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OPERATING
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MAI NTENANCE
MANUAL
2nd Edition
CAT. No.ZD60115UV
S/N: F5DM96183R
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MILL!
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Table of Contents
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Summary of Contents for Millipore Milli-Q UV Plus

  • Page 1 - --- --- __ ,_,-- __ ___ ---·�---------- OPERATING · AN D MAI NTENANCE MANUAL 2nd Edition CAT. No.ZD60115UV S/N: F5DM96183R ,_\./ PORE MILL!
  • Page 2 OPERATI NG · MAINTENANCE MANUAL 2nd Edition MILLIPORE...
  • Page 3 Trademarks Millipore is a registered trademark of Millipore Corporation. Milli-Q, QPAK, Millipak, and Organex-Q are trademarks of Millipore Corporation. Delrin and Teflon are trademarks of El. duPont de Nemours and Co., Inc. Iwaki is a trademark of Iwaki Nary! is a trademark of General Electric.
  • Page 4: How To Use This Manual

    Milli-Q Plus system. Chapter includes technical Technical Information - service and ordering information, system specifications, and the Millipore warranty. Appendix 1 Advanced Maintenance and Troubleshooting describes how to adjust and Functions - troubleshoot the Milli-Q Plus system PC board.
  • Page 5 Make sure adequate feedwater exists to supply the system during Plus system. operation. If you do not have a Millipore installation contract with your Keep water at 30°( or lower local service representative, contact Millipore to review the installation and start-up procedures with a Millipore water If water temperature reaches higher than 30°C, the Milli-Q...
  • Page 6: Table Of Contents

    Installation Technical Assistance Preinstallation Requirements Ordering Information Electrical Feed Water Specifications Setting Up Your New Milli-Q UV Plus System Warranty Connect Polisher Cartridge Tubing Appendix Cut and Connect Feed Water Tubing Advanced Maintenance and Troubleshooting Install the QPAK Purification Pack...
  • Page 7 purification pack Point of use Milli pak final filter PRODUCTION/RECIRCULATION valve Control panel Purification pack retaining Lighted indicators LCD display Control panel push buttons Wet port Wall mounting hole plug Handwheel (Cover Release) Remote control jack A-c power input System fuse holder A-c power switch Top door...
  • Page 8 ABBREVIATIONS USED IN THIS MANUAL • Abbreviation Definition Abbreviation Definition L/min Uters per minute Alternating Current milliliters Ohm (electrical resistance) parts per billion Volt (electrical potential) colony forming unit Ampere (electrical Reverse Osmosis current) De-ionized Watt (electrical power) Total Organic Carbon foot (measurement) micron inch...
  • Page 10: Chapter 1: Introduction

    (RO), distillation, contamination. or deionization (DD. Superior Total Organic carbon (TOC) removal makes the Milli-Q UV Plus system ideal for low TOC (nm) By generating 185 nanometers and 254 light, the •...
  • Page 11: How The System Works

    The recirculation frequency When power is restored, the unit will restart in the correct can be changed to every 3 hours by Millipore service personnel. mode. The contrast of the LCD display can be adjusted by Each time you switch the Milli-Q Plus system from STANDBY Millipore service personnel.
  • Page 12: Recirculation/Production

    REMOTE STANDBY until water is needed (as in regular Resistivity sensor standby, water automatically recirculates for 5 minutes every 55 RECIRCULATION/PRODUCTION valve minutes). When the remote unlt calls for Milli-Q UV Plus system Water to production water, the system automatically switches to OPERATE. Water through recirculation loop...
  • Page 13 4 I N T R 0 CT I 0 N...
  • Page 14: Chapter 2: Installation

    Preinstallation Requirements To ensure adequate feed pressure, yourMilli-Q UVP!us system must be installed: Before you install your new Milli-Q UV Plus system, electrical within 3 m (9.8 ft) of your feedwater system • and feedwater systems must meet the following requirements.
  • Page 15: Setting Up Your New Milli-Q Uv Plus System

