Endress+Hauser StamoLys CA 71 MN Operating Instructions Manual

Endress+Hauser StamoLys CA 71 MN Operating Instructions Manual

Manganese analyzer

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BA 363C/07/en/01.03
51512330
Valid of:
Software version 5.0
Quality made by
Endress+Hauser
ISO 9001
StamoLys CA 71 MN
Manganese Analyzer
Operating Instructions

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Summary of Contents for Endress+Hauser StamoLys CA 71 MN

  • Page 1 StamoLys CA 71 MN BA 363C/07/en/01.03 51512330 Valid of: Manganese Analyzer Software version 5.0 Operating Instructions Quality made by Endress+Hauser ISO 9001...
  • Page 3: Table Of Contents

    StamoLys CA 71 MN Table of contents Safety instructions ....5 Trouble-shooting ....37 Designated use .
  • Page 4: Safety Instructions

    • Installation instructions • Local prevailing standards and regulations. Return If the analyzer has to be repaired, please return it cleaned to the Endress+Hauser sales centre responsible. Please use the original packaging, if possible. Please enclose the completed Dangerous Goods sheet (copy the second last page of these Operating instructions) with the packaging and also the shipping documents.
  • Page 5: Notes On Safety Icons And Symbols

    StamoLys CA 71 MN Safety instructions Notes on safety icons and symbols Warning! This symbol alerts you to hazards. They can cause serious damage to the instrument or to persons if ignored. " Caution! This symbol alerts you to possible faults which could arise from incorrect operation.
  • Page 6: Identification

    Identification StamoLys CA 71 MN Identification Device designation 2.1.1 Nameplate Check the order code on the nameplate (at the analyzer) with the product structure (see below) and your order. C07-CA71MNx-18-08-00-xx-001.EPS Fig. 1: Example of a nameplate 2.1.2 Product structure Measuring range Measuring range 1 ...
  • Page 7: Scope Of Delivery

    The product meets the legal requirements of the harmonised European standards. Endress+Hauser confirms compliance with the standards by affixing the symbol. 2.3.2 Manufacturer certificate Quality certificate With the certificate Endress+Hauser confirms compliance with all technical regulations and the successful testing individually for your product. Endress+Hauser...
  • Page 8: Installation

    The original packaging offers the best protection. Also, keep to the approved ambient conditions (see "Technical data"). • If you have any questions, please contact your supplier or your Endress+Hauser sales centre responsible (see back page of these Operating Instructions).
  • Page 9 StamoLys CA 71 MN Installation C07-CA71xxx-06-08-00-en-002.eps Fig. 3: CA 71 dimensions, GFK version 3.2.2 Connecting the sample line C07-CA71xxx-11-08-00-xx-001.eps C07-CA71xxx-06-08-02-en-003.eps Fig. 4: Collecting vessel at analyzer (optionally) Fig. 5: Collecting vessel dimensions Ventilation variable, freely adjustable dimensions Sample inlet from sampling...
  • Page 10 Installation StamoLys CA 71 MN One-channel version E+H Collecting vessel (at CA 71, with or without level measurement) Connection hose ID 3.2 mm (0.13") Customer collecting vessel Connection hose ID 1.6 mm (0.06") Max. distance from collecting vessel to analyzer 1 m (3.28 ft)
  • Page 11: Installation Instructions

    – Sample conditioning using ultrafiltration for heavily soiled media, e.g. from the primary settling tank. For questions regarding sample conditioning and its automation, please contact Endress+Hauser Service or the Endress+Hauser Sales Centre responsible for your region. Connect the tubes from canisters containing reagents, standard and cleaning...
  • Page 12: Installation Examples

    Installation StamoLys CA 71 MN Installation examples 3.4.1 CAT 430 or customer-specific ultra filtration and two CA 71 analyzers • Permeate can contain air bubbles (CAT 430) or is free of bubbles (customer-supplied ultrafiltration) • Distance between the analyzers as short...
  • Page 13: Wiring

    StamoLys CA 71 MN Wiring Wiring Electrical connection Warning! • The electrical connection must only be carried out by authorised technical personnel. • Technical personnel must have read and understood the instructions in this manual and must adhere to them.
  • Page 14 Wiring StamoLys CA 71 MN 4.1.2 Terminal assignment Function Designation Terminal without Terminal with cooling device cooling device Mains Alarm value 1, channel 1 Alarm value 2, channel 1 – Alarm value 1, channel 2 – – – Alarm value 2, channel 2 –...
  • Page 15: Signal Connection

