Vaisala HPP272 User Manual

Vaisala HPP272 User Manual

Peroxcap hydrogen peroxide, humidity and temperature probe
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M211972EN-B
User Guide
â
Vaisala PEROXCAP
Hydrogen Peroxide,
Humidity and Temperature Probe
HPP272

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Summary of Contents for Vaisala HPP272

  • Page 1 M211972EN-B User Guide â Vaisala PEROXCAP Hydrogen Peroxide, Humidity and Temperature Probe HPP272...
  • Page 2 Street address: Vanha Nurmijärventie 21, FI-01670 Vantaa, Finland Mailing address: P.O. Box 26, FI-00421 Helsinki, Finland Phone: +358 9 8949 1 Visit our Internet pages at www.vaisala.com. © Vaisala 2017 local rules and regulations No part of this manual may be...
  • Page 3: Table Of Contents

    About This Document................... 5 Version Information..................5 Related Manuals....................5 Documentation Conventions................5 Trademarks......................6 Patent Notice.....................6 Product Overview................... 7 Introduction to HPP272..................7 Basic Features and Options................8 Safety........................8 ESD Protection....................9 Measured Parameters..................9 2.5.1 Understanding Relative Humidity and Relative Saturation....10 Probe Filter......................11...
  • Page 4 HPP272 User Guide M211972EN-B Using Probe with Indigo Transmitters..........29 Indigo Overview..................... 29 7.1.1 Wireless Configuration Interface Overview.........30 Attaching Probes..................... 31 Connecting to Wireless Configuration Interface........32 Logging in to Wireless Configuration Interface..........33 Maintenance....................34 Cleaning the Probe..................34 8.1.1 Chemical Tolerance.................34 Calibration and Adjustment................
  • Page 5 H O concentration evenly distributed)....19 Figure 7 Probe M12/5 Pins....................22 Figure 8 Wiring Example for Connecting HPP272 to a PLC in Analog Mode..................... 23 Figure 9 Pins on the M12 male connector..............24 Figure 10 Connecting Probe to Insight................. 28 Figure 11 Attaching Probes to Indigo................
  • Page 6 HPP272 User Guide M211972EN-B List of Tables Table 1 Document Versions....................5 Table 2 Related Manuals....................5 Table 3 Applicable Patents or Applications..............6 Table 4 Available Parameters...................9 Table 5 Measurement Performance................41 Table 6 Inputs and Outputs....................42 Table 7 Mechanical Specifications................43 Table 8 Operating Environment..................43...
  • Page 7: About This Document

    Chapter 1 – About This Document 1. About This Document 1.1 Version Information This document provides instructions for installing, using, and maintaining Vaisala PEROXCAPâ Hydrogen Peroxide, Humidity and Temperature Probe HPP272. Table 1 Document Versions Document Date Description Code M211972EN-B December 2017 This document. Added description and Modbus registers for...
  • Page 8: Trademarks

    Indicates that you need to take some notes during the task. 1.4 Trademarks Vaisalaâ, HUMICAPâ, and PEROXCAPâ are registered trademarks of Vaisala Oyj. Indigo ™ is a trademark of Vaisala Oyj. All other product or company names that may be mentioned in this publication are trade names, trademarks, or registered trademarks of their respective owners.
  • Page 9: Product Overview

    2. Product Overview 2.1 Introduction to HPP272 Vaisala PEROXCAPâ Hydrogen Peroxide, Humidity and Temperature Probe HPP270 series is designed for demanding hydrogen peroxide bio-decontamination processes. The probes are suitable for a variety of applications such as isolator, material transfer hatch, and room bio- decontamination.
  • Page 10: Basic Features And Options

    • Analog output: 2 x 4 ... 20 mA (default). • Easy plug-in, plug-out. • Can be used as a stand-alone probe or with Vaisala Indigo 200 series transmitters. • Can be connected to Vaisala Insight software for configuration, diagnostics, and temporary online monitoring.
  • Page 11: Esd Protection

    2.4 ESD Protection Electrostatic Discharge (ESD) can cause immediate or latent damage to electronic circuits. Vaisala products are adequately protected against ESD for their intended use. However, it is possible to damage the product by delivering an electrostatic discharge when touching, removing or inserting any objects inside the equipment housing.
  • Page 12: Understanding Relative Humidity And Relative Saturation

    2.5.1 Understanding Relative Humidity and Relative Saturation Water and hydrogen peroxide have a very similar molecular structure, and they both affect the humidity of the air in which they are present. HPP272 measurement makes a difference between the humidity caused by both H...
  • Page 13: Probe Filter

