Analyzer for photometric determination of phosphate (68 pages)
Summary of Contents for Endress+Hauser StamoLys CA 71 FE
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StamoLys CA 71 FE BA 360C/07/en/01.03 51512324 Valid of: Iron Analyzer Software version 5.0 Operating Instructions Quality made by Endress+Hauser ISO 9001...
• Installation instructions • Local prevailing standards and regulations. Return If the analyzer has to be repaired, please return it cleaned to the Endress+Hauser sales centre responsible. Please use the original packaging, if possible. Please enclose the completed Dangerous Goods sheet (copy the second last page of these Operating instructions) with the packaging and also the shipping documents.
This symbol alerts you to hazards. They can cause serious damage to the instrument or to persons if ignored. " Caution! This symbol alerts you to possible faults which could arise from incorrect operation. They could cause damage to the instrument if ignored. Note! This symbol indicates important items of information. Endress+Hauser...
With collecting vessel with level measurement (one-channel version only) Housing version Without housing With GFK housing With stainless steel 1.4301 (AISI 304) housing Communication 0/4 ... 20 mA, RS 232 Additional equipment Quality certificate CA 71 FE - complete order code Endress+Hauser...
The product meets the legal requirements of the harmonised European standards. Endress+Hauser confirms compliance with the standards by affixing the symbol. 2.3.2 Manufacturer certificate Quality certificate With the certificate Endress+Hauser confirms compliance with all technical regulations and the successful testing individually for your product. Endress+Hauser...
The original packaging offers the best protection. Also, keep to the approved ambient conditions (see "Technical data"). • If you have any questions, please contact your supplier or your Endress+Hauser sales centre responsible (see back page of these Operating Instructions).
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Connecting the sample line C07-CA71xxx-11-08-00-xx-001.eps C07-CA71xxx-06-08-02-en-003.eps Fig. 4: Collecting vessel at analyzer (optionally) Fig. 5: Collecting vessel dimensions Ventilation variable, freely adjustable dimensions Sample inlet from sampling Sampling for analyzer Collecting vessel Analyzer outlet Electrical connections Sample overflow Analyzer sample inlet Endress+Hauser...
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Pull the marked pipe (position 3) downwards due to your application (1, 2 or 3 analyzers). C07-CA71xxx-11-08-00-xx-004.eps C07-CA71xxx-11-08-00-xx-003.eps C07-CA71XXx-11-08-02-xx-001.eps Fig. 6: One Analyzer Fig. 7: Two analyzers Fig. 8: Three analyzers M 3x12 (0.47") M 3x12 (0.47") M 3x12 (0.47") M 3x35 (1.38") M 3x20 (0.79") Mark 3 Mark 1 Mark 2 Endress+Hauser...
– Sample conditioning using ultrafiltration for heavily soiled media, e.g. from the primary settling tank. For questions regarding sample conditioning and its automation, please contact Endress+Hauser Service or the Endress+Hauser Sales Centre responsible for your region. Connect the tubes from canisters containing reagents, standard and cleaning...
Collecting vessel overflow Sampling lines T-pieces Post-installation check • After installation, check that all connections are fitted tightly and are leakage resistant. • Ensure that the hoses can not be removed without effort. • Check all hoses for damage. Endress+Hauser...
• Ensure before beginning the connection work that there is no voltage at the power cable. 4.1.1 Quick wiring guide Note! The device does not have a mains switch. Therefore, it is advantageous to have a fused socket near to the device. C07-CA71xxxx-04-08-00-a2-001.eps Fig. 11: Connection sticker CA 71 Endress+Hauser...
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• If there is a 24 V voltage at terminal 57, the analyzer will not begin measurement (sample not ready). To start measurement, the voltage must stay at 0 V for at least 5 seconds. Endress+Hauser...
Alarm value 1 exceeded or undershot Signal outputs AV 2 Alarm value 2 exceeded or undershot Fault Retrieves error message using operation menu l-1 channel 1 0 or 4 mA = measuring range start Analog output 20 mA = measuring range end Endress+Hauser...
0 V = channel 1 Channel selection 24 V = channel 2 Alternative selection Switching contacts One-channel version Connection Terminal connection for Terminal connection for Terminal connection for condition fulfilled condition not fulfilled power off AV 1 AV 2 Fault Unassigned Endress+Hauser...
