Bruker BioSpin 500'154 USP User Manual
  1. Manuals
  2. Brands
  3. Bruker Manuals
  4. Laboratory Equipment
  5. BioSpin 500'154 USP
  6. User manual
Bruker BioSpin 500'154 USP User Manual

Bruker BioSpin 500'154 USP User Manual

Hide thumbs
Table of Contents

Advertisement

Quick Links

Download this manual
500´154 USP
User Manual
NMR Spectroscopy

Advertisement

Table of Contents
loading
Need help?

Need help?

Do you have a question about the BioSpin 500'154 USP and is the answer not in the manual?

Questions and answers

Subscribe to Our Youtube Channel

Related Manuals for Bruker BioSpin 500'154 USP

Summary of Contents for Bruker BioSpin 500'154 USP

  • Page 1 500´154 USP User Manual NMR Spectroscopy...
  • Page 2 Product names used are trademarks or registered trademarks of their respective holders. © September 2010, Bruker BioSpin AG Fällanden, Switzerland ZTKS0160 / Z31926 / Rev.: 00...
  • Page 3 Contact ......................9 Introduction....................11 Safety......................13 Transportation .....................29 Assembling ....................35 Operation......................37 Troubleshooting ..................39 Maintenance....................55 Disassembling .....................57 Appendix ......................59 ZTKS0160 / Z31926 / Rev.: 00...
  • Page 4 ZTKS0160 / Z31926 / Rev.: 00...

  • Page 5: Table Of Contents

    Contact ......................9 Introduction....................11 General Information....................11 1.1.1 Limitation of Liability ....................11 1.1.2 Customer Service....................11 1.1.3 Warranty......................... 11 1.1.4 Copyright ........................ 11 General View......................12 Safety......................13 Persons in charge ....................13 Customer Responsibilities..................14 Key Words......................15 Residual Risks......................16 2.4.1 Persons ........................
  • Page 6 Troubleshooting ..................39 Safety ........................39 Problem ........................40 6.2.1 During Transportation..................... 40 6.2.2 During Assembling ....................40 6.2.3 During Cool Down ....................42 6.2.4 During Energizing and Shimming ................46 6.2.5 During Operation of the Magnet Stand..............48 6.2.6 During Standard Operation..................50 6.2.7 During De-energizing and Warming up ..............
  • Page 7 ZTKS0160 / Z31926 / Rev.: 00...
  • Page 8  ZTKS0160 / Z31926 / Rev.: 00...

  • Page 9: Contact

    Contact Manufacturer: Bruker BioSpin AG Industriestrasse 26 CH-8117 Fällanden Schweiz Phone: +41-44-825-91-11 Fax: +41-44-825-96-96 http://www.bruker.com Please refer to the Model No., Serial No. and Internal Order No. in all correspondence regarding the NMR system or components thereof. ZTKS0160 / Z31926 / Rev.: 00...
  • Page 10 ZTKS0160 / Z31926 / Rev.: 00...

  • Page 11: Introduction

    • use of unauthorized spare parts or accessories. 1.1.2 Customer Service Technical support is provided by Bruker service via telephone or e-mail. For contact information see page 9 of this document. 1.1.3 Warranty The warranty terms can be found in the sales documents of the magnet system and in the Terms and Conditions of Bruker BioSpin AG.

  • Page 12: General View

    General View 1 RT vessel 2 High current lead turret 3 Current lead turret 4 Helium flow system 5 Helium fill-in turret with helium fill-in port 6 Nitrogen flow system 7 Nitrogen turrets 8 RT bore 9 Magnet stand Figure 1.1: General view Cryostat of the Magnet System The heart of the magnet system is a superconducting magnet located inside the helium vessel, which is filled with liquid helium.

  • Page 13: Safety

    The supplied cryostat of the magnet system was designed and manufactured according best available technical knowledge and practice, archived in over 50 years of experience of Bruker BioSpin AG. International standards for quality and approval recommended for cryostats of superconducting magnets were certified.

