Related Manuals for Endress+Hauser Stamolys CA71
Summary of Contents for Endress+Hauser Stamolys CA71
- Page 1 Operating Instructions Stamolys CA71PH Analyzer for Photometric Determination of Phosphate BA356C/07/en/07.06 71092653 Valid as of: Software version 5.8...
- Page 2 → ä 36, → ä 61 Maintenance schedule → ä 36 Replacing consumables and wear parts → ä 42, → ä 56 Accessories Æ → ä 44 Troubleshooting → ä 46, → ä 56 Spare parts Æ → ä 50 Technical data Endress+Hauser...
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Page 3: Table Of Contents
Maintenance kit ......42 Hose cleaner ......42 Endress+Hauser... -
Page 4: Safety Instructions
Please enclose the completed "Declaration of Contamination and Cleaning" form (copy the second last page of these Operating Instructions) with the packaging and also the shipping documents. The unit cannot be repaired if this declaration is not duly completed! Endress+Hauser... -
Page 5: Notes On Safety Icons And Icons
This symbol alerts you to hazards. They could cause serious injuries as well as damage to the instrument if ignored. Caution! " This symbol alerts you to possible faults which could arise from incorrect operation. They could cause damage to the instrument if ignored. Note! This symbol indicates important items of information. Endress+Hauser... -
Page 6: Identification
Stainless steel (1.4301 / AISI 304) without vent. Output 0/4 to 20 mA, RS 232 Profibus DP Reagents To be ordered separately One set inactive, PH-A+E 3 sets inactive, PH-A+E One set inactive, PH-B+D Three sets inactive, PH-B+D CA71PH- complete order code Endress+Hauser... -
Page 7: Scope Of Delivery
4 mark. 2.3.2 Manufacturer's certificate Quality certificate With this certificate, the manufacturer confirms that all technical regulations are met and specified tests have been carried out individually for your product. Endress+Hauser... -
Page 8: Installation
• Valve V1 – Hose at front: sample supply – Hose at rear: supply from valve V2 (cleaner or standard) • Valve V2 – Hose at front: supply from canister with standard – Hose at rear: supply from canister with cleaner Endress+Hauser... -
Page 9: Incoming Acceptance, Transport, Storage
Version with stainless steel housing Detail A 30(1.18) 3(0.12) 38(1.5) 163(6.42) 9(0.35) 15(0.59) 250 (9.84) 330 (13.0) 160 (6.30) 140 (5.51) 15(0.59) 100(3.94) 60(2.36) 200 (7.87) 326 (12.8) Ø 26(1.02) 360 (14.2) 207 (8.15) 436 (17.2) mm(inch) a0001361 Fig. 3: Stainless steel version Endress+Hauser... - Page 10 465 (18.3) mm(inch) 500 (19.7) a0001354-en Fig. 4: GFR version Open version 381 (15.0) 351 (13.8) 19 (0.75) 197 (7.76) RS 232 RS 232 325 (12.8) mm (inch) 8 (0.31) 9 (0.35) a0001356 Fig. 5: Version without housing (open design) Endress+Hauser...
- Page 11 • In the two-channel version, level monitoring is only possible for one channel. • One collecting vessel can be mounted on the housing. A second vessel would have to be made available near the device. Endress+Hauser...
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Page 12: Installation Instructions
ID 19 to the nozzle with a hose clip (only CA71PH-F). Insert the valve hoses accordingly. These were partly removed from the valves for transportation. This prevents the hoses from sticking or pressure being applied to a point in the hose over an extended period. CA71→ å 11 Endress+Hauser... - Page 13 For questions regarding sample conditioning and its automation, please contact Service or the sales center responsible for your region. Connect the tubes from canisters containing reagents, standards and cleaning agents to the following nozzles: Canister Tube designation (mark) Sample Reagent 1 Reagent 2 Standard solution Cleaner Endress+Hauser...
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Page 14: Installation Examples
CAT 411 Sample lines and CAT 430. T-sections Post-installation check • After installation, check that all connections are secure and leaktight. • Ensure that the hoses cannot be removed without effort. • Check all hoses for damage. Endress+Hauser... -
Page 15: Wiring
(item 2). RS 232 a0001370 Fig. 15: Folding out the frame Allen screws AF 6 Terminal block Note! The device does not have a power supply switch. Therefore, it is advantageous to have a fused socket near the device. Endress+Hauser... - Page 16 Last / load: 2A bei / at 115/230V AC, 1A bei / at 30V DC max. Last / load: 2A bei / at 115/230V AC, 1A bei / at 30V DC a0001372 Fig. 17: Analyzer from above (open/folded out) Connection compartment sticker Board with terminal block Rear of analyzer Endress+Hauser...