The following commands can be sent from the PC, in order to read out data: • "D" = Data memory-Measured values • "C" = Data memory-Calibration factors • "S" = Setup (parameter entry, configuration...) • "F" = Frequency (current) Endress+Hauser...
Browse to the next current values (4, 12, 20 mA, depending on the setting). Check that the respective current values are also on your PLC, PCS or your data logger. If the values are not there, check the terminal assignment for analogue output 1 or 2. Endress+Hauser...
In chapter “Commissioning” you will find the procedure for initial start-up and for daily analyzer operation. Display and operating elements M CE RS 232 ENDRESS+HAUSER STAMOLYS CA 71 C07-CA71xxx-19-08-00-xx-005.eps Fig. 13: CA 71 display and operating elements LED (measured value)
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• the time of the first measurement has not yet been reached or • the measuring interval has not yet expired. Note! "Measuring" flashes when the analyzer is ready for the next measurement but has not yet received the enable signal from the sample collector or the sample conditioning unit. Endress+Hauser...
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Delay to sample Delay to sample 80 s 80 s there is definitely only fresh sample in the mixer. If there is sufficient sample available, select the highest possible value. Endress+Hauser...
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Calibrate off s Calibrate offset yes / no yes: K no: E measurement for compensating the reagent’s inherent colour. – 5000 ... +5000 f -Off set [Hz ] Frequency offset Manually changing the frequency offset. Endress+Hauser...
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Number of measurements at channel 1 before Channel 1 switching to channel 2. Frequency of Two-channel version only! 0 ... 9 n* Channel 2: measurement Number of measurements at channel 2 before Channel 2 switching to channel 1. Endress+Hauser...
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• Always synchronise calibration and flushing time. • Carry out flushing with standard cleaning solution approx. 3-4 hours before the next calibration. Flushing with special cleaning solution (e.g. hydrochloric acid) has a lasting effect on calibration. Therefore, carry out this cleaning 3-4 hours after calibration. Endress+Hauser...
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Signal frequency of the photometer The reagent and sample pumps can be switched on together, so that they run in the same ratio as for Mixture filling the sample-reagent mixture in measurement mode. Selection between s (stop) and g (go). Endress+Hauser...
The following table provides an overview of the standard calibration data (frequency-offset = 0). Note! Compare these values to your own data. After changes in the CONFIGURATION menu and in case of software updates, you can check and, if necessary, change the calibration data in the sub-menu. Endress+Hauser...
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The rinse must be performed 3-4 hours before the next calibration. Proceed as described above to change the setting for the time of the 1st calibration. After changing to measuring mode, the analyzer automatically begins measuring, rinsing and calibrating at the defined times. Endress+Hauser...
The analyzer starts the "Calibration", "Measurement", and "Flushing" procedures automatically (triggered by control signal or integrated timer) in accordance with the device parameters that you have set (1st calibration, 1st measurement, 1st flushing times and the respective intervals control the temporal procedure). Endress+Hauser...
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T-connector. Switch P1 back "off". Note! For the two-channel version, valve V3 must be set additionally for switch-over between channel 1 and channel 2. Now proceed as with dry commissioning (from step 2). Endress+Hauser...
6 months – Replace pump hoses – see chapter "Replacing pump hoses" – Replace valve hoses Note! Whenever working on the reagent hoses, the hoses must be disconnected from the canisters, in order to prevent contamination of the reagents. Endress+Hauser...
"s". Determine the reagent blank value by using destilled water as a sample (see chapter "Calibration"). Enter the measured value as the frequency offset (CONFIGURATION / "Frequency offset"). Then carry out a calibration (see chapter "Calibration"). Endress+Hauser...
Replace the new pump hoses in the reverse sequence of operations. Ensure that the hoses are connected correctly ( → Fig. 14). After installation, refill the hoses with sample, standard or cleaning agent (SERVICE). Carry out a calibration (PARAMETER ENTRY). Endress+Hauser...
Unscrew the four screws on the photometer housing and remove it. Unscrew the four screws on the side of the photometer, on which there is no ribbon cable. Separate the photometer’s electronics from each other. Take out the cell and remove the hoses. Insert the new cell. Endress+Hauser...
Remove hoses from the water and allow the pumps to run until the hoses are completely dry. If you are using a continuous sample supply, disconnect sampling line. Flush sampling hoses with clean water. Slacken hose clips and remove pump hoses from the contact rollers. Endress+Hauser...