  • Page 14: Customer Responsibilities

    Customer Responsibilities The customer of the magnet system must obey the security advice and the rules for safety, accident prevention and environmental protection correctly for the magnet systems. Furthermore, the customer is responsible for keeping the magnet system in correct technical condition. In particular: •...

  • Page 15: Key Words

    Key Words DANGER Indicates a hazardous situation which, if not prevented, will result in death or serious injury. WARNING Indicates a hazardous situation which, if not prevented, could result in death or serious injury. CAUTION Indicates a hazardous situation which, if not prevented, may result in minor or moderate injury.

  • Page 16: Residual Risks

    Work must only be carried out by approved persons with applicable qualifications. The necessary qualifications are specified in the beginning of the relevant chapter. • In case of doubt, contact Bruker Service. Contact information see page 9 of this document. 2.4.2 Intended Use WARNING Risk of damage to life and limb by incorrect use of the magnet system.

  • Page 17: Safety Devices

    2.4.3 Safety Devices WARNING Risk of damage to life and limb due to not sufficient safety devices. Several safety devices ensure safe operation of the magnet system. They must always be in correct working condition. Thus: • Do not block safety devices. •...

  • Page 18: Signs And Labels

    Thus: • Maintain signs and labels in a readable state. • Replace damaged or not readable signs and labels immediately. New signs and labels can be obtained from Bruker Service. 2.4.6 Technical Risks Magnetic Field WARNING Risk of damage to life and limb due to high magnetic fields.
  • Page 19 Liquid and gaseous cryogenic agents are extremely cold. Contact with liquid or gaseous cryogenic agents will lead to cold burns. Thus: • Only use cryogenic agents in well ventilated rooms. In case of doubt ask Bruker Service. • Wear an oxygen monitor on the body during service and maintenance work.
  • Page 20 The evaporating helium will displace oxygen. In case of not sufficient ventilation this may result in death by suffocation. Thus • The magnet system site must be well ventilated. In case of doubt contact Bruker Service. • The evaporating gas may resemble smoke. Never pour water on the magnet system.
  • Page 21 Low Temperatures WARNING Risk of injury due to low temperatures of liquids and metal parts. Physical contact with extremely cold liquids and metal parts may cause serious inju- ries. Contact with the skin may cause cold burns. Contact with the eyes may cause blindness.
  • Page 22 Risk of Tilting WARNING Risk of injury due tilting of the magnet system. The magnet system is very sensitive to lateral forces. It may tilt. Thus: • Do not climb onto the magnet system. • Do not lean items against the magnet system. •...

  • Page 23: Cautions

    2.4.7 Cautions CAUTION Risk of injury and property damage due to incorrect transportation. The box may tilt, movement may get out of control. Thus persons may get injured and the cryostat or further equipment may be damaged. Thus: • Do not move arbitrarily. •...

  • Page 24: Personal Protective Equipment

    Personal Protective Equipment The personal protective equipment must be worn at any time while working on the magnet system and to avoid health hazards. Protective Goggles Used to protect the eyes from injury due to flying cold liquids and parts. Protective Gloves Used to protect the hands from injury caused by contact with extremely cold liquids or surfaces and for protection from injury caused by rough edges.

  • Page 25: Description Of Signs And Labels

    Description of Signs and Labels Signs and labels are always related to their immediately vicinity. The following signs and labels are found on the magnet system and in the vicinity. Prohibition sign: No person with pacemakers! People with pacemakers are endangered in the identified area of 0.5 mT (5 Gauss) and are not allowed to enter these areas.

  • Page 26: Safety Devices

    Safety Devices The cryostat of the supplied magnet system is equipped with the following safety devices: 1 Quench Valves 2 Bursting Disc 3 Safety Valve 4 Drop Off Plate Figure 2.1: Safety Devices of the Cryostat Quench Valve The quench valves (1) are the safety devices of the helium vessel. They open with a defined pressure.