- Page 17 Operating Instructions of the sample conditioning system. • If there is a 24 V voltage at terminal 57, the analyzer will not begin measurement (sample not ready). To start measurement, the voltage must stay at 0 V for at least 5 seconds. Endress+Hauser...
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Page 18: Signal Connections
Signal outputs Fault Error message, can be retrieved using operation menu Measurement end Displays "Measurement finished" (5 s) l-1 channel 1 0 or 4 mA = start of measuring range Analog output 20 mA = end of measuring range Endress+Hauser... -
Page 19: Switching Contacts
1718 Unassigned 2216 2014 Two-channel version Terminal connection for Terminal connection for Terminal connection for condition fulfilled condition not fulfilled power off AV 1 - 1 AV 1 - 2 AV 2 - 1 AV 2 - 2 Fault Endress+Hauser... -
Page 20: Serial Interface
The following commands can be sent from the PC in order to read out data: • "D" = Data memory-Measured values • "C" = Data memory-Calibration factors • "S" = Setup (parameter entry, configuration...) • "F" = Frequency (current) Endress+Hauser... -
Page 21: Post-Connection Check
PLC, DSC or data logger. If these current values are correct, please check your PLC, DCS, the data logger and/or the electrical cables. Endress+Hauser... -
Page 22: Operation
Error message must be called up – Accept value, move forward in submenu (horizontal) – Selection in the sub-menu Cleaning interval running – Select sign +/- The number of decimal places can be changed by pressing the key and the key simultaneously. Endress+Hauser... - Page 23 • The time of the first measurement has not yet been reached or • The measuring interval has not yet elapsed Note! "Measuring" flashes when the analyzer is ready for the next measurement but has not yet received the enable signal from the sample collector or the sample conditioning unit. Endress+Hauser...
- Page 24 Delay to sample 80 s in the mixer. If sufficient sample is available, or in the event of an external collecting vessel with a long supply line, select the highest possible value. Endress+Hauser...
- Page 25 Redetermine the frequency offset every time the reagents are changed or the photometer is replaced. To do so, instead of sample connect deionized water to the sample inlet to determine the frequency offset (blank value). The value is generally between 0 and 10 Hz. Endress+Hauser...
- Page 26 – Set the time to 8:00 to track the effects of calibration in the curve. – If you have started a calibration manually, you should redefine the time of the 1st calibration because the interval is calculated starting from the last calibration. Endress+Hauser...
- Page 27 • Causes of faults are queried with every measurement. If an error which occurred previously no longer exists, the message is automatically deleted. If this does not happen automatically, error messages can be deleted by quickly switching the analyzer off and back on again. Endress+Hauser...
- Page 28 You can output all data sets (in ASCII-format) via the serial interface. For this, the PC must be configured as Serial output follows: 9600, N, 8, 1. To send data, the PC must send the ASCII character 68 ("d"). Clear data This deletes all data sets. Endress+Hauser...
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Page 29: Calibration
Frequency [Hz] Phosphate, molybdenum blue, 0.05 to 2.5 mg/l 0.00 lower measuring range PH-A 0.25 0.50 0.75 1.00 1.25 1.50 1.75 2.00 2.50 Phosphate, molybdate vanadate, 0.5 to 20.0 mg/l lower measuring range PH-B 10.0 12.0 14.0 16.0 20.0 Endress+Hauser... - Page 30 Rinsing must be performed 3-4 hours before the next calibration. Proceed as described above to change the setting for the time of the 1st calibration. After changing to the measuring mode, the analyzer automatically begins measuring, rinsing and calibrating at the defined times. Endress+Hauser...
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Page 31: Commissioning
Range of adjustment Measurement Flushing (sample) 3 x 15 Delay to sample 20 to 999 CONFIGURATION / "Delay to sample" Stabilization 1. measurement (basis) SERVICE / "Pumps and valves" Fill mixture Reaction see Technical 2nd measurement (plateau) data Flushing (sample) Endress+Hauser... - Page 32 • The dilution factor is not taken into account until the measured value is calculated. • The concentration information you specify for the measuring range and the alarm values in PARAMETER ENTRY refer to the concentrations of the original sample. Endress+Hauser...
