Hach Intellical MTC30101 User Manual

Refillable orp/redox probe
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User Manual
Refillable ORP/Redox Probe: Model MTC30101 or MTC30103
Safety information
Precautionary labels
Electrical equipment marked with this symbol may not be disposed of in European domestic or public disposal
systems. Return old or end-of-life equipment to the manufacturer for disposal at no charge to the user.
Specifications
Specifications
Probe type
Range
Resolution
Temperature accuracy
Operating temperature range
Storage temperature range
Junction
Reference potential versus Standard
Hydrogen Electrode
Fill solution
Reference type
Minimum sample depth
Dimensions
Cable connection
Product overview
Read all labels and tags attached to the instrument. Personal injury or damage to the
instrument could occur if not observed. A symbol on the instrument is referenced in the
manual with a precautionary statement.
Note: Specifications are subject to change without notice.
Details
Digital combination electrode with a refillable Ag/AgCl reference and a built-
in temperature sensor
±1200 mV
0.1 mV
±0.3 °C (±0.54 °F)
0 to 80 °C (32 to 176 °F)
5 to 40 °C (41 to 104 °F)
Ceramic
207 mV at 25 °C
3M KCl with saturated AgCl
Ag/AgCl (3 M KCl)
20 mm
Diameter: 12 mm (0.47 in.)
Length: 175 mm (6.89 in.)
Cable length: 1 or 3 m (3.28 or 9.84 ft)
M12 digital output and connector compatible with HQd meters
The MTC301 series probe is a refillable, combination oxidation reduction potential
(ORP/Redox) probe with a built-in temperature sensor
MTC30103 probe is available with a 1 or 3 m (3.28 or 9.84 ft) cable and is intended for
laboratory use. The probe measures absolute mV values in wastewater, drinking water
and general applications. The probe measures ORP/Redox in wastewater, drinking water
and general applications. A 59 mL bottle of reference electrolyte filling solution (3M KCl
solution saturated with AgCl) is included with the probe.
DOC022.52.80026
(Figure
1). The MTC30101 or
1

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Summary of Contents for Hach Intellical MTC30101

  • Page 1 User Manual DOC022.52.80026 Refillable ORP/Redox Probe: Model MTC30101 or MTC30103 Safety information Precautionary labels Read all labels and tags attached to the instrument. Personal injury or damage to the instrument could occur if not observed. A symbol on the instrument is referenced in the manual with a precautionary statement.
  • Page 2: Preparation For Use

    Figure 1 Probe overview 1 Probe soaker bottle 4 Protective tape and filing-hole 2 Reference junction, platinum and temperature sensor 5 1 or 3 meter (3.28 or 9.84 ft) cable 3 Filling-hole cap 6 Probe soaker bottle holder Preparation for use Prepare the probe for use before calibration or sample measurement.
  • Page 3 Calibration Before calibration: The probe must have the correct service-life time stamp. Set the date and time in the meter before the probe is attached. It is not necessary to recalibrate when moving a calibrated probe from one HQd meter to another if the additional meter is configured to use the same calibration options.
  • Page 4: Sample Measurement

    6. Push Read. 7. Push Done to 8. Push Store to Stir gently. The view the accept the display will show calibration calibration and go "Stabilizing" and a summary. back to the progress bar as measurement the probe mode. stabilizes in the sample.
  • Page 5 1. Connect the 2. To significantly 3. Rinse the probe 4. Put the probe in 5. Push Read. probe to the reduce the with the sample. the sample and The display will meter. Make sure stabilization time stir gently. Make show "Stabilizing"...
  • Page 6 Table 1 Standard potential of reference electrode (continued) Temperature (°C) Electrode potential in mV (E 172.1 176.4 180.3 184.4 188.4 192.3 196.1 199.8 203.4 207.0 210.5 214.0 217.4 220.9 224.2 Measurement—oxidation titrations procedure: Oxidation-reduction, or redox titrations, give a simple, reliable method to identify many substances in a solution.
  • Page 7: Run Check Standard

    1. Fill a 10 mL 2. Connect the 3. Pipet a 50 mL 4. Add titrant in 5. Plot the burette with a probe to the sample into a 0.5 to 1 mL electrode potential standard titrant meter. 150‑mL beaker. increments.
  • Page 8: Advanced Operation

    5. Put the probe in the standard solution. Make sure that the reference junction is fully in the standard. Move the probe up or down or lightly shake the probe to remove air bubbles. 6. Push Read. The display shows "Stabilizing" and a progress bar as the reading stabilizes.
  • Page 9: Change Calibration Options

    3. Select Modify Current Settings. 4. Select Measurement Options and update the settings: Option Description Response Time Sets the response time— • Fast (2 mV/minute) • Medium (1 mV/minute) (default) • Slow (0.5 mV/minute) The response time affects the speed of the measurement by adjusting the stabilization criteria.
  • Page 10: Change Check Standard Options

    6. If prompted, enter a name for the new method settings. Additional changes made to the settings of an existing method are automatically saved with the same method name. 7. Push EXIT until the meter returns to the measurement mode. Change check standard options 1.
  • Page 11: Fill The Probe

    2). 2. Rinse the probe with deionized water. Dry the probe with a lint-free cloth. 3. Fill the probe soaker bottle half full with Hach Electrode Storage Solution or 3 M potassium chloride (KCl) solution. 4. Loosen the soaker bottle cap and put the soaker bottle on the probe.
  • Page 12 Troubleshooting Message or symptom Possible cause Action Probe not supported Software not updated To download the most current version of the software, refer to the applicable product page on the manufacturer's website. Refer to the HQd Series meter manual for specific instructions for the meter model.
  • Page 13 Message or symptom Possible cause Action Slow stabilization time Contaminated platinum sensor Clean the probe (refer to Clean the probe on page 10). Probe not conditioned/pre-treated for To significantly reduce the response time for reducing type samples reducing type samples the platinum disc must undergo the following: Make sure that the platinum disc is clean and smooth.
  • Page 14 Message or symptom Possible cause Action Drifting/Inaccurate Contaminated platinum disc Clean the probe (refer to Clean the probe readings on page 10). Clogged reference Thoroughly rinse the reference junction holes with deionized water. Gently tap the probe with hand while holding the probe downward to remove any air bubbles.
  • Page 16 Fax (970) 669-2932 Fax +49 (0) 2 11 52 88-210 Tel. +41 22 594 6400 orders@hach.com info@hach-lange.de Fax +41 22 594 6499 www.hach.com www.hach-lange.de © Hach Company/Hach Lange GmbH, 2010, 2013, 2014. All rights reserved. Printed in U.S.A. 07/2014, Edition 3...

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