Hach BioTector B7000i User Manual
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Hach BioTector B7000i User Manual

Online toc analyzer
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Catalog Number: 10-MAT-1052
BioTector B7000i Online TOC Analyzer
USER MANUAL
September 2015, Edition 1
BS4Ai 05.00a
Dairy
© Copyright BioTector 2015. All rights reserved. Printed by BioTector. Printed in the Republic of Ireland.

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  • Page 1 Catalog Number: 10-MAT-1052 BioTector B7000i Online TOC Analyzer USER MANUAL September 2015, Edition 1 BS4Ai 05.00a Dairy © Copyright BioTector 2015. All rights reserved. Printed by BioTector. Printed in the Republic of Ireland.

  • Page 2: Table Of Contents

    Table of Contents SECTION 1 SAFETY PRECAUTIONS ................5 ............5 NFORMATION AND AFETY IGNS USED IN THE ANUAL ............ 6 RECAUTIONARY ABELS TTACHED TO THE NSTRUMENT ............8 ERTIFICATION ARKS TTACHED TO THE NSTRUMENT ................9 OTENTIAL YSTEM AFETY AZARDS 1.4.1 Ozone and Toxicity ........................
  • Page 3 SECTION 5 INSTALLATION ..................49 ..................49 ASIC YSTEM EQUIREMENTS ..................50 NPACKING AND NSTALLATION 5.2.1 Analyzer Dimensions and Mounting .................... 51 5.2.2 Wiring Power and Signal Terminals .................... 53 5.2.3 Wiring External Power Disconnection Switch ................55 5.2.4 System Fuse Specifications ......................56 .................
  • Page 4 8.3.5 Output Devices .......................... 127 8.3.6 Reaction Check ......................... 130 8.3.7 Result Integration ........................131 8.3.8 Fault Setup ..........................131 8.3.9 Fault Status ..........................133 8.3.10 CO2 Analyzer ........................134 8.3.11 Cooler Program ........................135 8.3.12 Ozone Destructor Program ....................136 8.3.13 Software Update ........................

  • Page 5: Safety Precautions

    Section 1 Safety Precautions Please read this manual before unpacking, setting up, or operating the BioTector. BioTector should only be used by qualified trained staff and for the purpose it is intended for. Do not use or install this equipment in any way other than the methods specified in this manual. The procedures and methods described in this manual are based on assuming the user have basic, fundamental background on electronics, chemistry and analyzer equipment.

  • Page 6: Precautionary Labels Attached To The Instrument

    Precautionary Labels Attached to the Instrument The labels and tags attached to the instrument are summarized below. Please read all labels and tags attached to the instrument. If not observed, personal injury or damage to the instrument could occur. This symbol, when displayed on the instrument, indicates that the user must gather the necessary operation and/or safety information given in the instruction manual.
  • Page 7 This symbol, when displayed on the instrument, indicates that the user must follow the necessary local, state and federal laws during the disposal of the display. Electrical equipment marked with this symbol may not be disposed of in European domestic or public disposal systems after 12 August 2005. In conformity with European local and national regulations (EU Directive 2002/96/EC), European electrical equipment users must now return old or end-of life equipment to the manufacturer for disposal at no charge to the...

  • Page 8: Certification Marks Attached To The Instrument

    Certification Marks Attached to the Instrument The certification marks attached to the instrument and their meanings are summarized below. This mark, which stands for European Conformity "Conformité Européene", indicates that “The instrument complies with the European product directives, health, safety environmental protection legislations”.

  • Page 9: Potential System Safety Hazards

    Potential System Safety Hazards The potential safety hazards, which are associated with a running BioTector system, are as follows:  Electrical hazards  Potentially hazardous chemicals  Oxygen gas and components generating Ozone gas Maintenance and operation should not be carried out unless personnel have been fully trained in the operation of the BioTector.

  • Page 10: Ozone And Toxicity

    Ozone and Toxicity 1.4.1 Ozone is found in gaseous form as a natural ingredient of the earth's atmosphere. It is not a poisonous chemical but a strong oxidizing chemical. Some of the chemical and physical properties of ozone are as follows: Terms Properties of Ozone (O...

