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6.2
Calibration Standards
All hygroscopic chemicals in crystal form should be dried in an oven set at 105°C for 3
hours to remove any traces of absorbed water. All prepared solutions must be mixed
thoroughly with a magnetic stirrer or inverted manually at least ten times or until all
crystals are completely dissolved inside the solution.
Caution
The following compounds can be used to prepare calibration standard solutions in BioTector.
To prepare a 1000mgC/l Total Organic Carbon (TOC) standard solution, use one of the following:
Potassium Hydrogen Phthalate, C
solubility: 80 g/L at 20°C.
Acetic acid, C
2
all proportions.
Glucose, C
H
6
12
To prepare a 1000mgC/l Total Inorganic Carbon (TIC) standard solution, use one of the following:
Sodium Carbonate, CNa
Sodium Hydrogen Carbonate, CHNaO
Potassium Carbonate, CK
The quantity of concentrated chemical required to prepare stock calibration solutions
will change with the % purity of the chemical used. If the purity of the chemical is
different than the figures displayed above, the necessary quantity needs to be
recalculated from the purity of the chemical. See example in the following page.
Caution
Depending on the system analysis ranges (see System Range Data screen
calibration standard solutions. The required concentration of the calibration standard
solutions can be identified in Span Calibration menu.
As the sample pressure normalization (line equalization function) is not activated for
Calibration/Manual Valve, it is recommended that the calibration standard solution flask
is placed at the same height with the Sample Pump.
H
KO
8
5
H
O
, 2.51g (99.8% purity) in one liter of deionized water. Water solubility: Miscible in
4
2
O
, 2.53g (99% purity) in one liter of deionized water. Water solubility: 512g/L at 25°C.
6
O
, 8.84g (99.9% purity) in one liter of deionized water.
2
3
O
, 11.62g (99.0% purity) in one liter of deionized water.
2
3
System Range Data Screen
, 2.13g (99.9% purity) in one liter of deionized water. Water
4
, 7.04g (99.5% purity) in one liter of deionized water.
3
for details), every BioTector requires specific
2.2.3
Page 65
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