Millipore ICW-3000 User Manual
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Millipore ICW-3000 User Manual

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Summary of Contents for Millipore ICW-3000

  • Page 1 User Manual ICW-3000 System...
  • Page 2 This manual is believed to be complete and accurate at the time of publication. In no event shall Millipore Corporation be liable for incidental or consequential damages in connection with or arising from the use of this manual.
  • Page 3 In the event of a breach of the foregoing warranty, Millipore’s sole obligation shall be to repair or replace, at its option, the applicable product or part thereof, provided the customer notifies Millipore promptly of any such breach.

  • Page 4: Table Of Contents

    AFETY NFORMATION ....................... 2 ONTACTING ILLIPORE Internet ..............................2 Manufacturing Site........................... 2 ........... 3 HAPTER RODUCT NFORMATION ICW-3000 S ..................... 3 YSTEM VERVIEW ICW-3000 S ............... 3 YSTEM RODUCT ATER PECIFICATIONS Water Flow rate Specification ......................... 3 Product Water Quality..........................3 ....................
  • Page 5 OW TO ESISTIVITY OR ONDUCTIVITY NITS With Temperature Compensated or non Temperature Compensated values........18 4-14 (C02)................20 OW TO ET THE ESISTIVITY ETPOINT ICW-3000 S ....... 21 HAPTER SING THE YSTEM ....................21 NDERSTANDING THE ISPLAY ............21 ISTRIBUTION HROMATOGRAPHY...
  • Page 6 How to View the Remaining Days on the UV Lamp Timer ..............37 How to Reset the UV Lamp Timer ......................38 ..........39 HAPTER ROUBLESHOOTING ........41 HAPTER RDERING NFORMATION ICW-3000 S ............... 41 ATALOGUE UMBERS FOR YSTEMS ................41 ATALOGUE UMBERS FOR ONSUMABLES...

  • Page 7: Chapter 1 Introduction

    AFETY NFORMATION Your ICW-3000 System should be operated according to the instructions in this manual. In particular, the hydraulic and electrical specifications should be followed and met. It is important to use this equipment as specified in this manual; using this equipment in a different manner may impair the safety precautions of the ICW-3000 System.

  • Page 8: Contacting Millipore

    NTRODUCTION ONTACTING ILLIPORE NTERNET The Millipore Internet Site can be used to find addresses, telephone/fax numbers and other information. Internet Site Address: www.millipore.com www.millipore.com/techservice ANUFACTURING Millipore SAS 67120 Molsheim FRANCE - 2 -...

  • Page 9: Chapter 2 Product Information

    YSTEM VERVIEW The ICW-3000 Water Purification System is designed to be connected to 1 or 2 ion chromatography systems (combined to an eluent generator). The ICW-3000 System distributes water to the ion chromatography system on both suppressor and eluent generator inlets.

  • Page 10: Chematic Of Ain Omponents

    SimpliPak Cartridge PERATING PRINCIPLE The ICW-3000 Water Purification System is fed with pretreated water (Elix system, distilled water) through its external tank. When Product Water is being distributed/dispensed, the Distribution Pump turns on. The feedwater (pretreated) water is then pumped into the UV Lamp. The UV Lamp emits radiation at 185 nm and 254 nm.

  • Page 11: Technical

    12.5 kg OISE EVEL An ICW-3000 System has a maximum noise level of 36 dB at a distance of 1 metre. LECTRICAL 100 VAC  10%, 50/60 Hz. 0.68 amp source, 2 amp T (Time Lag) fuse, Power = 100 VA 120 VAC ...

  • Page 12: Chapter Pre Installation

    Altitude < 3000 metres Installation Category Pollution Degree *Note: Product water quality specifications may not be met if the ICW-3000 System is fed with DI water, and it could shorten the lifetime of your consumables.  W ICW-3000 S ’...