CAV 740-1A ❑Interference suppressor for control, power and signal lines order no. 51512800 ❑Silicon spray order no. 51504155 ❑Valve set, 2 pieces, for two-channel version order no. 51512234 ❑Upgrade kit for upgrading from one-channel to two-channel version order no. 51512640 Endress+Hauser...
Replace defective components and clean and dry the CA 70 or those components Spillage error affected by the leak. Photometer defective Inform E+H Service No measuring signal Electrical connection Check all electrical connections. Fuse defective Replace fuse F4 or F5 (medium time-lag 0.2 A) Endress+Hauser...
See "Spillage error" error message Leak sensor Interrupt contact between two leak sensors (pins 67-66) bypassed Pumps fail to run Fuse Check all fuses and replace if necessary. Pump defective E+H-Service Measurement does Leak on photometer E+H-Service not start Endress+Hauser...
Fig. 15: Overview parts Sample input two-channel version Reagent 1 canister Standards and reagent canisters Standard solution canister Collecting vessel Sample Fig. 15 shows the components of the analyzer. Please, take the spare parts order numbers from the following sections. Endress+Hauser...
– FE-B / FE-C 51512070 Return If the device requires repair, please send it cleaned to the appropriate Endress+Hauser sales office. Please use the original packaging, if possible. Please enclose the completed Dangerous Goods sheet (copy the second last page of these Operating Instructions) with the packaging and the transportation documents.
50 VA Current consumption ca. 0.2 A at 230 V ca. 0.5 A at 115 V Fuses 1 x time-lag 0.5 A for electronics 2 x medium time-lag 0.2 A for photometer 1 x time-lag 0.1 A for motors Endress+Hauser...
Calibration Delay to CONFI- Photometer Dilution offset number settings unit factor sample GURATION LANGUAGE Deutsch English Français Nederlands Suomi Magyar Polski Italiano ERROR Error DISPLAY messages Pumps SERVICE Frequency Mixture and valves DATA Measured Output Clear data MEMORY values Endress+Hauser...
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StamoLys CA 71FE Appendix Standard Flushing Flushing solution Flushing interval time Analog Alarm value Alarm value Error act. Date/ Calibrate Frequency output contact time offset offset Endress+Hauser...
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GURATION Deutsch English Français Magyar Italiano LANGUAGE Nederlands Suomi Polski ERROR Error DISPLAY messages Pumps SERVICE Frequency Mixture and valves DATA Measured Output Clear data MEMORY 1 values DATA Measured Output Clear data MEMORY 2 values Endress+Hauser...
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Flushing interval alibration time Analog Analog Frequency Alarm value Alarm value Alarm value Alarm value Error act. Date/ Calibrate output 1 output 2 1 - 1 2 - 1 1 - 2 2 - 2 contact time offset offset Endress+Hauser...
Alkaline cleaning agent P3-Ultrasil 130, 5 l CAY747-V01AAE Acidic cleaning agent P3-Ultrasil 130, 100 ml CAY747-V10AAE Acidic cleaning agent P3-Ultrasil 130, 1 l CAY747-V50AAE Acidic cleaning agent P3-Ultrasil 130, 5 l Place Date Signature Delivery one week after orders received. Delivery is unpaid. Endress+Hauser...
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51512088 Photometer Type Silicon spray 51504155 Cleaning syringe 51503943 Please, take the photometer type and the order no. from chapter "Trouble-shooting/Spare parts" and write it down here! Place Date Signature Delivery one week after orders received. Delivery is unpaid. Endress+Hauser...
⇒ turn on the pump tubings in the hose holder unit (monthly) , change (all 6 month) Attention: Whenever working on the reagent hoses, the hoses must be disconnected from the canisters and the T-connectors near the reagent pump, in order to prevent contamination of the reagents. ⇒ cleaning drain lines done Mär date C07-CA71XXx-16-08-00-en-006.pdf Endress+Hauser...
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StamoLys CA 71FE Appendix Endress+Hauser...
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Appendix StamoLys CA 71FE Endress+Hauser...
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Declaration of contamination Dear customer, Because of legal determinations and for the safety of our employes and operating equipment we need this “Declaration of contamination” with your signature before your order can be handled. Please put the completely filled in declaration to the instrument and to the shipping documents in any case. Add also safety sheets and/or specific handling instructions if necessary.