    If you want to mount your system on the wall, order Connect the 1/2 in. male to 1/4 in. female reducing the optional wall mounting bracket from Millipore. See CHAPTER bushing (B) to the 1/2 in. female threaded fitting.
  • Page 16 ,_ ----------------------------------' Box 2 From the Starter Kit (second box): Note: To register your Milli-Q UV Plus system and become QPAK purification pack eligible for discounts, special promotions, and a free 0.22 IJ. m Millipak 40 final filter subscription to Millipore News, you must fillout and return the information card that came with your Milli­...
  • Page 17: Connect Polisher Cartridge Tubing

    • CONNECT POLISHER CARTRIDGE TUBING Plug Open the back cover: Collar turn the handwheel on the cover counterclockwise • (to your left, the lock and unlock directions are Polisher marked on the back of the cabinet). cartridge inlet set the handwheel and washer aside •...
  • Page 18: Cut And Connect Feedwater Tubing

    4. Take the remaining loose end of tubing coming from the (resistivity sensor inlet) connection behind the CAUTION: The Milli-Q UV Plus system pump is "self· cartridge and remove the cap. Insert this end into the priming"- it automat ically draws water into polisher cartridge (outlet) connector at the bottom of itself when it starts.
  • Page 19 Plug 8 mm feed- water tubing· IllEr PilOil!XT D1W1 If you use a Millipore feed tank, you can connect Note: tubing to the 8 tank connector . If your feed source (for example, a DI line) terminates with a 1/2 in. male threaded fining, you must first connect the 1/2 in.
  • Page 20: Install The Qpak Purification Pack

    0 /?i::! K Pack-retaining arm Remove the protective plugs from the t.v.ro pack receiving ports on the front of the Milli-Q UV Plus system. Protective caps Protective plugs IN S T A L L A T I O N...
  • Page 21 Hold the Milli-Q UV Plus system with one check for water leaks at the internal tubing connections with a-c power hand while you guide the pack into place with your other hand.
  • Page 22: Clear Trapped Air

    CLEAR TRAPPED AIR • If you installed an iso lating valve, open it . The QPAK purification pack and the polisher cartridge contain Press the bottom half of the a-c power switch to make carbon fines which must removed bef ore installing the sure the power is off.
  • Page 23 Turn on the power by pressing the top half of the a-c Press OPERATE/STANDBY to put the system into the OPERATE mode.and to start the pump. power switch at the rear of the system. The dis play will read RECIRCUlATION minutes, then STANDBY.
  • Page 24 If water leaks from a tubing connection WARNING: turn off system a-c power and remove Note: before, the system will run through the Auto Test the a-c power connection from the sequence; the display will read TEST: 15 M.Q em(± 1 unit.
  • Page 25: Install The Millipak 40 Final Filter

    • INSTALL THE MILLIPAK FINAL FILTER Note: before, the system will run through the Auto Test sequence; the display will read TEST, 15 MQ em(± 1 Wrap the thread on the Millipak final filter two or megohm-em), and will then show the actual resistivity three times with Teflon tape to seal the thread.
  • Page 26 Snap the Mi llipak 40 final filter into the center of the poin t-of-use cover . Millipak 40 final (point· Tabs of-use) filter Slot Point-of-use cover You are now r eady to operate your Milli-Q UV Plus system. I N S T A L L A T I O N...
  • Page 27 I N ST A l l A T I ON...
  • Page 28: Chapter 3: Operation

    Make sure you have done the following before you operate the Milli-Q UV Plus system: directly from the unit and by remote control. This chapter describes direct operation of the Milli-Q UV Plus system. For polisher cartridge tubing connected instructions on how to operate the system by remote control, feed water connection made see APPENDIX 2.
  • Page 29: Drain The First Ten Liters Of Water