  • Page 13: Chapter 4 Installation

    NSTALLATION Chapter 4 NSTALLATION REPARATION OF THE YSTEM  Open the front cover. Locate the tie wrap used to hold the Booster Pump in place during shipping (A).  Press on the tab of the tie wrap (B). Remove and pull the tie wrap out. ...

  • Page 14: Connecting And

    ONNECTING AND ILLING THE  Rotate the ICW-3000 System so you can see the back of the system.  Locate the 2 tubing exiting from the bottom of the system (A). Remove tie-wraps and connect a male CPC connector to the end of each tubing (there are 2 different sizes of tubing and connector).

  • Page 15: Connection Examples

    XAMPLES 4 different examples of connection are shown below: THE 4 DIAGRAMS SHOWN BELOW ARE PROVIDED ONLY AS EXAMPLES. MILLIPORE SHALL NOT BE RESPONSIBLE FOR CONSEQUENTIAL, INCIDENTAL, SPECIAL OR ANY OTHER INDIRECT DAMAGES RESULTING FROM THE CONNECTION OF THE ICW-3000 SYSTEM TO ANY NON-MILLIPORE EQUIPMENT.
  • Page 16 From eluent line on the back of ICW-3000 ICW-3000 Suppressor Pure water tank Regen IN 6 mm tubing, 8 mm tubing 1/8” Teflon tubing From suppressor line on the back of Flow regulator valve ICW-3000 Supply from ICW-3000 to two Dionex ICS-2000 units - 10 -...

  • Page 17: Installation Of Air Vent Filter

    ON/OFF switch. A 0-5VDC signal will transit through the cable. MILLIPORE SHALL NOT BE RESPONSIBLE CONSEQUENTIAL, INCIDENTAL, SPECIAL OTHER INDIRECT DAMAGES RESULTING FROM THE CONNECTION OF THE ICW-3000 SYSTEM TO ANY NON-MILLIPORE EQUIPMENT. - 11 -...

  • Page 18: Connection Of The Power Cord  Turning On The System Power

    NSTALLATION  T ONNECTION OF THE OWER URNING ON THE YSTEM OWER  Open the front cover of the system (A). This will allow the system to go into STANDBY mode once the system is powered.  Plug the Power Cord into the system (B). ...

  • Page 19: Installation Of The

    NSTALLATION NSTALLATION OF THE IMPLI ARTRIDGE Do not touch the UV Lamp when installing the SimpliPak HAZARD Cartridge. NSTALLATION  Make sure front cover opened. STANDBY should be viewed on the Display (A).  Remove the SimpliPak Cartridge from its shipping box.
  • Page 20 NSTALLATION  Install the SimpliPak Cartridge until it is fully seated into the system ports as shown (B, C and  CLOSE THE FRONT COVER. - 14 -...

  • Page 21: Installation Of The Tygon ® Tubing

    NSTALLATION ® T NSTALLATION OF THE YGON UBING  Locate the clear Tygon Tubing and the Barbed Fitting in the Accessories Bag.  Screw the Barbed Fitting onto the bottom end of the POU Dispenser (A). Do not use any white tape on the threads of the Barbed Fitting.

  • Page 22: Purging Air From The System

    NSTALLATION 4-10 URGING IR FROM THE YSTEM  At this time you should have installed the SimpliPak Cartridge, Barbed Fitting and the Tygon Tubing. Air trapped in the SimpliPak Cartridge should now be purged from the system.  Press the Main Button to put the system into DISPENSING mode (A).
  • Page 23 NSTALLATION 4-12 NSTALLATION AND INSING OF THE INAL ILTER  Obtain a Final Filter for example Millipak® Express 20 Filter.  Remove the Tygon Tubing and the Barbed Fitting from the POU Dispenser.  Screw the Final Filter onto the end of the POU Dispenser. The Final Filter should be turned until it is hand tight (A).