    The purge is automatically performed: • At probe start-up. • At intervals (default 24 hours, configurable between 1 hour ... 1 week using Vaisala Insight software, Modbus, or Indigo 200 transmitters). Purge is postponed by 30 minutes if H is present or RH is not steady.
  • Page 14: Environmental Compensation For Pressure

    More Information ‣ Configuration Registers (page 48) 2.10 Connectivity to Vaisala Insight Software The probe can be connected to Vaisala Insight software using a Vaisala USB cable (no. 242659). With the Insight software, you can: • See device information and status.
  • Page 15: Additional Features With Indigo Transmitters

    ‣ Connecting to Insight Software (page 28) 2.11 Additional Features with Indigo Transmitters The probes are compatible with Vaisala Indigo 200 transmitters starting from Indigo transmitter serial number N4650357 (Indigo 200 transmitter software version 1.3.2 or higher). Connecting the probe to an Indigo transmitter provides a range of additional options for outputs, measurement viewing, status monitoring, and configuration interface access.
  • Page 16: H 2 O 2 Measurement

    PEROXCAP sensor within a day, and the sensor will not recover. PEROXCAPâ sensor technology works using measurements from two Vaisala HUMICAPâ sensors. HUMICAP sensors guarantee quality and reliability, with their reputation for repeatability, accuracy, excellent long-term stability, and negligible hysteresis – even in the most demanding high-concentration H applications in atmospheric pressure.
  • Page 17: Figure 3 Operating Principle Of Peroxcap Measurement

    Thin film polymer between two electrodes. Alumina substrate. In addition to measuring vaporized H concentration, HPP272 provides measurement for relative saturation, relative humidity, and temperature. Relative humidity (RH) is a parameter that indicates the humidity value derived from water vapor only, whereas relative saturation (RS) indicates the humidity percentage derived from water vapor and H vapor together.
  • Page 18: Typical Applications

    HPP272 User Guide M211972EN-B 3.2 Typical Applications The probe is not intended for safety level measurement. The probe is not intended to be used in vacuum applications. Vaporized hydrogen peroxide is used for bio-decontamination in several applications from healthcare and pharmaceutics to food and beverage industry. Vaporized hydrogen peroxide is...
  • Page 19: Figure 4 Example Behavior Of H Concentration, Relative Saturation (Rs), And Relative Humidity (Rh) In A Vaporized H Bio-Decontamination Cycle (Non- Condensing Conditions)

    Chapter 3 – H2O2 Measurement More 100% CONDENSATION POINT VAPORIZED HYDROGEN PEROXIDE CONCENTRATION Humidity Concentration RELATIVE SATURATION (RS) RELATIVE HUMIDITY (RH) Less Cycle Phase Figure 4 Example behavior of H concentration, relative saturation (RS), and relative humidity (RH) in a vaporized H bio-decontamination cycle (non-condensing conditions) In the non-condensing bio-decontamination cycle example shown in Figure 4 (page...
  • Page 20: Condensation Monitoring

    HPP272 User Guide M211972EN-B For condensation monitoring, choosing the right measurement location is very important. If the bio-decontaminated space has surfaces with a lower temperature than where RS is measured, condensation may start to form on those surfaces even before RS reaches 100 %RS in the exact measurement location.
  • Page 21: Figure 6 Decontaminated Space With Different Temperatures And Rs Levels (H And H O Concentration Evenly Distributed)

    Chapter 3 – H2O2 Measurement T= 21 ˚C RS= 100 %RS T= 21.5 ˚C RS= 94.5 %RS T= 22 ˚C RS= 89.5 %RS Figure 6 Decontaminated space with different temperatures and RS levels (H and H concentration evenly distributed) Center of the decontaminated space. The center is warmer than the wall and the window, and the RS level is lower.
  • Page 22: Installation

    HPP272 User Guide M211972EN-B 4. Installation Accurate RH and RS measurement requires both humidity and temperature data from the same environment. Install the H and humidity probe and the temperature probe in the same measurement environment and temperature, approximately 6 ... 10 cm apart from each other.
  • Page 23 Seal the lead-throughs on the metal body of the probes. The figure shows an example installation using Vaisala spare part glands (HPP272MOUNTINGSET1). Nut for tightening the probe in place Nut for mounting the gland 4 cm (recommended) Ø...
  • Page 24: Wiring

