisable to stick a piece of paper on the air outlet, which can be gently sucked. If the exhaust air volume is too large, it will affect the flame stability, and if it is too small, it will not be able to exhaust air.

  • Page 11: Acceptance

    3.3 Acceptance According to the above requirements and regulations, after the installation of the instrument is completed, the acceptance of the instrument can be carried out. Before acceptance, Trainees should carefully read the operating instructions, understand the functions of the various knobs of the instrument, and be familiar with the operating methods and steps of the instrument, and then start powering on the instrument.

  • Page 12: The Packing List

    3.4 The Packing List Item Quantity Specification 主机 ICP-AES (DW-TY-9900) 1 Pc Host 计算机 1 Set Computer 打印机 1 Pc Printer 石英炬管 2 Pcs Quartz torch 高效雾化器 2 Pcs High efficiency atomizer 雾室 2 Pcs Fog chamber 雾室盖 1 Pc...
  • Page 13 公牛双排 6 孔 插线板 1 Pc Patch panel 串口电缆 自产 1 Pc Serial cable 电源线 主机内控制板 1 Pc Power cable Host control board 电子管水套密封圈 防腐, 防油 2 Pcs Electronic tube water jacket sealing Anti-corrosion and oil-proof ring 精密减压阀 2 Sets Precision pressure reducing valve 精密减压阀气管接头...

  • Page 14: Chapter 4 Operation

    4.1.1 Boot Operation DW-TY-9900 ICP-AES Follow the Steps Below 1. Boot: the first open cycle cooling water tank and water pump power switch, (ICP pressure...

  • Page 15: Software Function And Operation Interface

    background intensity) → Finished when the maximum value. 4.2 Software Function and Operation Interface The software uses two types of input devices, keyboard and mouse, respectively. Output device use both screen and printer, which is used to prompt analysts to the next step and how to run the process in the data, graphics, status, and display and printing.
  • Page 16 In the new method, enter the method name. The following window appears determined→...
  • Page 17 OK displays the following window...
  • Page 18 In the method, as shown by adding lines→ upper right corner of input elements to be analyzed to select the elements of the spectral lines → Double Click → → closed or out of the first floor window into the next window → In the window are the default subject →...
  • Page 19 attenuation measurement standards → measure the sample. Selection Method...
  • Page 20 Double-click or select the following points to determine Measurement → automatic searching for peak (peak with the preparation of standard solution actively look for a good looking peak)
  • Page 21 Automatic peak search...
  • Page 22 → automatic attenuation measurement in the analysis(using standard solutions prepared from standard to high attenuation)as shown below (The first method requires the establishment of the future does not need automatic attenuation)
  • Page 23 Measurement standards in the analysis and measurement of the sample (analysis sample) (to select multiple windows). Testing standards...
  • Page 25 After you finish testing the standard point of exit to save. Test sample...
  • Page 26 Historical database free to choose to print to analyze data (hold down the Ctrl key, point to print the number).
  • Page 27 Test results and historical data...
  • Page 28 At the same time the software developed for the professional spectrum analysis capabilities, even the most professional personnel must be based on the function of a good analysis. The function - Analysis of Measurement - Spectrum ray trace - Professionals can make the sample case - tracing the edit icon in the View →...

  • Page 29: Chapter 5 Daily Maintenance And Precautions

    Chapter 5 Daily Maintenance and Precautions 5.1 Daily Maintenance 1. Ambient temperature: The normal working environment temperature requirement of ICP spectrometer (25℃±3℃) (temperature change rate within 2℃/h). 2. Relative humidity: the relative humidity should be below 70% for storage and normal operation.

  • Page 30: Precautions For Turn On/Off

    and the inlet of the water tank is connected to the outlet of the instrument). After changing the water tank, pay attention to exhaust the air in the water pump and pipeline, otherwise the water in the water tank may not circulate due to the air when the water pump is turned on. 11.

  • Page 31: Precautions For Daily Maintenance

    the joint should be replaced when there are impurities such as metal oxides at the water pipe joint. 5.3 Precautions for Daily Maintenance 1. To replace the parts installed on the working coil( such as the torch), the high-voltage power supply must be turned off(or the ICP power supply).

  • Page 32: Chapter 6 Common Fault Diagnosis Analysis And Elimination

    Chapter 6 Common Fault Diagnosis Analysis and Elimination Failure Phenomenon Cause Analysis Elimination Method Power box 2A, 5A fuse blown Replace the fuse Turn on the water The cooling water tank pump is not turned on Turn on the power pump and check if switch, the indicator the water pressure...
  • Page 33 damaged, or the connection is faulty manufacturer for maintenance There is anode Whether the tube is damaged( It can be used to measure the insulation resistance between the If damaged, contact current but no grid poles with a 2500V megohmmeter, and the the manufacturer current resistance between any two poles is ≥20MΩ...
  • Page 34 manufacturer for maintenance. The method of replacing tube:unplug the water pipe connecting the ICP and the water tank→Open the ICP back shell→Open the high-frequency box and gradually remove the parts connected to the tube→After changing the tube, install it again→Reconnect the boiling water pipe (note the water in and out)→Check if it leaks→Boot test...

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