  • Page 11: General Safety Precautions

    General Safety Precautions Please pay attention to all caution, warning and danger statements at all times. Non-observance of the safety instructions can result in serious personal injury, death or damage to the equipment. Therefore observe the following:  Only engineers trained by the manufacturer should carry out maintenance on the BioTector. ...

  • Page 12: Electrical And Burn Precautions

    1.5.1 Electrical and Burn Precautions BioTector contains electrical components operating under high voltages. Contact may result in electric shock and severe or fatal injury. DANGER During system installation, maintenance or servicing:  Isolate the system power lines before starting any work in the electronic enclosure. ...

  • Page 13: Carrier Gas And Exhaust Gas Precautions

    1.5.2 Carrier Gas and Exhaust Gas Precautions BioTector uses oxygen (O ) gas as the carrier gas during its operation. The oxygen gas must be free of carbon dioxide (CO ) and nitrogen (N ) gases. The average rate of oxygen consumption in BioTector is 22 L/hour (367 ml/min).

  • Page 14: Chemical Precautions

    1.5.3 Chemical Precautions A number of chemicals and compounds to be used with BioTector are listed in Section 6 Reagents and Calibration Standards. Some of these compounds are harmful, corrosive, acidic and oxidizing. Appropriate precautions must be taken when handling these chemicals or solutions prepared from these chemicals.

  • Page 15: Sample Stream Precautions

    1.5.4 Sample Stream Precautions The user is responsible to establish the potential hazard associated with each sample stream. Necessary precautions must be taken, to avoid physical contact with any harmful sample stream, which may contain chemical or biological hazards. System components and their composition, which come in contact with the sample liquid and possible volatile gases from the sample, are tabulated in table 1 below.

  • Page 16: Précautions Relatives Aux Échantillons

    1.5.4 Précautions relatives aux échantillons L’usager assume la responsabilité d’établir le danger possible que représente chaque échantillon. Il est essentiel de prendre les précautions voulues afin d’éviter le contact physique avec tout échantillon nocif qui pourrait présenter un danger chimique ou biologique. Le tableau 1 ci-dessous présente les composants de l’analyseur (et leur composition) qui entrent en contact avec l’échantillon liquide et les éventuels gaz volatiles émanant de l’échantillon.

  • Page 17: Operator's Manual

    Operator’s Manual Section 2 2.1 Software Screens and Software Menu Diagram The BioTector is equipped with a built-in microprocessor, which has been programmed to enable the user to control the instrument using just six buttons of its membrane keypad. By pressing the appropriate button, the user can move through the various levels of the software menu.
  • Page 18 Software Menu Diagram Page 18...

  • Page 19: Startup State

    2.1.1 Startup State When the BioTector is powered up, its LCD screen will automatically display the Analysis Data screen after a delay of 60 seconds. By pressing the ESCAPE key the user moves from the Analysis Data screen to the Analysis Graph screen. Pressing the ENTER key on the Analysis Graph screens brings the user back to the Analysis Data screen.

  • Page 20: Analysis Data Screen

    2.1.3 Analysis Data Screen B I O T E C T O R R U N N I N G 0 9 : 1 7 : 2 8 1 2 - 0 9 - 0 2 0 9 : 1 3 : 0 2 1 2 - 0 9 - 0 2 R E A C T I O N S T A R T...

  • Page 21: Analysis Graph Screen

    2.1.4 Analysis Graph Screen 1 0 1 . 5 [ k P a ] 0 9 : 1 7 : 2 8 1 2 - 0 9 - 0 2 T I C m g u 1 2 . 4 9 5 6 C O 2 T O C m g u 1 5 6 .

  • Page 22: Select Level Menu

    2.1.6 Select Level Menu S E L E C T L E V E L 0 9 : 1 7 : 2 8 1 2 - 0 9 - 0 2 1 < O P E R A T I O N C A L I B R A T I O N M A I N T E N A N C E The Select Level screen allows the user to access the operation, calibration and maintenance menus.

  • Page 23: Operation Menu

    Operation Menu Operation Menu Diagram Operation menu allows the user to start and stop the analyzer. Menus related to system operation are also accessed using this menu. 2.2.1 Start Stop The user can Start or Stop the BioTector using the Start Stop menu. 1.
  • Page 24 2. Start. This function starts the BioTector. When BioTector is started, the multi-stream operation sequence (if programmed) is reset. BioTector performs Ozone Purge, Pressure/Flow Test, Reactor Purge and Analyzer Purge sequences automatically before starting its analysis.  Ozone Purge sequence purges any residual ozone through the ozone destructor. ...