    StamoLys CA 71 MN Wiring Signal connection 4.2.1 Screening of the analog outputs The interference suppressor attenuates electromagnetic effects on control, power and signal lines. After the connection of the data transfer cables clip the interference suppressor (in scope of delivery) on the cable cores (not on the outer insulation of the cable!). Place the cable screen out of the interference suppressor and connect it to PE (brass screw with bolt, top right in the connection compartment) ( →...
  • Page 16: Switching Contacts

    Wiring StamoLys CA 71 MN 4.2.3 Two-channel version Connection Designation Function Leak Liquid has collected in the drip pan Signal inputs No sample No sample available, measurement is not started, display flashes AV 1 - 1 Alarm value 1, channel 1 exceeded or undershot...
  • Page 17: Serial Interface

    StamoLys CA 71 MN Wiring Two-channel version Connection Terminal connection for Terminal connection for Terminal connection for condition fulfilled condition not fulfilled power off AV 1 - 1 AV 1 - 2 AV 2 - 1 AV 2 - 2 Fault Channel ½...
  • Page 18: Post-Connection Check

    Wiring StamoLys CA 71 MN Post-connection check Carry out the following checks after electrical connection: Device status and specifications Note Is the analyzer or cable externally undamaged? Visual inspection Electrical connection Note Does the supply voltage correspond to the data on the nameplate? 230 V AC / 50 Hz 115 V AC / 60 Hz...
  • Page 19: Operation

    StamoLys CA 71 MN Operation Operation Operation and commissioning The following chapters provide you with information on the analyzer’s operating elements and explain how to make settings. In chapter “Commissioning” you will find the procedure for initial start-up and for daily analyzer operation.
  • Page 20 Operation StamoLys CA 71 MN 5.3.1 Main menu Access the main menu by holding down the key until “AUTO MEASURING” is displayed. For the main menu options and information about them, please see the following table. Selection Display Info Calibration, measurement, flushing time-controlled...
  • Page 21 StamoLys CA 71 MN Operation 5.3.3 CONFIGURATION Note! Some settings that can be made in this menu affect the defaults in the PARAMETER ENTRY menu. In view of this, complete the CONFIGURATION menu first during initial start-up. Option Range of adjustment...
  • Page 22 Operation StamoLys CA 71 MN Option Range of adjustment Display Info (default settings in bold) Selection for the scope of channel 1 measuring range. If the concentration measuring range is Analog output 1 Analog output 1 0 ... 5 mg/l, this corresponds to 0 mg/l either 4 mA 4- 20 mA or 0 mA.
  • Page 23 StamoLys CA 71 MN Operation 5.3.4 PARAMETER ENTRY Note! In the following table and in the tables in the next chapter, example images can be found for each option under "Display". In addition to the numerical values, the parameter is also displayed in some options. This is not shown in the images. Moreover, individual numerical values in the images can differ from the actual settings.
  • Page 24 Operation StamoLys CA 71 MN Option Range of adjustment Display Info (default settings in bold) Time of 1st calibration (DD.MM.YY, time hh.mm). After each change the instrument does not wait for the calibration interval. If the calibration is to start immediately, set the time in the past.
  • Page 25 StamoLys CA 71 MN Operation 5.3.5 LANGUAGE The following languages are available: • Deutsch • English • Français • Nederlands • Suomi • Magyar • Polski • Italiano. 5.3.6 ERROR DISPLAY Note! • This menu is a "Read-Only-Menu". • You can find the individual error messages, their meaning and solutions to problems in chapter "Trouble-shooting instructions".
  • Page 26: Calibration

    Operation StamoLys CA 71 MN 5.3.8 DATA STORAGE-Measured values Note! Two menus, "DATA MEMORY 1" and "DATA MEMORY 2", are only for the two-channel version. In the one-channel version there is only one menu "DATA MEMORY". Selection Display Info The data memory contains the last 1024 concentration measured values with date and time.
  • Page 27 StamoLys CA 71 MN Operation Measuring range Concentration [mg/l] Frequency [Hz] Manganese, lower measuring range 1 ... 150 µg/l MN-A 15.0 30.0 45.0 60.0 75.0 90.0 105.0 120.0 1233 150.0 1772 Manganese, upper measuring range 10 ... 2000 µg/l MN-B...
  • Page 28: Commissioning