    HPP272 User Guide M211972EN-B 4.1 Wiring Figure 7 Probe M12/5 Pins Pin # Function Notes Wire Color Power supply With digital output: 15 ... 30 VDC Brown With analog output: 15 ... 25 VDC When using analog outputs, it is recommended to use a low supply voltage to minimize self-heating and maximize measurement performance.
  • Page 25: Power Supply

    Pin #1 (Power supply) Pin #3 (Power and signal GND) Figure 8 Wiring Example for Connecting HPP272 to a PLC in Analog Mode More Information ‣ Accessories (page 44) ‣ Triggering Purge in Analog Mode (page 27) 4.2 Power Supply Operating voltage range of the probe: •...
  • Page 26: Figure 9 Pins On The M12 Male Connector

    HPP272 User Guide M211972EN-B Figure 9 Pins on the M12 male connector 1. If the probe is powered on, power off the probe. 2. Select the output mode with pin #5: a. To set the probe in analog mode, connect pin #5 to ground.
  • Page 27: Operation

    . This variation is normal and does not require any actions. If needed, you can hide the variation by setting a low clipping limit with the Vaisala Insight software, Modbus configuration register 030C , or an Indigo 200 transmitter. For example, if you set the low clipping limit to 3 ppm,...
  • Page 28: Modbus

    HPP272 User Guide M211972EN-B More Information ‣ Vaisala Insight Software (page 28) ‣ Configuration Registers (page 48) 5.4 Modbus The probe can be accessed using the Modbus serial communication protocol. The supported Modbus variant is Modbus RTU (Serial Modbus) over RS-485 interface.
  • Page 29: Triggering Purge In Analog Mode

    Chapter 5 – Operation More Information ‣ Analog Output Error State (page 40) 5.5.2 Triggering Purge in Analog Mode In the analog mode, pin #5 in the probe's M12 male connector is connected to ground. Additionally, pin #5 is used to trigger a purge in analog mode. To be able to trigger a purge, do not connect pin #5 to ground permanently, but instead, use a relay or similar to control the pin.
  • Page 30: Vaisala Insight Software

    • Calibrate and adjust the device. Download Vaisala Insight software at www.vaisala.com/insight. The probe can be connected to Vaisala Insight software using a Vaisala USB cable (no. 242659). 6.1 Connecting to Insight Software • Computer with Insight software installed •...
  • Page 31: Using Probe With Indigo Transmitters

    Cable locking wheel: insert cable, hold in place, and turn the wheel counterclockwise. Wireless configuration interface (WLAN) activation button. Rubber lead-through with strain relief. Cable feedthrough option also at back of transmitter. Input/output cable. The probe can be connected to Vaisala Indigo transmitters by using a cable.
  • Page 32: Wireless Configuration Interface Overview

    HPP272 User Guide M211972EN-B Indigo transmitters are host devices that extend the feature set of connected probes with a range of additional options for outputs, configuration access, measurement viewing, and status monitoring. The selection of available additional features (for example, output and connectivity options) varies depending on the Indigo transmitter model.
  • Page 33: Attaching Probes

    Chapter 7 – Using Probe with Indigo Transmitters 7.2 Attaching Probes Figure 11 Attaching Probes to Indigo 1. Connect the cable to the probe. 2. Insert the other end of the cable in Indigo's cable connector and lock it in place by turning the locking wheel counterclockwise.
  • Page 34: Connecting To Wireless Configuration Interface

    HPP272 User Guide M211972EN-B 7.3 Connecting to Wireless Configuration Interface Indigo 201   Select WLAN to connect to: 74.2 1. WLAN XYZ RS (H O+H O ) 2. Indigo_IDxx 32.4 3. WLAN ABC °C  WLAN is activated Figure 12 Enabling and Accessing Indigo's Wireless Configuration Interface...
  • Page 35: Logging In To Wireless Configuration Interface

    Chapter 7 – Using Probe with Indigo Transmitters 7.4 Logging in to Wireless Configuration Interface Figure 13 Indigo Login View When you open Indigo's wireless configuration interface in your browser, you are prompted to log in. There are 2 available user levels: •...
  • Page 36: Maintenance

    HPP272 User Guide M211972EN-B 8. Maintenance 8.1 Cleaning the Probe CAUTION! Do not remove the filter. CAUTION! Do not attempt to clean the sensors under the filter in any way. Avoid exposing the probe to cleaning agents for unnecessarily long periods of time.
  • Page 37: Calibration And Adjustment