  • Page 25: Reagents Setup

    2.2.2 Reagents Setup This menu allows the user to access the Reagent menus. 1. Install New Reagents. Menu used to install and prime the reagents in the BioTector. Any “85_Reagents Low” and “20_No Reagents” warnings and notifications can also be reset in this menu. 2.

  • Page 26: Purge Reagents & Zero

    When all or the necessary reagents have been confirmed to be connected and reset in this menu, and when Start New Reagent Cycle is selected, the Install New Reagents cycle will be executed. It is the responsibility of the user to make sure that all reagent volumes are programmed correctly in Reagents Monitor menu, the reset of the reagents monitoring are carried out correctly in Install New Reagents menu and finally if necessary the Zero Calibration cycle is activated either with the Start New Reagent Cycle function in Install New Reagents menu or with the Run Zero Calibration function in Zero Calibration menu.

  • Page 27: Manual Program Menu

    2.2.4 Manual Program Menu M A N U A L P R O G R A M 0 9 : 1 7 : 2 8 1 2 - 0 9 - 0 2 1 < R U N A F T E R N E X T R E A C T I O N R U N...

  • Page 28: Reaction Archive Screen

    2.2.5 Reaction Archive Screen The Reaction Archive holds information on TIC, TOC, TC, VOC (in mgC/l), COD, BOD (in mgO/l), LPI (%), LP (l/h), Flow (m /h), stream valve, reaction range, start date & time and related analysis information for the last 9999 reactions depending on system analysis type and specific configuration settings.

  • Page 29: Fault Archive Menu

    2.2.6 Fault Archive Menu In the Fault Archive menu, the user can view the last 99 faults/warning/notification events logged in the system, confirm if these events are current or not, and acknowledge the current events. If the archive is full, then every new event overwrites the oldest one in the archive.

  • Page 30: Calibration Menu

    Calibration Menu Calibration menu allows the user to calibrate the analyzer. Zero and Span Calibration menus allow the user to run the zero and span calibration cycles for a single range or for all system ranges available. Calibration Menu Diagram ENTER PASSWORD CALIBRATION ZERO CALIBRATION...
  • Page 31 1. The Zero Adjust settings for each range are updated automatically by the system using the un- calibrated TOC measurement (not the results seen on the LCD screen). If a Zero Check is used to check the zero offset, the suggested values are shown in brackets “[ ]” next to the actual Zero Adjust settings.

  • Page 32: Span Calibration

    2.3.2 Span Calibration S P A N C A L I B R A T I O N 0 9 : 1 7 : 2 8 1 2 - 0 9 - 0 2 1 < T O C S P A N A D J U S T 1 .
  • Page 33 4.-6. TIC Span Adjust. This menu item allows the user to set the TIC span adjust factors manually for each range as described for TOC Span Adjust above. 10. Run Span Calibration. This function starts the Span Calibration cycle. The span calibration reactions are run at a single range programmed by the RANGE in this menu below.
  • Page 34 20. TC Cal Std. In VOC systems, the sum of the TIC and TOC Calibration Standard solution is displayed as TC Calibration Standard. When TOC Calibration Standard is programmed as 0.0mgC/l, and when a concentration of TIC Calibration Standard is programmed above, BioTector displays the TC Calibration Standard as 0.0mgC/l on purpose.

  • Page 35: Technical Specifications

    Section 3 Technical Specifications TYPICAL TECHNICAL DATA Enclosure: Fiberglass Reinforced Polyester Dimensions (HxWxD): 1250mm x 750mm x 320mm Enclosure height may increase to 1750mm, depending on system optional features. 90 kg – 120 kg Weight: Enclosure weight may change depending on system optional features. Power Consumption: 300 W (VA) Mains Connection:...
  • Page 36 4-20mA Outputs: As individual signal up to maximum of 6 or as multiplex signal up to maximum of 35. Maximum impedance: 500 ohms. Hazardous Area: Certification options are available to European Standards (ATEX for Zone 1 and Zone 2) and to North American Standards (Class I Division 1 and Class I Division 2).
  • Page 37 SAMPLE & ENVIRONMENTAL CONDITIONS Sample Volume: Up to 8.0ml Sample Inlet Pressure: Typically ambient (for applications with high sample pressure, sampling systems are available) Drain Pressure: Typically ambient (for applications with high drain pressure, optional systems are available) 2°C – 60°C Sample Inlet Temperature: (36°F - 140°F) Sample Flow Rate:...