    Commissioning StamoLys CA 71 MN Commissioning Function check Warning! • Check that all connections have been made correctly. Check, in particular, that all hose connections are secure, so that no leaks occur. • Ensure that the mains voltage corresponds to the voltage specified on the nameplate.
  • Page 29 StamoLys CA 71 MN Commissioning The following summary presents procedures carried out in the device and the intervals you have programmed: Function Duration [s] Range of adjustment Measurement Flushing (sample) 3 x 15 Delay to sample 20 ... 300 CONFIGURATION / "Delay to sample"...
  • Page 30: Maintenance

    Maintenance StamoLys CA 71 MN " Maintenance Caution! You must not carry out any procedures not listed in the following chapters, yourself. This work must only be carried out by the E+H Service. Note! Please, find accessories and wear parts in chapter "Accessories".
  • Page 31: Replacing Reagents

    StamoLys CA 71 MN Maintenance Replacing reagents Warning! • There is a danger of crushing limbs at doors, inserts and pump heads. • Refer to the warning instructions in the safety data sheets when handling reagents. Wear protective clothing, gloves and goggles.
  • Page 32: Replacing Pump Hoses

    Maintenance StamoLys CA 71 MN Replacing pump hoses Warning! When removing hoses from the hose nozzles, beware of reagent splashing. For this reason, wear protective gloves and goggles. The peristaltic pumps used for the analyzer convey the medium in a combination of vacuum and displacement pump.
  • Page 33: Replacing The Static Mixer

    StamoLys CA 71 MN Maintenance C07-CA71xxx-00-08-00-xx-005.eps Fig. 14: Valves and valve hoses Valve 1 Valve 2 To the pump Y-piece, Y-piece, connecting hose to valve 1, behind it Hose valve 2, front, standard Hose valve 2 back, cleaning agent Hose valve 1 front, sample...
  • Page 34: Cleaning

    Maintenance StamoLys CA 71 MN " Caution! Do not under any circumstances touch the optical window of the cell with your fingers! Otherwise, traces of grease remain on the optical surfaces. This can lead to corrupted measured values. Connect the cell to the hoses such that the sample is fed in from below.
  • Page 35: Accessories

    StamoLys CA 71 MN Accessories Accessories Collecting vessel • for sampling from pressurized systems • results in an unpressurized continuous sample stream ❑Collecting vessel without level measurement; order no. 51512088 ❑Collecting vessel with level measurement (conductive); order no. 51512089 Reagents, cleaner, standard solution ❑Reagent set, 1 l MN1+MN2+MN3 each;...
  • Page 36: Trouble-Shooting

    Trouble-shooting StamoLys CA 71 MN Trouble-shooting Trouble-shooting instructions Although the analyzer is not very prone to faults due to its simple assembly, problems can, of course, not be completely ruled out. Possible errors, their causes and their possible remedies are listed below.
  • Page 37: Process Errors Without Messages

    StamoLys CA 71 MN Trouble-shooting Process errors without messages Error message Possible cause Tests and / or corrective measures Reagents Simple check: Add about 20 ml of standard solution with about 1 ml of reagent in a vessel. If it contaminated or aged does not change colour after max.
  • Page 38: Spare Parts

    Trouble-shooting StamoLys CA 71 MN Error message Possible cause Tests and / or corrective measures Time of 1st The date must be between 01.01.1996 and the current date. measurement not "Measurement" reached display flashes Interval not expired Change parameters. Time of 1st calibration The date must be between 01.01.1996 and the current date.
  • Page 39: Return

    51512071 – MN-B 51512163 Return If the device requires repair, please send it cleaned to the appropriate Endress+Hauser sales office. Please use the original packaging, if possible. Please enclose the completed Dangerous Goods sheet (copy the second last page of these Operating Instructions) with the packaging and the transportation documents.
  • Page 40: Technical Data

    Technical data StamoLys CA 71 MN Technical data 10.1 Input Measured variable Mn [µg/l] Measuring range 1 ... 150 µg/l (MN-A) 10 ... 2000 µg/l (MN-B) Wave length 565 nm (MN-A) 502 nm (MN-B) Reference wave length 880 nm 10.2...
  • Page 41: Performance Characteristics