    DRAIN THE FIRST TEN LITERS OF WATER • The fi r st time you use your Milli-Q UV Plus system, discard the first ten liters of water. If you turn off the Milli-Q UV Plus system for any length of time, you should again drain the first ten liters before collecting water for laboratory use.
  • Page 30: Collect Water For Laboratory Use

    • COLLECT WATER FOR LABORATORY USE CAUTION: Do not allow water to recirculate continuously for more than hours, the water temperature Turn o n the pump b y pressing OPERATE/STANDBY. may reach or exceed 30'C (86'F). If the TEST: 14.5 M n em The display will normally read water temperature does reach or exceed Product: 18.2 M Q em.
  • Page 31: Summary Of Milli-Q Uv Plus System Functions

    You can have the setting for recirculation frequency changed so that the water recirculates for 5 minutes every 3 hours (see APPENDIX I). This should be done by a trained Millipore service representative. Summary Milli-Q UV Plus System Functions The chart below summarizes the system functions. It also lists the messages that will be shown when a Milli-Q Plus system component needs to be replaced.
  • Page 32 UV lamp assembly needs to be replaced [either model UV light indicator not 'on' Several Milli-Q UV Plus system components are expendable: Component Lifetime Millipak 40 fmal filter variable 4 to 6 months...
  • Page 33: Chapter 4: Maintenance

    CHAPTER 4, MAINTENANCE, provides instructions for replacing exhausted components. If you encounter problems wirh your Milli-Q UV Plus system see CHAPTER 5, TROUBLESHOOTING, to help you diagnose and solve problems in the system. You can also contact Milli p ore Technical Service for assistance;...
  • Page 34: System Shutdown

    M A I NT E N A N C E System Shutdown (NOT SHOWN) your Milli-Q Plus system will not be used for more than one week, remove the expendable components: Turn the RECIRCULATION/PRODUCTION valve RECIRCULATION. Turn off the a-c power switch at the back of the Milli-Q Plus system.
  • Page 35: Changing The Qpak Purification Pack And The Polisher Cartridge

    If product resistivity readings decrease to an unacceptable level When you wish to operate your Milli-Q UV Plus system again: (below 10 megohm-em), replace the purification pack. To Install a new polisher cartridge (B) by performing the order a new QPAK purification pack, see CHAPTER 6.
  • Page 36 CAUTION: If the amber EXCHANGE PACK lamp is lit continuously, theQPAKpurification pack might be loose. Make sure the purification pack is securely in place and the pack retaining arm is locked. Replace the polisher cartridge. � If you are going to change the Q P AK, go to the next Note: paragraph (CHANGING THE POLISHER...
  • Page 37: Changing The Polisher Cartridge

    CHANGING THE POLISHER CARTRIDGE The average life of the polisher pack is 4 to 6 months. Therefore, it is usually replaced when th � QPAK purification pack is changed. The polisher cartridge (B) should be replaced at the end of the day to allow the activated carbon to hydrate overnight.
  • Page 38 Once a tube is fi rmly secured, avoid removing and reinstalling it You are now ready to operate your Milli-Q UV Plus system frequently. again. MA I N T E N AN C E...
  • Page 39: Changing The Uv Lamp Assembly

    Changing The UV Lamp Assembly WARNING: Do not perform these procedures with a-c power applied to your system. You must not look directly at the UV lamp when the system's power is on (the UV light indicator on the control keypad will be lit when the UV lamp is on and a purple ring will be visible through the top of the stainless steel...
  • Page 40: Install A New Uv Lamp

    INSTALL A NEW UV LAMP Always remove the Millipak 40 final filter before Note: you flush the system to drain. Replace it after the CAUTION: Wear gloves when handling the UV lamp flushing operation is complete. assembly to prevent contamination of the lamp. Discard the first ten liters of water that is produced.
  • Page 41: Changing The Millipak 40 Final Filter