  • Page 38: Introduction

    Section 4 Introduction BioTector Major Components 4.1.1 Analysis Enclosure Figure 1 and table 2 below shows the typical major analysis enclosure components of BioTector TOC Analyzers. Figure 1 BioTector analysis enclosure major components Page 38...
  • Page 39 Table 2 BioTector analysis enclosure major components Air Isolation Valve, OV1 Pressure Relief Valve Cooler Ozone Generator Ozone Destructor Exhaust Valve, MV1 Exhaust Filter Hepa Filter Rotary Valve, OV2 Injection Valve, MV7 NDIR CO Analyzer Oxygen Pressure Regulator Non-return Valve (Check Valve) Ozone Line Filter Sample Valve (ARS Valve), MV4 Molecular Sieve Bed...

  • Page 40: Electronics Enclosure

    4.1.2 Electronics Enclosure Figure 2 and table 3 below shows the major electronics enclosure components of BioTector TOC Analyzer. Figure 2 BioTector electronics enclosure major components Table 3 BioTector electronics enclosure major components Power Supply (for Main Board/Motherboard) Power Supply (for Pumps and Valves) Power PCB (Mains PCB) Main Power Switch Mains Terminals...
  • Page 41 Figure 3 and table 4 below shows the BioTector main board (motherboard) components. Figure 3 BioTector main board components Table 4 BioTector main board components Motherboard (Main Board) LCD Screen Contrast Adjustment Dial Processor PCB MMC/SD Flash Memory Card Slot Page 41...

  • Page 42: Biotector Operation

    BioTector Operation Detailed information on the system operation is available, in presentation format, in the MMC/SD card shipped with the BioTector. It is recommended to review this file to understand the system operation. The BioTector is designed to provide continuous online single-component (e.g. TOC) or multi-component (e.g.

  • Page 43: Biotector Sample Injection

    4.2.2 BioTector Sample Injection The BioTector analyzes a precise volume of liquid. The Sample Pump injects a pre-programmed number of pulses (half revolutions of pump) of liquid into the reactor for each measurement and therefore the volume of liquid included in each pulse is consistent irrespective of sample source pressure. Sample is initially drawn from the source by a peristaltic Sample Pump.
  • Page 44 Figure 4 BioTector analysis layout (typical TIC & TOC system) Page 44...

  • Page 45: Biotector Oxygen Concentrator

    4.2.3 BioTector Oxygen Concentrator The operation of BioTector oxygen concentrator is based on the crystalline zeolite molecular sieves, which permits the separation of oxygen gas from the mixture of gases that comprise air. As air flows through a column or bed of molecular sieve, the component gases it contains are adsorbed and stratified in the order of their relative affinity to the molecular sieve material.
  • Page 46 Figure 6 BioTector oxygen concentrator layout Page 46...

  • Page 47: Biotector Analysis Types

    4.2.4 BioTector Analysis Types BioTector TOC analyzer has four factory calibrated analysis types: 1. TIC & TOC (NPOC) Analysis: Total Inorganic Carbon & Total Organic Carbon (Non-Purgeable Organic Carbon) Analysis 2. TC Analysis: Total Carbon Analysis 3. VOC (POC) Analysis: Volatile (Purgeable) Organic Carbon Analysis 4.2.4.1 TIC &...

  • Page 48: Voc (Poc) Analysis

    4.2.4.3 VOC (POC) Analysis BioTector Volatile Organic Carbon (VOC) analysis type is a combination of TC analysis followed by a TIC & TOC (NPOC) analysis. The VOC result obtained from the VOC analysis type represents the Purgeable Organic Carbon (POC) content of the sample. When both TC and TIC & TOC analysis are complete, the flowing data is available: ...