  • Page 24: How To Show Resistivity Or Conductivity Units (C01)

    NSTALLATION 4-13 (C01) OW TO ESISTIVITY OR ONDUCTIVITY NITS EMPERATURE OMPENSATED OR NON EMPERATURE OMPENSATED VALUES Temperature compensation is a way of ‘standardizing’ Resistivity or Conductivity to measurements that would be seen if the water temperature was 25 C. The Compensation Mode is enabled by default.
  • Page 25 NSTALLATION Press the “+” or “-“ Button to select Non Temperature Compensated Conductivity Units: S/cm. To exit the menu, press and hold the Main Button for 2 seconds. To display the next menu option, press the Main Button once. - 19 -...

  • Page 26: How To Set The Resistivity Setpoint (C02)

    The Resistivity Setpoint is used to inform you when the Product resistivity is low. When the resistivity is below the setpoint, the Resistivity display flashes and the red Pack Alarm is blinking (see Section 5-6 How to Understand ICW-3000 System Messages). The factory default resistivity value is set to 15 M.cm @25 C.

  • Page 27: Chapter 5 Using The Icw-3000 System

    UV lamp ISTRIBUTION HROMATOGRAPHY YSTEM When the Ion Chromatography System requests water, The product resistivity and temperature displays the ICW-3000 system starts the distribution mode. flash during distribution chromatography system. NOTE: During the DISTRIBUTION mode, no water can be dispensed.

  • Page 28: System

    ICW-3000 S SING THE YSTEM ICW-3000 S OW TO ATER FROM THE YSTEM SING THE EYPAD To dispense water, press the Main Button: NOTE: To stop dispensing water, press the Main Button again. During distribution to the Ion Chromatography system, no water can be dispensed.

  • Page 29: Operating Modes

    ICW-3000 S SING THE YSTEM PERATING ODES TANDBY STANDBY mode is displayed when the front cover is removed. To depressurize the system, the Main Button has to be pressed down when STANDBY is blinking on the Display for 10 seconds. All system operations are disabled.

  • Page 30: Dispensing

    ICW-3000 S SING THE YSTEM ISPENSING During distribution to the ion chromatography system or dispensing, the icon shown to the right (A) is displayed and indicates the pump is working. The resistivity and temperature of the Product Water are displayed during distribution and dispensing. The resistivity and temperature remain displayed for a maximum of 10 seconds after dispensing.

  • Page 31: How To View The

    ICW-3000 S SING THE YSTEM OW TO VIEW THE RODUCT ESISTIVITY AND EMPERATURE The Display shows the last Product resistivity and temperature values Press: measured during distribution or during dispensing. The values are displayed for 5 seconds. NOTE: The Product resistivity and temperature are displayed automatically during distribution mode or during dispensing.

  • Page 32: How To Understand Icw-3000 System Messages

    When the red Pack Alarm is displayed as a steady icon, the SimpliPak Cartridge is not installed correctly or not installed at all. If the SimpliPak Cartridge has been reinstalled and the Alarm is still displayed, then contact Millipore. UV L LARM The system will prompt you to change the UV Lamp using a red UV Lamp Alarm icon.

  • Page 33: Chapter 6 Maintenance

    AINTENANCE Chapter 6 AINTENANCE AINTENANCE CHEDULE WHAT TO DO WHEN? HOW TO? When the Pack Alarm display is blinking. SimpliPak Cartridge See Section 6-2. Replacement When the system resistivity display is blinking. Inline Filter When the SimpliPak Cartridge is replaced or when the Replacement Product Water flow rate drops.

  • Page 34: How To Replace The Simpli Pak Cartridge

    AINTENANCE OW TO EPLACE THE IMPLI ARTRIDGE Do not touch the UV Lamp when replacing the SimpliPak HAZARD Cartridge. EMOVING THE IMPLI ARTRIDGE  Remove the front cover to go into STANDBY mode. Press the Main Button. Wait for the system to depressurize.

  • Page 35: Installing The New Simplipak Cartridge

    AINTENANCE NSTALLING THE NEW IMPLI ARTRIDGE  Remove the new SimpliPak Cartridge from its shipping box.  Remove the protective caps on the ports of the SimpliPak Cartridge.  Locate the O-rings on the ports. Wet them with water. It is preferable to wet them with ultrapure water.