  • Page 27: Behavior In Danger And Emergency Situations

    Behavior in Danger and Emergency Situations Preparations • Keep the emergency exits free at all times. • Prepare and maintain an up-to-date list of emergency telephone numbers in the magnet system area. In Case of Emergency • Leave the danger zone immediately. •...
  • Page 28 ZTKS0160 / Z31926 / Rev.: 00...

  • Page 29: Transportation

    Transportation The transportation is carried out by Bruker Service or approved persons. However, it may happen that other persons have to receive the delivery of the shipping boxes. In this case it is essential to obey the instructions in this chapter and to inform these persons before.

  • Page 30: Transport Inspection

    Contact Bruker Service before installation. The claim for damage expires after the fixed period Thus: Report damages to Bruker Service immediately after detection of damage. For contact information see page 9 of this document. ZTKS0160 / Z31926 / Rev.: 00...

  • Page 31: Transportation By Fork Lift / Pallet Jack

    Transportation by Fork Lift / Pallet Jack Recommended for transporting the boxes to the installation site. Persons in charge: Approved forklift / pallet jack operator Precondition: The fork lift / pallet jack must be approved for the transportation weight (see chapter Appendix, Technical Data). Transport Check the route of transport for the minimal height and width.

  • Page 32: Transportation With A Crane

    Transportation with a Crane Recommended for lifting the cryostat out of the box. Persons in charge: Approved crane operator Precondition: The crane must be approved for the transportation weight (see chapter Appendix, Technical Data). Attachment Points Exclusively use the marked eyelets (1) as attachment points for the lifting equipment.

  • Page 33: Storing

    Storing If it is necessary to store the cryostat and accessories before installation obey the follo- wing instructions: • Store the boxes in a closed, dry and dust-free room. • Store the boxes upright. • Do not tilt the boxes. •...
  • Page 34 ZTKS0160 / Z31926 / Rev.: 00...

  • Page 35: Assembling

    Assembling Safety Persons in charge: Bruker Service only ZTKS0160 / Z31926 / Rev.: 00...
  • Page 36 ZTKS0160 / Z31926 / Rev.: 00...

  • Page 37: Operation

    Operation Safety WARNING Gas under Pressure Cryogenic Agents Electricity Persons in charge: Bruker Service, approved persons of the customer ZTKS0160 / Z31926 / Rev.: 00...

  • Page 38: Set Into Operation

    5.1.1 Set into Operation Mount the further equipment of the supplied magnet system respecting their manuals. If the magnet system is equipped with a magnet stand with pneumatic insulators: Set the magnet stand into operation by switching the pneumatic controller to UP position (1).

  • Page 39: Troubleshooting

    Troubleshooting Troubleshooting must be performed only with approved qualification. In case of doubts or problems not specified in the following list contact Bruker Service immediately. For contact information see page 9 of this manual. Safety WARNING Magnetic Fields Gas under Pressure...

  • Page 40: Problem

    Ceiling height too Site does not meet Choose another site that low for assembling the required condi- meets the required condi- Bruker Service on magnet stand. tions. tions. Ceiling height too Site does not meet Insert the helium level sensor...
  • Page 41 For this work the bottom plate has to be removed. Check the suspension tubes of the helium vessel are not broken. Install the safety device for fall protection (not supplied). Contact Bruker Service Headquarter for further information.

  • Page 42: During Cool Down

    6.2.3 During Cool Down Indicator Possible reason Solution Precooling with Empty transport Refill or change transport liquid nitrogen conti- Bruker Service dewar. dewar. nue too slowly. Transfer pressure Increase transfer pressure Bruker Service too low. slightly. Transport dewar is leaky; no transfer...
  • Page 43 Do not remove pumping unit until liquid helium fill- in is finished. Vacuum is broken or RT vessel becomes • Continue as in problem Bruker Service cold and wet. less than 10 mbar. Vacuum in RT vessel does not reach mbar above Stop cool down.
  • Page 44 90 K. during pumping and Repeat pumping and Nitrogen ice in the flushing were too flushing and carefully Bruker Service helium vessel. long and remaining check with the dipstick to nitrogen was boiling be sure that the helium off and got frozen.
  • Page 45 Check the connection in the sensor is not con- sor can not be adju- helium fill-in turret between nected correctly with Bruker Service sted at the beginning helium level sensor and con- the connector in the of cooling down with nector.