    Follow the instructions in CHAPTER 2, INSTAL­ lATION to install and vent the new Millipak 40 fi n al filter. You are now ready to operate your Milli-Q UV Plus system again. Millipak 40 final filter Point-of-use cover Point-of-use connector...
  • Page 42: Replacing The Fuse

    • Fuse holder If these conditions are met, replace the fuse as f ollows: Turn off t he Milli-Q UV Plus system. Unplug theunlt from the a-c poweroutlet and disconnect t he power co rd from the unit . WARNING:...
  • Page 43 If the power lamp still is not lit, save both fuses. You may need to replace the fuse on the PC board. See APPENDIX 1, or contact Millipore Technical Service for assistance. M A I N T E N A N C E...
  • Page 44: Chapter 5: Troubleshooting

    T R O U B L E S H O O T I N G The chart below will help you diagnose and solve problems that you might encounter with the Milli-Q UV Plus system. If you are unsure what the problem is or how to approach solving a problem, contact Millipore Technical Service for assistance.
  • Page 45 Water at bottom of pack QPAK purification pack not secured make sure QP purification pack retaining arm is locked in place purification pack microswitch not working contact Millipore Technical Service, CHAPTER 6 leak at RECIRCULATION/PRODUCTION contact Millipore Technical Service, CHAPI'ER 6 valve...
  • Page 46: Chapter 6: Technical Information

    Millipore, S.A. Comercio Ltda. PB 307 For technical assistance with your Millipore product, contact Rua Prof. Campos de 78054 Saint-Quentin­ your local Millipore sales or service representative, or telephone Oliveira, 430 Yvelines Cedex the Millipore office nearest you. CEP 04675 France In North America, you can telephone the Technical Service Tel.
  • Page 47 Telex 56556 MILLIP England Telex 24948 Tel. (0923) 81 6375 Spain Telex 24191 milpor g Mexico Millipore Iberica, S.A. Millipore S.A. de C.V. A venida del Llano West Germany A venlda Ingenieros Castellano, 13-3 Millipore GmbH Militares 85-PB 28034 Madrid Hau ptstrasse 87 Mexico 11230 D.F.
  • Page 48: Ordering Information

    Ordering Information Description Catalogue Number MILLI-Q PLUS SYSTEM Milli-Q UV Plus system, 115V, 60Hz SLIP 191 M1/ZD6o 115 UV '>< MPGL 04S K2 EXPENDABLES Millipak final (point-of-use) filter unit, 0.22 fJ.m sterile w/1/4 in. NPTM inlet, 2/package �CDEX POL UV...
  • Page 49 Description Catalogue Number SPARE PARTS (Continued) LCD display, 16 digits with cable ZFZO 000 30 Main power fuse, 2A, 250V, 5 20 mm FTPF 002 78 Slo-Blo (for 115V, 60Hz) Pack adapter with thread, 1/4 in. ZFZO 000 09 Pack microswitch with cable ZF20 000 20 PC board fuse, 0.16A FTPF 030 00...
  • Page 50: Specifications

    Catalogue Number Description UV ASSEMBLY SPARE PARTS tube ITPF 027 13 stem, 90 ° elbow . ITPF039 65 Stainless steel housing Ballast, 120V, 60Hz ITPF 039 Stainless steel washer ITPF 039 67 O ring ITPF 039 Housing nipple ITPF 039 69 Key board sticker ITPF 029 94 UV Tube Detail...
  • Page 51 Specifications (Continued) Materials of Construction Components Quartz tube quartz Resistivity sensor 316 stainless steel, electropolished Tubing polyamide UV housing stainless steel Washer stainless steel 3-way valve PVDF Connections Specifications Feed connector polyamide tubing, 8 mm O .D. Product connector 1/4 in. NPTF connector, PVDF Dimensions Specifications (19.5 in.)
  • Page 52 Specifications (Continued} Pump and Motor Specifications Bypass adjustment maximum pressure 0.67 bar (10 psi) to 2.67 ± 0.13 bar (40 ± 2 psi) Electrical 115V, 60Hz, 1A Maximum discharge pressure 2.67 bar ( 40 psi) Type positive displacement, magnetic gear pump System Performance Specifications Product quality"...
  • Page 53: Warranty