    The probe is fully calibrated and adjusted as shipped from the factory. A typical calibration interval is 1 year, depending on how frequently and long your probe is exposed to vaporized Calibration and adjustment is performed by Vaisala. For contact information, visit www.vaisala.com/calibration.
  • Page 38: Troubleshooting

    If you have a problem with using the probe, check the following tables before contacting Vaisala. If the problem you have is not listed in the tables, or if the proposed solution does not fix the problem, contact Vaisala technical support.
  • Page 39 Solution: In analog mode: The scaling of Check and change the analog output scaling with Insight the output is unsuitable, software (see Vaisala Insight Software (page 28)). preventing the change from showing. In analog mode: The error level Check the probe diagnostics with the Insight software (see...
  • Page 40 HPP272 User Guide M211972EN-B Problem: Measurement reading appears incorrect. The filter is not installed on the Do not use the probe without the filter. Install the filter on the probe. probe. The yellow transport cap is still Remove the yellow transport cap when measuring with the on the probe.
  • Page 41 (for communication settings with the Insight software. See example the device address) • Vaisala Insight Software (page 28) are incorrect either in the probe or in the system where the probe is connected. Problem: In analog mode, there is no output signal (signal level is 0 mA).
  • Page 42: Analog Output Error State

    HPP272 User Guide M211972EN-B Problem: In analog mode, there is no output signal (signal level is 0 mA). The probe cable is not properly Check the cable connection and correct it if needed. connected. Power input to the probe is off.
  • Page 43: Technical Data

    Chapter 10 – Technical Data 10. Technical Data Table 5 Measurement Performance Property Description/Value Hydrogen Peroxide Sensor PEROXCAPâ Measurement range 0 ... 2000 ppm Measurement temperature range +5 ... +50 °C (+41 ... +122 °F) Repeatability at +25 °C (+77 °F), 500 ppm H ±20 ppm Accuracy (including non-linearity, hysteresis, and ±10 ppm or 5 % of reading (whichever...
  • Page 44: Table 6 Inputs And Outputs

    HPP272 User Guide M211972EN-B Property Description/Value Factory calibration uncertainty, at +25 °C (77 °F), 0 ppm H at 0 … 40 %RH ±0.6 %RH at 40 … 95 %RH ±1 %RH Temperature Sensor Pt-1000 RTD Class F0.1 Accuracy over temperature range ±0.2 °C (±0.36 °F)
  • Page 45: Dimensions

    Operating temperature +0 ... +70 °C (+32 ... +158 °F) Storage temperature -20 ... +70 °C (-4 ... +158 °F) Ambient pressure Normal atmospheric pressure EMC compliance EN61326-1, Controlled Environment 10.1 Dimensions 118.3 38.5 Ø=30 Ø=16/18.5 Ø=18.5 69.8, Ø=4.8 Figure 14 HPP272 Dimensions...
  • Page 46: Accessories

    Probe cable with open wires (10 m) 216546SP Probe cable with open wires and 90° plug (0.6 m) 244669SP Filter DRW246363SP Gland set for through-wall installation, HPP272 HPP272MOUNTINGSET1 Transmitters Indigo 200 series www.vaisala.com/indigo Connection cable to Indigo (1 m) INDIGOCABLE1M...
  • Page 47: Appendix A: Modbus Reference

    Appendix A – Modbus Reference Appendix A. Modbus Reference A.1 Default Communication Settings Table 10 Default Modbus Serial Communication Settings Description Default Value Serial bit rate 19200 Parity Number of data bits Number of stop bits Modbus device address A.2 Function Codes Table 11 Modbus Function Codes Function Code Function Code Name...
  • Page 48: 16-Bit Integer Format

    HPP272 User Guide M211972EN-B Despite the specification, some Modbus masters may expect "big-endian" word order (most-significant word first). In such case, you must select "word-swapped" floating point format in your Modbus master for the Modbus registers of the device. A "quiet NaN" value is returned for unavailable values. A quiet NaN is, for example, 7FC00000 ;...
  • Page 49: Measurement Data Registers

    Appendix A – Modbus Reference A.4.1 Measurement Data Registers Table 13 Modbus Measurement Data Registers (Read-Only) Address Address Register Description Data Unit (Decimal) (Hexadecimal) Format 0000 Vaporized hydrogen peroxide 32-bit float concentration by volume 0002 relative saturation 32-bit float 0004 Temperature used for calculation. By 32-bit float °C default, shows the temperature from...
  • Page 50: Configuration Registers