  • Page 46: During Energizing And Shimming

    The current lead can The connector is warm helium gas. not be inserted covered with ice. To remove small ice spots use Bruker Service completely into the (frozen moisture or the dipstick or the precooling connector. nitrogen ice). tube as tubing for the warm helium gas.
  • Page 47 The connector is warm helium gas. To remove Shorting plug cannot covered with ice small ice spots use the dip- Bruker Service be removed. (frozen moisture or stick or the precooling tube as nitrogen ice). tubing for the warm helium gas.

  • Page 48: During Operation Of The Magnet Stand

    Repeat shimming. 6.2.5 During Operation of the Magnet Stand In case of doubt contact Bruker Service and refer to the supplied manual of the Magnet Stand Indicator Possible reason Solution The NMR spectrum...
  • Page 49 5 to 8 bar (70 to 112 psi). customer If the problem is still not Approved solved, contact Bruker persons of the Service. customer The magnet system Stop the pneumatic isolators. is not leveled cor-...

  • Page 50: During Standard Operation

    Watch helium boil off daily. sing. customer Contact Bruker Service The helium flow sys- Approved immediately! Do not try to tem is covered with persons of the remove ice of the helium flow ice.
  • Page 51 See chapter ”After a Approved Loss of quench” on page 6-53 Quench persons of the superconductivity. Contact Bruker Service customer immediately! Approved Cold spots within the Alignment not cor- Contact Bruker Service. persons of the RT bore.

  • Page 52: During De-Energizing And Warming Up

    The magnet system The helium level was Refill helium at least to the quenches during de- too low for de-ener- minimum allowed level (see Bruker Service energizing. gizing. Appendix Technical Data). The power supply is Replace power supply. Bruker Service defective.

  • Page 53: Troubleshooting Work

    Check the nitrogen turrets for icing. Start the refill with liquid helium as soon as possible after the quench (within one hour after the quench; refer to the supplied refill manual). Contact Bruker Service immediately. ZTKS0160 / Z31926 / Rev.: 00...
  • Page 54 If the quench occurs unattended or helium transfer was not possible within one hour after the quench, it is recommended to warm up the system to 90 K. ZTKS0160 / Z31926 / Rev.: 00...

  • Page 55: Maintenance

    Maintenance Maintenance must be performed only with approved qualification. In case of doubt contact Bruker Service. For contact information see page 9 of this document. Safety WARNING Magnetic Fields Gas under Pressure Cryogenic Agents Electricity Spontaneous Ignition and Explosion Persons in charge...

  • Page 56: Cleaning

    • Record the filling session. Deviation from estimated con- sumption may used for identifica- tion of troubles. In this case contact Bruker Service. • Check the nitrogen level. weekly Cryostat Approved persons of the customer •...

  • Page 57: Disassembling

    Disassembling Safety Persons in charge: Bruker Service only ZTKS0160 / Z31926 / Rev.: 00...
  • Page 58 ZTKS0160 / Z31926 / Rev.: 00...

  • Page 59: A Appendix

    Appendix Warning Signs Figures Tables Glossary / Abbreviations Technical Data Index ZTKS0160 / Z31926 / Rev.: 00...
  • Page 60 ZTKS0160 / Z31926 / Rev.: 00...

  • Page 61: Warning Signs

    Warning Signs Gefahr/Danger Art und Quelle der Gefahr Kind and Source of Danger................15 Warnung/Warning Art und Quelle der Gefahr Kind and Source of Danger......13, 15 Vorsicht/Caution Art und Quelle der Gefahr Kind and Source of Danger..............15 Information Hinweise, die dem Anwender die Arbeit erleichtern Information and links for touble-free handling and operation ......
  • Page 62 ZTKS0160 / Z31926 / Rev.: 00...