  • Page 49: Installation

    Section 5 Installation Basic System Requirements Power and Signal Requirements  Mains Connection: 115V AC, 60Hz or 230V AC, 50Hz (10%)  Mains Wire Specification: Number of Cores = 3 Current Rating minimum = 10 Amps CSA (Cross Sectional Area minimum) = 1.50mm ...

  • Page 50: Unpacking And Installation

    Unpacking and Installation The BioTector analyzer weighs more than 100kg (220lb). Therefore, appropriate precautions are required for unpacking and installing the BioTector. Caution The BioTector analyzer is shipped ready to be installed, with a kit of parts including sample tubes, reagent tubes and a selection of spare parts, spare fuses and ferrules.

  • Page 51: Analyzer Dimensions And Mounting

    5.2.1 Analyzer Dimensions and Mounting The BioTector TOC analyzer enclosure is a dual compartment Fiberglass Reinforced Polyester (FRP) cabinet. This enclosure facilitates easy access to all components and thus eases the service and maintenance procedures. Figure 7 and table 5 below gives the dimensions of various BioTector enclosures. Figure 7 BioTector Dimensions Table 5 Various BioTector Dimensions Height...
  • Page 52 Figure 8 below illustrates the BioTector door clearance dimensions. Figure 8 BioTector Door Clearance Dimensions  When BioTector is being mounted on a wall or a stand, the support has to be strong enough to carry typically four times of the weight of BioTector (~400 kg). ...

  • Page 53: Wiring Power And Signal Terminals

    5.2.2 Wiring Power and Signal Terminals BioTector contains electrical components operating under high voltages. Contact may result in electric shock and severe or fatal injury. DANGER Figure 9 and figure 10 below show the typical mains (for both 230 and 115 volts systems respectively) and the 4-20mA signal connections in BioTector.
  • Page 54 All electrical, sample, reagent, drain and exhaust connections should be carried out in accordance with the technical specifications and drawings given in this manual. Errors as a result of non-conformity to these specifications will not be covered by the warranty. Figure 10 Mains and 4-20mA terminal diagram for 115 V systems The wiring and earth connections to the analyzer should be carried out in accordance with local regulations, and securely terminated in the phase, neutral and earth terminals in the BioTector.

  • Page 55: Wiring External Power Disconnection Switch

    5.2.3 Wiring External Power Disconnection Switch The mains power must be connected through an external 2-pole disconnection switch, so that the power to the analyzer can be isolated without opening the electronics enclosure.  The external power disconnection switch must be located in an easily accessible location, with a maximum distance of 2 meters from the analyzer.

  • Page 56: System Fuse Specifications

    5.2.4 System Fuse Specifications Table 6 below summarizes the location and specification of the fuses used in BioTector. The locations of the fuses are also displayed in figure 9 and figure 10 above. BioTector contains electrical components operating under high voltages. Contact may result in electric shock and severe or fatal injury.

  • Page 57: Air Supply And Reagent Connections

    Air Supply and Reagent Connections The orientation of the ferrules inside each fitting of BioTector is critical for the correct operation of the system. Incorrect ferrule orientation may create gas/liquid leak and/or introduce air bubbles into the system lines. Therefore, the ferrules on all carrier gas, reagents, drain, exhaust and vent fittings have to be fitted with the correct orientation.

  • Page 58: Air Supply Connection

    5.3.1 Air Supply Connection The recommended air quality for BioTector is -20°C dew point, free of water, oil and dust. A filter pack may be required to meet or exceed the air quality specification. BioTector Air Compressor can be supplied by BioTector distributors as an option.

  • Page 59: Reagent Connections

    5.3.2 Reagent Connections Special precautions are needed when working with chemical reagents, both when renewing reagents and when dealing with leaks or spills. Some reagents can cause chemical burns and may cause injury or death if swallowed. Please refer to the symbols and codes on the reagent containers. DANGER Use of 25 liter containers is recommended for each BioTector reagents.
  • Page 60 As can be seen in the figure 14 above, unlike all other reagents, base reagent container does not contain any vent (breathing) hole. The breathing air into the base container is supplied through the CO filter, which must be fitted on the base container lid. Figure 15 below shows the detailed connections on BioTector base reagent.