    HPP272 User Guide M211972EN-B Address Address Register Description Data Unit (Decimal) (Hexadecimal) Format 0103 Relative humidity 16-bit %RH *100 signed integer 0104 Absolute hydrogen peroxide 16-bit mg/m signed integer 0107 Water concentration by volume 16-bit signed integer 0108 Water vapor pressure...
  • Page 51: Table 14 Modbus Configuration Data Registers (Writable)

    Appendix A – Modbus Reference Table 14 Modbus Configuration Data Registers (Writable) Address Address Register Description Data Unit / Valid Range (Decimal) (Hexadecimal) Format 0300 Volatile value for 32-bit float pressure compensation 813.25 ... 1213.25 (value cleared at probe (default 1013.25 hPa) reset).
  • Page 52 HPP272 User Guide M211972EN-B Address Address Register Description Data Unit / Valid Range (Decimal) (Hexadecimal) Format 030A Measurement filtering 32-bit float Range: 0.01 ... 1 factor (does not affect 1 = Filter is disabled temperature, water, or RH < 1 = Reading is a...
  • Page 53 Appendix A – Modbus Reference Address Address Register Description Data Unit / Valid Range (Decimal) (Hexadecimal) Format 1286 0505 Temperature 16-bit 0 = Off compensation on/off boolean 1 = On. If turned on, overrides the temperature from the temperature probe in the calculation of other measurement parameters.
  • Page 54 HPP272 User Guide M211972EN-B Address Address Register Description Data Unit / Valid Range (Decimal) (Hexadecimal) Format 1793 0700 Output mode enum 0 = Off 1 = 0 ... 20 mA 2 = 4 ... 20 mA (default: 2 = 4 ... 20 mA)
  • Page 55 Appendix A – Modbus Reference Address Address Register Description Data Unit / Valid Range (Decimal) (Hexadecimal) Format 2053 0804 Scale high end 32-bit float Set the upper limit of the measurement scale for the output parameter chosen in register 0801 (Output parameter).
  • Page 56: Status Registers

    HPP272 User Guide M211972EN-B A.4.3 Status Registers Table 15 Modbus Status Registers (Read-Only) Address Address Register Description Data Notes (Decimal) (Hexadecimal) Format 0200 Device status 16-bit 0 = Status OK. 1 = Critical error, maintenance needed. 2 = Error, device may recover automatically.
  • Page 57: Table 16 Error Codes In Register 0201

    Appendix A – Modbus Reference Address Address Register Description Data Notes (Decimal) (Hexadecimal) Format 0210 Status of Hydrogen 16-bit 0 = Status OK. peroxide concentration 2 = Reading is not by volume reliable. 0211 Status of H 16-bit 32 = Reading is locked relative saturation during purge.
  • Page 58: Device Identification Objects

    HPP272 User Guide M211972EN-B Value of Error Message Severity Register 0201 1024 Humidity sensor failure (open circuit). Error 16384 Temperature sensor failure (open circuit). Error 32768 Temperature sensor failure (short circuit). Error 262144 Temperature sensor failure (open circuit). Error 524288 Temperature sensor failure (short circuit).
  • Page 59: Test Value Registers

    Object Id Object Id Object Name Example Contents (decimal) (hexadecimal) ProductName Hydroxen Peroxide, Humidity, and Temperature Probe HPP272 SerialNumber Serial number of the device (for example “K0710040”) Calibration date Date of the factory calibration Calibration text Information text of the factory calibration A.4.5 Test Value Registers...
  • Page 60: Modbus Communication Examples

    HPP272 User Guide M211972EN-B A.5 Modbus Communication Examples Reading H Concentration Value Device address used in the following examples is 240 (F0 The values returned by the device differ depending on the ambient conditions and/or device settings. Your device might not return exactly same values.
  • Page 61 (Hexadecimal) (Hexadecimal) (silence for 3.5 bytes) Start of Modbus RTU (silence for 3.5 bytes) Start of Modbus RTU frame frame HPP272 address HPP272 address Function (Write Function (Write Multiple Registers) Multiple Registers) Register address Register address Number of registers to...
  • Page 62 HPP272 User Guide M211972EN-B Communication Description Value to write 0B40 = 2880 (minutes) (= 48 hours)
  • Page 63: Warranty

    Please see the applicable supply contract or Conditions of Sale for details of the warranty for each product. Technical Support Contact Vaisala technical support at helpdesk@vaisala.com. Provide at least the following supporting information: • Product name, model, and serial number •...
  • Page 64 HPP272 User Guide M211972EN-B...
  • Page 66 www. v aisala.com...

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