  • Page 63: Figures

    Figures Figure 1.1: General view Cryostat of the Magnet System........12 Figure 2.1: Safety Devices of the Cryostat............. 26 Figure 3.1: Packaging (without surrounding panels)..........29 Figure 3.2: Transportation by forklift ..............31 Figure 3.3: Attachment points for lifting equipment..........32 Figure 5.1: Start the Magnet Stand ................
  • Page 64 ZTKS0160 / Z31926 / Rev.: 00...

  • Page 65: Tables

    Tables Table 7.1: Maintenance Timetable............... 56 $Table A.1: Glossary....................67 Table A.2: Abbreviations ..................67 Table A.1: Weight Cryostat................... 69 Table A.2: Weight Magnet Stand................69 Table A.3: Dimensions of Transportation Box for the Cryostat ......69 Table A.4: Dimensions of Transportation Box for the Magnet Stand....69 Table A.5: Dimension Cryostat - Front View ............
  • Page 66 ZTKS0160 / Z31926 / Rev.: 00...

  • Page 67: Glossary / Abbreviations

    Glossary / Abbreviations Used term Description Any kind of package used to protect sensitive parts during transportation. Cryostat The collective of all parts providing a temperature of 4 K inside for the superconducting magnet. The cryostat also provides the safety devices and the access ports for the cryogenic agents and electricity.
  • Page 68 ZTKS0160 / Z31926 / Rev.: 00...