- Page 33 Route this hose in the device in such a way that is guided at least 20 cm upwards and then into the open outlet. This prevents the hose from running dry. " Caution! Do not connect the outflow hoses of the dilution module and the photometer. Endress+Hauser...
- Page 34 The following section only lists the parameters where you have to make changes to the standard settings. Start with CONFIGURATION. CONFIGURATION Delay to sample Increase the value of the standard setting by 40 seconds since additional sample volume is drawn in. Endress+Hauser...
- Page 35 If you are using a dilution module with the factor 10, for example, multiply the settings to measuring range end 2 date (without the dilution module) by 10. Alarm values AV 1-1 / 1-2 / 2-1 / 2-2 Calibration solution Enter the original concentration (undiluted) of the standard here. Endress+Hauser...
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Page 36: Maintenance
The reagents must be replaced when: • The reagents have been contaminated by sample (see "Troubleshooting instructions") • The reagents are too old • The reagents have been spoilt by incorrect storage conditions or environmental influences. Endress+Hauser... -
Page 37: Replacing Pump Hoses
– Press against the lower retainer (item 3). – You can now remove the hose box along with the pump hose. – Remove the old hose from the case any dispose of it. – Clean the hose box and the roller head (item 1) with water. Endress+Hauser... - Page 38 Release the adjuster screw (→ å 23, item 3) to the extent that no more sample is pumped. Tighten the screw just to the point that sample is pumped. Make sure that the hoses are bubble-free when filled. If not, check the sample flow rate (see below). Endress+Hauser...
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Page 39: Replacing Valve Hoses
V1-4 Valves 1, 2 and 4 (if present) Channel switching Sample To the pump Y-piece, hose connection to valve 1, at rear Outlet hose Hose valve 2 at front, standard Hose valve 2 at rear, cleaner Hose valve 1 at front, sample Endress+Hauser... -
Page 40: Replacing The Static Mixer
Reassemble the photometer and tighten the screws and nuts. Attach the photometer housing and screw it down. After installation, refill the hoses with sample, standard or cleaning agent (SERVICE). Carry out an f-offset measurement (CONFIGURATION) and a calibration ("Calibration"). Endress+Hauser... -
Page 41: Cleaning
Flush the sampling hoses with clean water and then with compressed air to empty the hoses completely. Remove the valve hoses from the valves. Release the pump hoses by removing the hose box from the holder from below. Note! Store open reagent and standard containers in the refrigerator. Bear the shelf life in mind. Endress+Hauser... -
Page 42: Accessories
– 1 set of pump hoses, black/black – 1 pack of hose connectors each Order No. CAV 740-1A Hose cleaner • Alkaline cleaner, 100 ml (3.4 fl.oz.); Order No. CAY746-V01AAE • Acidic cleaner, 100 ml (3.4 fl.oz.); Order No. CAY747-V01AAE Endress+Hauser... -
Page 43: Dilution Module
• Interference suppressor for control, power and signal lines Order No. 51512800 • Silicone spray, Order No. 51504155 • Valve set, 2 pieces, for two-channel version, Order No. 51512234 • Upgrade kit for upgrading from one-channel to two-channel version, Order No. 51512640 Endress+Hauser... -
Page 44: Troubleshooting
Cell filled with air Pump sample for 1 minute (SERVICE). Photometer defective Inform Service No measuring signal Electrical connection Check all electrical connections and make sure the fuses are firmly seated. Fuse defective Replace fuse F4 or F5 (semi-delay 0.2 A) Endress+Hauser... - Page 45 See "Spillage error" error message Leak sensor bypassed Interrupt the contact between the two leak sensors (terminals 67-66) Pumps fail to run Fuse Check all fuses and replace if necessary. Pump defective Service Measurement does not Leak at photometer Service start Endress+Hauser...
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Page 46: Spare Parts
Spare parts 9.2.1 Overview for 170/171 a0001375 Fig. 25: Overview of components and spare parts Sample input, two-channel version Cleaner canister Standard and reagent canisters Reagent 1 canister Collecting vessel Reagent 2 canister (only PH-A/C/E) Sample Standard solution canister Endress+Hauser... - Page 47 – 1 pack of hose connectors each Photometer cell 51505778 Photometer – PH-A (molybdenum blue, blue) 51512063 – PH-B (molybdate vanadate, yellow) 51512064 – PH-C (molybdenum blue, blue) 51512065 – PH-D (molybdate vanadate, yellow) 51512066 – PH-E (molybdenum blue, blue) 71006301 Endress+Hauser...
