Endress+Hauser StamoLys CA 71 FE Operating Instructions Manual

Endress+Hauser StamoLys CA 71 FE Operating Instructions Manual

Iron analyzer

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BA 360C/07/en/01.03
51512324
Valid of:
Software version 5.0
Quality made by
Endress+Hauser
ISO 9001
StamoLys CA 71 FE
Iron Analyzer
Operating Instructions

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Summary of Contents for Endress+Hauser StamoLys CA 71 FE

  • Page 1 StamoLys CA 71 FE BA 360C/07/en/01.03 51512324 Valid of: Iron Analyzer Software version 5.0 Operating Instructions Quality made by Endress+Hauser ISO 9001...
  • Page 3: Table Of Contents

    Hose cleaner ......35 Additional accessories ....35 Endress+Hauser...
  • Page 4: Safety Instructions

    • Installation instructions • Local prevailing standards and regulations. Return If the analyzer has to be repaired, please return it cleaned to the Endress+Hauser sales centre responsible. Please use the original packaging, if possible. Please enclose the completed Dangerous Goods sheet (copy the second last page of these Operating instructions) with the packaging and also the shipping documents.
  • Page 5: Notes On Safety Icons And Symbols

    This symbol alerts you to hazards. They can cause serious damage to the instrument or to persons if ignored. " Caution! This symbol alerts you to possible faults which could arise from incorrect operation. They could cause damage to the instrument if ignored. Note! This symbol indicates important items of information. Endress+Hauser...
  • Page 6: Identification

    With collecting vessel with level measurement (one-channel version only) Housing version Without housing With GFK housing With stainless steel 1.4301 (AISI 304) housing Communication 0/4 ... 20 mA, RS 232 Additional equipment Quality certificate CA 71 FE - complete order code Endress+Hauser...
  • Page 7: Scope Of Delivery

    The product meets the legal requirements of the harmonised European standards. Endress+Hauser confirms compliance with the standards by affixing the symbol. 2.3.2 Manufacturer certificate Quality certificate With the certificate Endress+Hauser confirms compliance with all technical regulations and the successful testing individually for your product. Endress+Hauser...
  • Page 8: Installation

    The original packaging offers the best protection. Also, keep to the approved ambient conditions (see "Technical data"). • If you have any questions, please contact your supplier or your Endress+Hauser sales centre responsible (see back page of these Operating Instructions).
  • Page 9 Connecting the sample line C07-CA71xxx-11-08-00-xx-001.eps C07-CA71xxx-06-08-02-en-003.eps Fig. 4: Collecting vessel at analyzer (optionally) Fig. 5: Collecting vessel dimensions Ventilation variable, freely adjustable dimensions Sample inlet from sampling Sampling for analyzer Collecting vessel Analyzer outlet Electrical connections Sample overflow Analyzer sample inlet Endress+Hauser...
  • Page 10 Pull the marked pipe (position 3) downwards due to your application (1, 2 or 3 analyzers). C07-CA71xxx-11-08-00-xx-004.eps C07-CA71xxx-11-08-00-xx-003.eps C07-CA71XXx-11-08-02-xx-001.eps Fig. 6: One Analyzer Fig. 7: Two analyzers Fig. 8: Three analyzers M 3x12 (0.47") M 3x12 (0.47") M 3x12 (0.47") M 3x35 (1.38") M 3x20 (0.79") Mark 3 Mark 1 Mark 2 Endress+Hauser...
  • Page 11: Installation Instructions

    – Sample conditioning using ultrafiltration for heavily soiled media, e.g. from the primary settling tank. For questions regarding sample conditioning and its automation, please contact Endress+Hauser Service or the Endress+Hauser Sales Centre responsible for your region. Connect the tubes from canisters containing reagents, standard and cleaning...
  • Page 12: Installation Examples

    Collecting vessel overflow Sampling lines T-pieces Post-installation check • After installation, check that all connections are fitted tightly and are leakage resistant. • Ensure that the hoses can not be removed without effort. • Check all hoses for damage. Endress+Hauser...
  • Page 13: Wiring