  • Page 69: Technical Data Ms 500'154 Usp

    Technical Data MS 500‘154 USP Technical Data MS 500‘154 USP A.5.1 Dimensions Weights Cryostat Value Unit Weight, empty, without magnet stand 1500 Weight, completely filled, without magnet stand 2000 Weight, empty, ready for transportation including box 2300 Table A.1: Weight Cryostat Magnet Stand Value Unit...
  • Page 70 Technical Data MS 500‘154 USP Dimensions Cryostat Front view Figure A.1: Dimension Cryostat - Front View ZTKS0160 / Z31926 / Rev.: 00...
  • Page 71 Technical Data MS 500‘154 USP Dimensions Cryostat Value Unit 3910 Operational Ceiling Height D-RT Diameter RT Bore Tube 1040 Diameter RT vessel 1100 Diameter Bottom Plate 1510 Height Cryostat (bottom plate to top flange) 1861 Height Cryostat (minimum height for transportation) 2040 Height Cryostat (bottom plate to flow system) 1050...
  • Page 72 Technical Data MS 500‘154 USP Top view Figure A.2: Dimension Cryostat - Top View Dimensions Cryostat Value Unit 1597 1435 1783 Table A.6: Dimensions Cryostat - Top View 1. Keep at least an additional free space of 1.5 m around the magnet system for service. ZTKS0160 / Z31926 / Rev.: 00...
  • Page 73 Technical Data MS 500‘154 USP A.5.2 Technical Data Cryostat Supplies during installation The consumption of liquid cryogenic agents during installation consists of consumption for cooling down the cryostat and the volume to fill the vessels. Cryogenic Agent Value Unit Nitrogen Helium Table A.7: Installation Consumption...
  • Page 74 Technical Data MS 500‘154 USP Nitrogen Level Graph Figure A.3: Nitrogen Level Graph ZTKS0160 / Z31926 / Rev.: 00...
  • Page 75 Technical Data MS 500‘154 USP Helium Level Graph Figure A.4: Helium Level Graph ZTKS0160 / Z31926 / Rev.: 00...
  • Page 76 Technical Data MS 500‘154 USP This side is intentionally left blank. ZTKS0160 / Z31926 / Rev.: 00...
  • Page 77 Technical Data MS 500‘154 USP Helium Level Sensor The helium level sensor is inserted in the helium fill-in turret. Helium Level Sensor Material No. Value Unit Level Sensor Type Z103297 Overall length 1185 Active length Calibration 0 %, Calibration resistor Z53168 Ω...
  • Page 78 Technical Data MS 500‘154 USP Temperature Sensors The temperature sensors (PT 100 and IBT) will be used to monitor the temperature of the magnets during cooling and warming up of the magnet system. PT 100 Measure the resistance with a maximum current of 1 mA. Temperature Unit Resistance...
  • Page 79 Technical Data MS 500‘154 USP IBT Carbon Resistor Measure the Resistance with a maximum current of 0.1 mA. Temperature Unit Resistance Unit Room Temperature Ω Liquid Nitrogen Ω Ω Ω Ω Ω Ω Ω Liquid Helium Ω Table A.11: Characteristic Values IBT Figure A.7: Characteristic Curve IBT ZTKS0160 / Z31926 / Rev.: 00...
  • Page 80 Technical Data MS 500‘154 USP Environmental conditions Value Unit Minimum surrounding temperature °C Maximum surrounding temperature °C Maximum relative humidity up to 31°C Maximum relative humidity between 31°C and 40°C 80-50 linear decreasing Table A.12: Environmental conditions Identification Plate The identification plate is on the right back side of the cryostat fixed at the bottom plate. Contents of the identification plate: •...
  • Page 81 Technical Data MS 500‘154 USP A.5.3 Technical Data Magnet Technical Data Magnet Value Unit Proton frequency Central field 11.74 Coil inductance Magnetic energy 2654 Magnetic centre from bottom flange (design value) Maximum drift rate 0.015 ppm/h Hz/h Radial stray field at 0.5mT Axial stray field at 0.5mT Table A.13: Specification of the Magnet...
  • Page 82 Technical Data MS 500‘154 USP High Current Lead Figure A.8: High Current Lead 2 pins ZTKS0160 / Z31926 / Rev.: 00...
  • Page 83 Technical Data MS 500‘154 USP Current Lead Figure A.9: Current Lead 55 pins ZTKS0160 / Z31926 / Rev.: 00...
  • Page 84 Technical Data MS 500‘154 USP Wiring Diagram Magnet Figure A.10: Wiring Diagram Magnet ZTKS0160 / Z31926 / Rev.: 00...
  • Page 85 Technical Data MS 500‘154 USP Wiring Diagram Magnet Control and Shims Figure A.11: Wiring Diagram Magnet - Control and Shims ZTKS0160 / Z31926 / Rev.: 00...
  • Page 86 Technical Data MS 500‘154 USP Wiring Diagram Magnet Diagnostic and Temperature Sensors Figure A.12: Wiring Diagram Magnet - Diagnostic and Temperature Sensors ZTKS0160 / Z31926 / Rev.: 00...
  • Page 87 Technical Data MS 500‘154 USP Resistance at Room Temperature _ _ _´_ _ _´_ _ _´_ _ Connector Description Value Unit From: PIN V 19 PIN Con CONTROL Main Heater Ω PIN S 19 PIN Con CONTROL From: PIN D 19 PIN Con CONTROL Z Heater Ω...
  • Page 88 Main heater current Shim heater current Table A.15: Heater currents Energizing Assignment and Currents Energizing Currents Sense voltage Remarks Bruker Test Site [mV] 4000 2000 1000 Overshoot (0.25 % of final current) 10 Minutes break at overshoot current Total energizing time [min] Table A.16:...
  • Page 89 Technical Data MS 500‘154 USP Energizing Currents _ _ _´_ _ _´_ _ _´_ _ Energizing Currents Value Value Value Unit Bruker Test Customer Customer Site Site #1 Site #2 Magnet main current Z-Shim current -Shim current -Shim current X–Shim current Y–Shim current...
  • Page 90 Technical Data MS 500‘154 USP Cycling Assignment and Shim Currents _ _ _´_ _ _´_ _ _´_ _ (recommended only for 500MHz and more) Cycling Assignment and Shim Currents Value Unit Time between energizing and cycling (at least 12 h) Time between cycling and shimming (at least 12 h) Current rate Z-Shim current...
  • Page 91 Technical Data MS 500‘154 USP Deenergizing Assignment and Currents _ _ _´_ _ _´_ _ _´_ _ Deenergizing Currents Sense voltage Remarks Bruker Test Site [mV] 1000 2000 through external diodes Total deenergizing time [min] Table A.19: Deenergizing Assignment and Currents...
  • Page 92 Technical Data MS 500‘154 USP This side is intentionally left blank. ZTKS0160 / Z31926 / Rev.: 00...
  • Page 93 Technical Data MS 500‘154 USP Shorting Plug The shorting plug is plugged after removal of the current lead. After inserting the shorting plug the current flows through the shorting plug and no longer through the current lead and the power supply. Figure A.13: Shorting Plug 55 pins 1 Shorting Plug Tool for fitting and removing the shorting plug 2 Shorting Plug...
  • Page 94 Technical Data MS 500‘154 USP Fringe Field Plot Figure A.14: Fringe field plot Fringe Field Unit R max Unit Z max Unit 0.05 3.31 4.85 2.55 3.95 2.00 3.25 1.50 2.55 1.32 2.15 1.07 1.66 0.97 1.48 Table A.20: Fringe Field Values ZTKS0160 / Z31926 / Rev.: 00...
  • Page 95 Technical Data MS 500‘154 USP Nitrogen Refill Report Nitrogen level Nitrogen level Refill Volume Date, Time Signature before refill [%] after refill [%] [ l ] ZTKS0160 / Z31926 / Rev.: 00...
  • Page 96 Technical Data MS 500‘154 USP Nitrogen Refill Report Nitrogen level Nitrogen level Refill Volume Date, Time Signature before refill [%] after refill [%] [ l ] ZTKS0160 / Z31926 / Rev.: 00...
  • Page 97 Technical Data MS 500‘154 USP Nitrogen Refill Report Nitrogen level Nitrogen level Refill Volume Date, Time Signature before refill [%] after refill [%] [ l ] ZTKS0160 / Z31926 / Rev.: 00...
  • Page 98 Technical Data MS 500‘154 USP Helium Refill Report Helium level Helium level Refill Volume Date, Time Signature before refill [%] after refill [%] [ l ] ZTKS0160 / Z31926 / Rev.: 00...
  • Page 99 Technical Data MS 500‘154 USP Helium Refill Report Helium level Helium level Refill Volume Date, Time Signature before refill [%] after refill [%] [ l ] ZTKS0160 / Z31926 / Rev.: 00...
  • Page 100 Technical Data MS 500‘154 USP ZTKS0160 / Z31926 / Rev.: 00...