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Page 48: Software History
• New startup message • Fault elimination for output for current output, two-channel 05/2003 Extension/improvement BA354C/07/07.03 • New parameter CL • Memory correction • Time for "Delay to sample" is used for zero measurement • Factory settings for MN, SI, HA changed Endress+Hauser... -
Page 49: Return
Operating Instructions) with the packaging and also the shipping documents. The unit cannot be repaired if this declaration is not duly completed! Disposal Electronic components are used in the product. For this reason, the product must be disposed of as electronic waste. Please observe local regulations. Endress+Hauser... -
Page 50: Technical Data
= reaction time + rinse time + waiting time + post rinse time + filling meas time+delay to sample + reject reagent (min. waiting time = 0 min) Maximum measured error ±2 % of end of measuring range Measuring interval ... 120 min meas Endress+Hauser... -
Page 51: Environment
Approx. 33 kg (73 lbs) Without housing Approx. 25 kg (55 lbs) Housing Stainless steel 1.4301 (AISI 304) or GFR Front windows Polycarbonate ® ® Materials Endless hose C-Flex , Norprene ® ® Pump hose Tygon , Viton ® Valves Tygon , silicone Endress+Hauser... -
Page 52: Appendix
Appendix Stamolys CA71PH Appendix 11.1 Operating matrix One-channel version a0001907-en Endress+Hauser... - Page 53 Stamolys CA71PH Appendix a0001908-en Endress+Hauser...
- Page 54 Appendix Stamolys CA71PH Two-channel version a0001909-en Endress+Hauser...
- Page 55 Stamolys CA71PH Appendix a0001910-en Endress+Hauser...
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Page 56: Ordering Forms
Standard 30 mg/l PO CAY242-V10C40AAE Standard 40 mg/l PO CAY242-V10C50AAE Standard 50 mg/l PO Chemicals for ultrafiltration Quantity Order No. Designation CAY746-V01AAE Alkaline cleaner P3-Ultrasil 130, 100 ml CAY746-V10AAE Alkaline cleaner P3-Ultrasil 130, 1 l CAY746-V50AAE Alkaline cleaner P3-Ultrasil T130, 5 l Endress+Hauser... - Page 57 Chemicals for ultrafiltration Quantity Order No. Designation CAY747-V01AAE Acidic cleaner P3-Ultrasil 130, 100 ml CAY747-V10AAE Acidic cleaner P3-Ultrasil 130, 1 l CAY747-V50AAE Acidic cleaner P3-Ultrasil 130, 5 l Place Date Stamp/Signature Earliest delivery one week after order received. Delivery is unpaid. Endress+Hauser...
- Page 58 CA71 kit, level monitoring, retrofitting for collecting vessel 71023419 Please take the designation and the Order No. from the "Troubleshooting/Spare parts" section and enter them here! Place Date Stamp/Signature Earliest delivery one week after order received. Delivery is unpaid. Endress+Hauser...
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Page 59: Analyzer Settings
Measuring range end: • mg/l • μg/l AV 1: • mg/l • μg/l AV 2: • mg/l • μg/l 1. measurement: Measuring interval: 1. calibration: Calibration interval: Calibration solution: • mg/l • μg/l 1. flushing: Flushing interval: Flushing hold on: Endress+Hauser... - Page 60 / μg/l F 4: mg/l / μg/l F 5: mg/l / μg/l F 6: mg/l / μg/l F 7: mg/l / μg/l F 8: mg/l / μg/l F 9: C10: mg/l / μg/l F 10: Date: Service technician: Endress+Hauser...
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Page 61: Maintenance Schedule
Stamolys CA71PH Appendix 11.4 Maintenance schedule a0001911-en Endress+Hauser... - Page 62 Appendix Stamolys CA71PH Endress+Hauser...
- Page 63 Stamolys CA71PH Appendix Endress+Hauser...
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Page 64: Index
Icons ......... 5 Endress+Hauser... - Page 65 Valves ........28 Endress+Hauser...
- Page 66 Stamolys CA71PH Endress+Hauser...
- Page 67 Erklärung zur Kontamination und Reinigung Please reference the Return Authorization Number (RA#), obtained from Endress+Hauser, on all paperwork and mark the RA# clearly on the outside of the box. If this procedure is not followed, it may result in the refusal of the package at our facility.
- Page 68 www.endress.com/worldwide BA356C/07/en/07.06 Printed in Germany / FM+SGML 6.0 / DT 71092653...