    • Ensure before beginning the connection work that there is no voltage at the power cable. 4.1.1 Quick wiring guide Note! The device does not have a mains switch. Therefore, it is advantageous to have a fused socket near to the device. C07-CA71xxxx-04-08-00-a2-001.eps Fig. 11: Connection sticker CA 71 Endress+Hauser...
  • Page 14 • If there is a 24 V voltage at terminal 57, the analyzer will not begin measurement (sample not ready). To start measurement, the voltage must stay at 0 V for at least 5 seconds. Endress+Hauser...
  • Page 15: Signal Connection

    Alarm value 1 exceeded or undershot Signal outputs AV 2 Alarm value 2 exceeded or undershot Fault Retrieves error message using operation menu l-1 channel 1 0 or 4 mA = measuring range start Analog output 20 mA = measuring range end Endress+Hauser...
  • Page 16: Switching Contacts

    0 V = channel 1 Channel selection 24 V = channel 2 Alternative selection Switching contacts One-channel version Connection Terminal connection for Terminal connection for Terminal connection for condition fulfilled condition not fulfilled power off AV 1 AV 2 Fault Unassigned Endress+Hauser...
  • Page 17: Serial Interface

    The following commands can be sent from the PC, in order to read out data: • "D" = Data memory-Measured values • "C" = Data memory-Calibration factors • "S" = Setup (parameter entry, configuration...) • "F" = Frequency (current) Endress+Hauser...
  • Page 18: Post-Connection Check

    Browse to the next current values (4, 12, 20 mA, depending on the setting). Check that the respective current values are also on your PLC, PCS or your data logger. If the values are not there, check the terminal assignment for analogue output 1 or 2. Endress+Hauser...
  • Page 19: Operation

    In chapter “Commissioning” you will find the procedure for initial start-up and for daily analyzer operation. Display and operating elements M CE RS 232 ENDRESS+HAUSER STAMOLYS CA 71 C07-CA71xxx-19-08-00-xx-005.eps Fig. 13: CA 71 display and operating elements LED (measured value)
  • Page 20 • the time of the first measurement has not yet been reached or • the measuring interval has not yet expired. Note! "Measuring" flashes when the analyzer is ready for the next measurement but has not yet received the enable signal from the sample collector or the sample conditioning unit. Endress+Hauser...
  • Page 21 Delay to sample Delay to sample 80 s 80 s there is definitely only fresh sample in the mixer. If there is sufficient sample available, select the highest possible value. Endress+Hauser...
  • Page 22 Calibrate off s Calibrate offset yes / no yes: K no: E measurement for compensating the reagent’s inherent colour. – 5000 ... +5000 f -Off set [Hz ] Frequency offset Manually changing the frequency offset. Endress+Hauser...
  • Page 23 Number of measurements at channel 1 before Channel 1 switching to channel 2. Frequency of Two-channel version only! 0 ... 9 n* Channel 2: measurement Number of measurements at channel 2 before Channel 2 switching to channel 1. Endress+Hauser...
  • Page 24 • Always synchronise calibration and flushing time. • Carry out flushing with standard cleaning solution approx. 3-4 hours before the next calibration. Flushing with special cleaning solution (e.g. hydrochloric acid) has a lasting effect on calibration. Therefore, carry out this cleaning 3-4 hours after calibration. Endress+Hauser...
  • Page 25 Signal frequency of the photometer The reagent and sample pumps can be switched on together, so that they run in the same ratio as for Mixture filling the sample-reagent mixture in measurement mode. Selection between s (stop) and g (go). Endress+Hauser...
  • Page 26: Calibration

    The following table provides an overview of the standard calibration data (frequency-offset = 0). Note! Compare these values to your own data. After changes in the CONFIGURATION menu and in case of software updates, you can check and, if necessary, change the calibration data in the sub-menu. Endress+Hauser...
  • Page 27 The rinse must be performed 3-4 hours before the next calibration. Proceed as described above to change the setting for the time of the 1st calibration. After changing to measuring mode, the analyzer automatically begins measuring, rinsing and calibrating at the defined times. Endress+Hauser...
  • Page 28: Commissioning