  • Page 101: Index

    Index Approved Persons of the Customer ..13 Attachment Points ........32 Bruker Service ..........13 Bursting Disc ..........26 Cleaning Staff ...........14 Complaint Process ........30 Cryogenic Agents ......18 Cryostat ............12 Disturbances ..........48 Drop Off Plate ...........26 Electricity ..........19 Emergency ..........27 Emergency Exit ........25 Fire Department ........27...
  • Page 102 Portable Oxygen Monitor ......24 Protective Clothes ........24 Protective Gloves ........24 Protective Goggles ........24 Quench ..........20 Quench Valve .......... 26 Rescue Equipment ........27 Safety Devices ......... 26 Safety Shoes ........... 24 Safety Valve ..........26 Shock Watch ..........
  • Page 103 Revision History List Index: Date: Alteration Type: September First version according the specific form of the Corporate Guide 2010 Line and the definition from the Bruker documentation group and a new order of content. ZTKS0160 / Z31926 / Rev.: 00...
  • Page 104 ZTKS0160 / Z31926 / Rev.: 00...
  • Page 105 With 50 years of experience in meeting the demands of the scientific community across a range of specialist disciplines, Bruker BioSpin has built a sound rapport with professionals from the scientific community through understanding their specific demands and providing them with effective solutions and a service of unmatched quality.

Table of Contents