  • Page 61: Sample, Drain And Exhaust Connections

    Sample, Drain and Exhaust Connections 5.4.1 Sample Inlet Tube Position For the fittings to remain leak proof, they must be kept clean and should not be over tightened. Over tightening of the fittings will damage them and cause eventual leakage. Caution BioTector operates on unfiltered samples, the setup of the sampling point is important for the correct operation of the system.
  • Page 62 Page 62...

  • Page 63: Drain, Bypass And Exhaust Connections

    5.4.2 Drain, Bypass and Exhaust Connections The BioTector should be installed in a well-ventilated area with the exhaust port piped to an external vent. The installation should be carried out in accordance with Section 1 Safety Precautions. WARNING All BioTector drain tubing must be positioned correctly so that any liquid pumped will drip freely into a larger drain chamber.

  • Page 64: Reagents And Calibration Standards

    Section 6 Reagents and Calibration Standards Reagents BioTector TOC analyzer uses following reagents: I. Acid: 1.8 N Sulfuric Acid (H ) Reagent containing 80mg/l Manganese Sulfate Monohydrate II. Base: 1.2 N Sodium Hydroxide (NaOH) Reagent Reagents should not contain high levels of organics, nitrates and phosphates. Ideally, the level of organics, nitrates and phosphates should be less than 100 g/l (ppb) in the deionized water used to prepare TOC analyzer reagents.

  • Page 65: Calibration Standards

    Calibration Standards All hygroscopic chemicals in crystal form should be dried in an oven set at 105°C for 3 hours to remove any traces of absorbed water. All prepared solutions must be mixed thoroughly with a magnetic stirrer or inverted manually at least ten times or until all crystals are completely dissolved inside the solution.
  • Page 66 The calculation of the quantities required to prepare Potassium Hydrogen Phthalate (KHP) standard solutions with various purities are given as an example below: Name: Potassium Hydrogen Phthalate Formula: Carbon, 12 Oxygen, 16 Potassium, 39 x 1 Hydrogen, 1 5____________ Total weight 204.22 g/mol 47% of KHP is Carbon.
  • Page 67 Preparation of Calibration Standard Solutions: Use eye protection and gloves. Standards solutions greater than 1000mg/l can be prepared directly without any dilution by simply mixing the necessary quantity solvent or salt with deionized water. Standard solutions below 1000mg/l concentration should be prepared by dilution technique. First a 1000mg/l standard stock solution should be prepared, and then the required lower concentration standard solution should be prepared by applying the necessary dilution procedures: ...

  • Page 68: Analyzer Commissioning And Startup

    Section 7 Analyzer Commissioning and Startup The check list below must be used to ensure that the installation has been properly carried out. Please proceed through the check list in the given order, completing the 5 sections below. Detailed commissioning and startup procedures are available in presentation format in the MMC/SD card shipped with the BioTector.
  • Page 69 Connect the Acid (1.8N Sulfuric Acid, H , containing 80 mg/l Manganese catalyst) and Base (1.2N Sodium Hydroxide, NaOH) containers to the BioTector’s ACID and BASE ports with ¼” PFA _____ tube. 20 or 25 liter containers are recommended. Confirm that weight fittings supplied are installed at the end of the acid and base reagent dip tubes.
  • Page 70 Check the air supply pressure. The set point pressure should be 1.5 bar. When the oxygen concentrator is running, the pressure typically cycles from 1.5 bar to 0.9 bar. Check the O2 PRESSURE SENSOR in O2-Controller Status menu. The pressure should be between 390 mbar _____ and 400 mbar at the idle 1 l/h “Mass Flow Controller”...
  • Page 71 4. COMMISSIONING MENU SETTINGS: Using the Commissioning menus (see Section COMMISSIONING MENU), follow below procedures to set up the BioTector for specific site requirements: In Reaction Time menu, program the INTERVAL time depending on the required sample analysis _____ frequency. In Sample Pump menu, set the correct Sample Pump FORWARD and REVERSE times.
  • Page 72 Go to Signal Simulate menu and test 4-20mA signals. Simulate 1mA, 4mA, 12mA and 20mA signals and confirm that the signals are received by the external process control device (e.g. _____ DCS). Simulate all digital input and output signals and confirm correct operation. 5.

  • Page 73: Maintenance Menu

    Section 8 Maintenance Menu Maintenance Menu Diagram Page 73...