    The analyzer starts the "Calibration", "Measurement", and "Flushing" procedures automatically (triggered by control signal or integrated timer) in accordance with the device parameters that you have set (1st calibration, 1st measurement, 1st flushing times and the respective intervals control the temporal procedure). Endress+Hauser...
  • Page 29 T-connector. Switch P1 back "off". Note! For the two-channel version, valve V3 must be set additionally for switch-over between channel 1 and channel 2. Now proceed as with dry commissioning (from step 2). Endress+Hauser...
  • Page 30: Maintenance

    6 months – Replace pump hoses – see chapter "Replacing pump hoses" – Replace valve hoses Note! Whenever working on the reagent hoses, the hoses must be disconnected from the canisters, in order to prevent contamination of the reagents. Endress+Hauser...
  • Page 31: Replacing Reagents

    "s". Determine the reagent blank value by using destilled water as a sample (see chapter "Calibration"). Enter the measured value as the frequency offset (CONFIGURATION / "Frequency offset"). Then carry out a calibration (see chapter "Calibration"). Endress+Hauser...
  • Page 32: Replacing Pump Hoses

    Replace the new pump hoses in the reverse sequence of operations. Ensure that the hoses are connected correctly ( → Fig. 14). After installation, refill the hoses with sample, standard or cleaning agent (SERVICE). Carry out a calibration (PARAMETER ENTRY). Endress+Hauser...
  • Page 33: Replacing The Static Mixer

    Unscrew the four screws on the photometer housing and remove it. Unscrew the four screws on the side of the photometer, on which there is no ribbon cable. Separate the photometer’s electronics from each other. Take out the cell and remove the hoses. Insert the new cell. Endress+Hauser...
  • Page 34: Cleaning

    Remove hoses from the water and allow the pumps to run until the hoses are completely dry. If you are using a continuous sample supply, disconnect sampling line. Flush sampling hoses with clean water. Slacken hose clips and remove pump hoses from the contact rollers. Endress+Hauser...
  • Page 35: Accessories

    CAV 740-1A ❑Interference suppressor for control, power and signal lines order no. 51512800 ❑Silicon spray order no. 51504155 ❑Valve set, 2 pieces, for two-channel version order no. 51512234 ❑Upgrade kit for upgrading from one-channel to two-channel version order no. 51512640 Endress+Hauser...
  • Page 36: Trouble-Shooting

    Replace defective components and clean and dry the CA 70 or those components Spillage error affected by the leak. Photometer defective Inform E+H Service No measuring signal Electrical connection Check all electrical connections. Fuse defective Replace fuse F4 or F5 (medium time-lag 0.2 A) Endress+Hauser...
  • Page 37: Process Errors Without Messages

    See "Spillage error" error message Leak sensor Interrupt contact between two leak sensors (pins 67-66) bypassed Pumps fail to run Fuse Check all fuses and replace if necessary. Pump defective E+H-Service Measurement does Leak on photometer E+H-Service not start Endress+Hauser...
  • Page 38: Spare Parts

    Fig. 15: Overview parts Sample input two-channel version Reagent 1 canister Standards and reagent canisters Standard solution canister Collecting vessel Sample Fig. 15 shows the components of the analyzer. Please, take the spare parts order numbers from the following sections. Endress+Hauser...
  • Page 39: Return

    – FE-B / FE-C 51512070 Return If the device requires repair, please send it cleaned to the appropriate Endress+Hauser sales office. Please use the original packaging, if possible. Please enclose the completed Dangerous Goods sheet (copy the second last page of these Operating Instructions) with the packaging and the transportation documents.
  • Page 40: Technical Data

    50 VA Current consumption ca. 0.2 A at 230 V ca. 0.5 A at 115 V Fuses 1 x time-lag 0.5 A for electronics 2 x medium time-lag 0.2 A for photometer 1 x time-lag 0.1 A for motors Endress+Hauser...
  • Page 41: Performance Characteristics

    Weight Stainless steel approx. 33 kg (72.8 lb) housing Housing Stainless steel 1.4301 (AISI 304) or GFK ® Front windows Plexiglass ® ® Materials Endless hose C-Flex , Norprene ® ® Pump hose Tygon , Viton ® Valves Tygon Endress+Hauser...
  • Page 42: Appendix