  • Page 36: Purging Air From The System

    AINTENANCE  Install the Barbed Fitting and Tygon Tubing (G). See Section 4-9 Installation of the Tygon Tubing. URGING IR FROM THE YSTEM  See Section 4-10 Purging Air from the System. YDRATING THE YSTEM  Hydrate the system (H). See Section 4-11 Hydrating the System.

  • Page 37: Inline Filter Replacement

    AINTENANCE NLINE ILTER EPLACEMENT The inline filter is usually replaced with the SimpliPak Cartridge. If the flow rate becomes low due to clogging, replace the filter immediately. Make sure that the SimpliPak Cartridge has been hydrated Attention overnight. Do not touch the UV lamp when replacing the inline filter.
  • Page 38 Attach the new filter (F).  Secure the filter tubing with the clip.  Plug in the power cable and attach the front cover and final filter.  Start up the ICW-3000 System from the ion chromatography system side - 32 -...

  • Page 39: How To Replace The Final Filter

    AINTENANCE OW TO EPLACE THE INAL ILTER The Final Filter is normally replaced when the SimpliPak Cartridge is replaced or at an earlier time if it becomes clogged. A clogged Final Filter can reduce the Product Water flow rate. Make sure the SimpliPak Cartridge has been hydrated overnight.

  • Page 40: Eplace The Uv Lamp

    AINTENANCE UV L OW TO EPLACE THE The red UV Lamp Alarm will be blinking on the Display when it is time to exchange the UV Lamp. The message is shown when the UV Timer has reached 0 days (see Section 6-6 How to View or Reset the UV Lamp Timer).

  • Page 41: Removing The Uv Lamp

    AINTENANCE UV L EMOVING THE   Detach the Velcro belt of the UV housing.  Pull the UV housing out so that the UV Lamp cable is accessible (D). NOTE: Use the gloves supplied with the UV replacement kit. ...

  • Page 42: Installing The New Uv Lamp

    AINTENANCE UV L NSTALLING THE NEW  Ensure that you use the gloves supplied with the UV replacement kit. Plug the electrical cable to the new UV Lamp (G).  Carefully insert the UV Lamp into the UV housing (H). ...

  • Page 43: How To View Or Reset The Uv Lamp Timer (C03)

    AINTENANCE UV L (C03) OW TO IEW OR ESET THE IMER The UV Lamp Timer should be reset only after the UV Lamp has been replaced (see Section 6-5 How to Replace the UV Lamp). The UV Lamp Timer displays the time left until the UV Lamp needs to be replaced. The Display will show the red UV Lamp Alarm icon blinking when the Timer reaches 0 days.

  • Page 44: How To Reset The Uv Lamp Timer

    AINTENANCE UV L OW TO ESET THE IMER Press the Main and “+“ Buttons together to enter the menu. The Display will show C01. Press the Main Button 3 times. The Display will show C03 and “0” days left on the UV Timer.
  • Page 45  Check the source of electrical The Display screen is blank. power. power.  Main Power Fuse is  Contact Millipore. blown.  The tank is empty.  Refill the tank with pretreated water  The tank is not installed correctly or not installed ...

  • Page 46: Chapter 7 Troubleshooting

     The UV Lamp is not  Power OFF the system and installed correctly or not reinstall the UV Lamp. installed at all.  If the red UV Lamp Alarm is still displayed, then contact Millipore. UV System only - 40 -...

  • Page 47: Ordering Information

    Every 16 months or when UV lamp (185 nm) SYN185UV1 replacement message is displayed Simultaneously with SimFilter inline kit HFBCTAFS SimpliPak Cartridge MilliPak Express 20 final Filter Flow rate drop MPGP02001 Needle Valve ICW-3000 FTPF11415 Tank ICW-3000 TANKICW3000 - 41 -...

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