    StamoLys CA 71 MN Technical data 10.4 Performance characteristics Time between two measurements: Response time t reaction time + rinse time + waiting time + rinse again time + filling time (minimum waiting time = 0 min) Maximum measured error...
  • Page 42: Appendix

    Appendix StamoLys CA 71 MN Appendix 11.1 Operating matrix One-channel version AUTO Calibration Measuring Waiting Flushing MEASURING Measuring Measuring Measuring Calibration Alarm value Alarm value PARAMETER range start range end interval Measurem. interval alibration ENTRY Concentrat. Code Default Measuring Calibration...
  • Page 43 StamoLys CA 71 MN Appendix Standard Flushing Flushing solution Flushing interval time Analog Alarm value Alarm value Error act. Date/ Calibrate Frequency output contact time offset offset Endress+Hauser...
  • Page 44 Appendix StamoLys CA 71 MN Two-channel version AUTO Calibration Measuring Flushing Waiting MEASURING Measuring Measuring Measuring Measuring Alarm value Alarm value Alarm value Alarm value PARAMETER range start1 range start2 range end 1 range end 2 ENTRY Measuring Code Default Calibration Concentr.
  • Page 45 StamoLys CA 71 MN Appendix Measuring 1 st Calibration Calibration Flushing Flushing Measurem. interval Channel 1 Channel 2 interval solution Flushing interval alibration time Analog Analog Frequency Alarm value Alarm value Alarm value Alarm value Error act. Date/ Calibrate output 1...
  • Page 46: Ordering Forms

    Appendix StamoLys CA 71 MN 11.2 Ordering forms to Fax no: Telefax for chemicals ordering to (adress of your E+H sales centre, see OM backpage) from (invoice adress) Company: Concern: Street: Zip code / Town: Telefax / Telephone: Adress for delivery (if not the above adress)
  • Page 47 StamoLys CA 71 MN Appendix to Fax no: Telefax for wear parts ordering to (adress of your E+H sales centre, see OM backpage) from (invoice adress) Company: Concern: Street: Zip code / Town: Telefax / Telephone: Adress for delivery (if not the above adress)
  • Page 48: Analyzer Settings

    Appendix StamoLys CA 71 MN 11.3 Analyzer settings Place: Type: Serial no. Analyzer: Serial no. Photometer: Software version: Date: Photometer Type: Measuring unit: Calibration factor: ❑ mg/l ❑ µg/l c-offset: Dilution: Delay to sample: ❑ 0-20 mA ❑ 4-20 mA Analog output: ❑...
  • Page 49 StamoLys CA 71 MN Appendix Submenu Error mask: MB >: MBE: Rinse again: Filling time: Reaction time: U/min: K floating mean: Points mg/l / µg/l F 1: mg/l / µg/l F 2: mg/l / µg/l F 3: mg/l / µg/l F 4: mg/l / µg/l...
  • Page 50: Maintenance Schedule

    Appendix StamoLys CA 71 MN 11.4 Maintenance schedule Form Maintenance schedule for Analyser Nr....weekly ⇒ Check and note calibration factor ⇒ visible control (Soiling or blinding, pump tubings, reagent, sample inlet etc.) done KW 1 KW 2 KW 3...
  • Page 51 StamoLys CA 71 MN Appendix Endress+Hauser...
  • Page 52 Appendix StamoLys CA 71 MN Endress+Hauser...
  • Page 53: Index

    StamoLys CA 71 MN Index Accessories ....... 36 Main menu ....... . . 21 AUTO MEASURING .
  • Page 54 StamoLys CA 71 MN Safety icons ....... . 6 Sample line....... . 10 Scope of delivery .
  • Page 55 Declaration of contamination Dear customer, Because of legal determinations and for the safety of our employes and operating equipment we need this “Declaration of contamination” with your signature before your order can be handled. Please put the completely filled in declaration to the instrument and to the shipping documents in any case. Add also safety sheets and/or specific handling instructions if necessary.
  • Page 56 Mexico – México, D.F Croatia – Zagreb Tel. (3) 94 40 80, Fax (9) 54 80 38 ❑ Endress+Hauser (México), S.A. de C.V. ❑ Endress+Hauser GmbH+Co. Sweden – Sollentuna Tel. (5) 5 55 68 24 07, Fax (5) 5 55 68 74 59 Malaysia –...

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