    Calibration Delay to CONFI- Photometer Dilution offset number settings unit factor sample GURATION LANGUAGE Deutsch English Français Nederlands Suomi Magyar Polski Italiano ERROR Error DISPLAY messages Pumps SERVICE Frequency Mixture and valves DATA Measured Output Clear data MEMORY values Endress+Hauser...
  • Page 43 StamoLys CA 71FE Appendix Standard Flushing Flushing solution Flushing interval time Analog Alarm value Alarm value Error act. Date/ Calibrate Frequency output contact time offset offset Endress+Hauser...
  • Page 44 GURATION Deutsch English Français Magyar Italiano LANGUAGE Nederlands Suomi Polski ERROR Error DISPLAY messages Pumps SERVICE Frequency Mixture and valves DATA Measured Output Clear data MEMORY 1 values DATA Measured Output Clear data MEMORY 2 values Endress+Hauser...
  • Page 45 Flushing interval alibration time Analog Analog Frequency Alarm value Alarm value Alarm value Alarm value Error act. Date/ Calibrate output 1 output 2 1 - 1 2 - 1 1 - 2 2 - 2 contact time offset offset Endress+Hauser...
  • Page 46: Ordering Forms

    Alkaline cleaning agent P3-Ultrasil 130, 5 l CAY747-V01AAE Acidic cleaning agent P3-Ultrasil 130, 100 ml CAY747-V10AAE Acidic cleaning agent P3-Ultrasil 130, 1 l CAY747-V50AAE Acidic cleaning agent P3-Ultrasil 130, 5 l Place Date Signature Delivery one week after orders received. Delivery is unpaid. Endress+Hauser...
  • Page 47 51512088 Photometer Type Silicon spray 51504155 Cleaning syringe 51503943 Please, take the photometer type and the order no. from chapter "Trouble-shooting/Spare parts" and write it down here! Place Date Signature Delivery one week after orders received. Delivery is unpaid. Endress+Hauser...
  • Page 48: Analyzer Settings

    ❑ mg/l ❑ µg/l Measuring range end: ❑ mg/l ❑ µg/l AV 1: ❑ mg/l ❑ µg/l AV 2: 1st measuring: Measuring interval: 1st calibration: Calibration interval: ❑ mg/l ❑ µg/l Calibration solution: 1st rinsing: Rinse interval: Rinse time: Endress+Hauser...
  • Page 49 / µg/l F 4: mg/l / µg/l F 5: mg/l / µg/l F 6: mg/l / µg/l F 7: mg/l / µg/l F 8: mg/l / µg/l F 9: C10: mg/l / µg/l F 10: Date: Service technician: Endress+Hauser...
  • Page 50: Maintenance Schedule

    ⇒ turn on the pump tubings in the hose holder unit (monthly) , change (all 6 month) Attention: Whenever working on the reagent hoses, the hoses must be disconnected from the canisters and the T-connectors near the reagent pump, in order to prevent contamination of the reagents. ⇒ cleaning drain lines done Mär date C07-CA71XXx-16-08-00-en-006.pdf Endress+Hauser...
  • Page 51 StamoLys CA 71FE Appendix Endress+Hauser...
  • Page 52 Appendix StamoLys CA 71FE Endress+Hauser...
  • Page 53: Index

    Interference suppressor ..... . 15 LANGUAGE ....... 25 Endress+Hauser...
  • Page 54 Valves........25 Wiring Connection sticker ..... . . 13 Endress+Hauser...
  • Page 55 Declaration of contamination Dear customer, Because of legal determinations and for the safety of our employes and operating equipment we need this “Declaration of contamination” with your signature before your order can be handled. Please put the completely filled in declaration to the instrument and to the shipping documents in any case. Add also safety sheets and/or specific handling instructions if necessary.
  • Page 56 Mexico – México, D.F Croatia – Zagreb Tel. (3) 94 40 80, Fax (9) 54 80 38 ❑ Endress+Hauser (México), S.A. de C.V. ❑ Endress+Hauser GmbH+Co. Sweden – Sollentuna Tel. (5) 5 55 68 24 07, Fax (5) 5 55 68 74 59 Malaysia –...

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