    Millipore promptly of any such defect. The exclusive remedy provided herein shall not be deemed to have failed of its essential purpose so long as Millipore is willing to repair or replace any nonconforming Millipore product or part. Millipore shall not be...
  • Page 54: Appendix

    • encounter problems with the PC board. Repairs changing the recirculation frequency setting • performed on the PC board by non-Millipore personnel will void the warranty for your M illi­ CAUTION: Be careful when working on the PC board. The Q UV Plus system.
  • Page 55: To Reassemble The Milli-Q Uv Plus System

    UV lamp is on. Also, a purple ring will be visible Connect the Milli-Q UV Plus system to the a-c power through the top of the stainless steel outlet.
  • Page 56: Changing The Fuse On The Pc Board

    The PC board includes the fuse and the LCD (Liquid Crystal Display) contrast, the temperature, and the resistivity potentiometer s. The PC board also includes a jumper duster used for changing the system temperature range, the time setting for the purification pack, and the calibration frequency setting for automatic recirculation.
  • Page 57 4. Assemble the system (see steps 2 through 6 in TO REASSEMBLE MILU-Q UV PLUS SYSTEM). the system power light does not go on, contact Millipore Technical Service for assistance. Open fuse New fuse A P P E N D I X...
  • Page 58: Adjusting The Temperature Potentiometer

    • ADJUSTING THE TEMPERATURE POTEN­ TIOMETER You may need to adjust the temperature circuitry potentiometer if the display reads TEST INCORRECT when the system auto tests. Before you adjust the temperature potentiometer, make sure the feed water temperature is between 5 °C and 40°C. If the water temperature is not in this range, correct the feedwater temperature.
  • Page 59: Adjusting The Resistivity Potentiometer

    °C when the system autotests, the thermistor is damaged. the test resistivity is not 15 ± 1 megohm-em (display does • Contact Millipore Technical Service for assistance. TEST: 15 M Q em) not read Before calibrating the resistivity potentiometer, make sure the calibration temperature is 25°C (see the section above).
  • Page 60: Adjusting The Lcd Contrast Potentiometer

    6 in TO REASSEMBLE Note: The resistivity set point can be changed upon request. 3. Follow steps 1 through MILLI-Q UV PLUS SYSTEM to assemble the system. Contact Millipore Technical Service for assistance. A P P E N D I X...
  • Page 61: Changing The Frequency Setting For

    AUTOMATIC RECIRCULATION The frequency setting for the QPAK purification pack is To maintain water quality, the Milli-Q UV Plus system will normally set at 4 months for optimum removal of TOCs and automatically recirculate water for 5 minutes every 55 minutes microorganisms.
  • Page 62: Troubleshooting The Pc Board

    Troubleshooting The PC Board Problem Cause Solution Power lamp is off1 replace PC board fuse; contact Millipore Technical PC board fuse blown system fuse O.K. Service or see CHANG!NG THE FUSE ON BOARD this chapter Autotest reads temperature or resistivity calibrate temperature or resistivity;...
  • Page 63 54 A P P E N D I X...
  • Page 64: Appendix

    A P P E N D I X Operating the Milli-Q UV Plus System by Remote The REMOTE STANDBY option enables you to control the operation of your Milli-Q Plus system from a remote location (such as a clinical analyzer) using a compatible remote control unit.
  • Page 65 pen receiving the proper signal from your remote unit, the Milli-Q lN Plus system will automatically supply the water required. The Milli-Q lN Plus system will automatically switch Note: from OPERATE to STANDBY when the remote unit does not need water, the display will read REMOTE STANDBY.

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