  • Page 74: Diagnostics Menu

    DIAGNOSTICS MENU This group of menu allows the user to access the Process Test, Simulate, Data Output, Input/Output Status and Service menus for diagnostic purposes. Diagnostics Menu Diagram Page 74...

  • Page 75: Process Test

    8.1.1 Process Test This group of menus allows the user to simulate the Pressure Test, Flow Test, Ozone Test, Sample Pump Test, pH Test and Sample Valve Test routines. Detailed Process Test procedures are available in the MMC/SD card shipped with the BioTector. It is recommended to review these documents for troubleshooting purposes when necessary.

  • Page 76: Flow Test

    8.1.1.2 Flow Test F L O W T E S T 0 9 : 1 7 : 2 8 1 2 - 0 9 - 0 2 1 < * E X H A U S T T E S T E X H A U S T F L O W S A M P L E...

  • Page 77: Ozone Test

    8.1.1.3 Ozone Test The ozone test uses the procedure described in information sheet “T021. Procedure to check the ozone level in BioTector with Mixer Reactor”, which is available in the MMC/SD card shipped with the BioTector. The user must read and understand the processes described in this sheet, and have all the correct parts listed before carrying out the test.
  • Page 78 Ozone Test, Phase 3: O Z O N E T E S T 0 9 : 1 7 : 2 8 1 2 - 0 9 - 0 2 * S T A R T T E S T 2 < S T O P T E S T T I M E...

  • Page 79: Sample Pump Test

    8.1.1.4 Sample Pump Test S A M P L E P U M P T E S T 0 9 : 1 7 : 2 8 1 2 - 0 9 - 0 2 V A L V E S T R E A M 2 <...

  • Page 80: Ph Test

    8.1.1.5 pH Test The user must understand the procedure for testing the pH in the BioTector. Use eye protection and gloves. Have all the relevant parts for this test ready (primarily beaker and pH paper) before carrying out the test. WARNING For the pH test to be accurate, the previous reaction should have finished normally, so that any liquid carried over from that reaction will not affect the pH...
  • Page 81 3. Start Test. This starts the pH test routine, which goes through the 6 phases described above. 4. Take Sample. Not applicable until the test is running. 5. Continue to next phase. Not applicable until the test is running. 6. Stop Test. When the test is running, activating this control will stop the test. Note that some phases have to be completed before the stop can be used.
  • Page 82 pH Test, Phase 3: T E S T 0 9 : 1 7 : 2 8 1 2 - 0 9 - 0 2 1 < R A N G E , V A L V E S T R E A M M O D E T I C + T O C S T A R T...
  • Page 83 pH Test, Phase 5: T E S T 0 9 : 1 7 : 2 8 1 2 - 0 9 - 0 2 1 < R A N G E , V A L V E S T R E A M M O D E T I C + T O C S T A R T...

  • Page 84: Sample Valve Test

    8.1.1.6 Sample Valve Test S A M P L E V A L V E T E S T 0 9 : 1 7 : 2 8 1 2 - 0 9 - 0 2 1 < * T E S T F I R S T F A I L U R E S E N 1...

  • Page 85: Base Wash Test

    8.1.1.7 Base Wash Test B A S E W A S H T E S T 0 9 : 1 7 : 2 8 1 2 - 0 9 - 0 2 V A L V E S T R E A M S T A R T T E S T S T O P...

  • Page 86: Simulate

    8.1.2 Simulate S I M U L A T E 0 9 : 1 7 : 2 8 1 2 - 0 9 - 0 2 M F C = 1 0 . 0 l / h C O 2 = 3 5 .
  • Page 87 1. MFC. Use this function to set the MFC setpoint. Press the ENTER key, set the required setpoint (e.g. 100 l/hr), and press the ENTER key again. The actual flow is shown at the top of the screen. An “*” is shown when the MFC has been activated.
  • Page 88 9. Sample Pump. Use this function to test the Sample Pump. The pump has four operating states: FWR (forward), REV (Reverse), P-FWR (run under pulse control forward), P-REV (run under pulse control in reverse). To run the pump in the required mode, press the ENTER key, and select that mode. If P-FWR or P-REV is selected, enter the number of pulses (½...
  • Page 89 21. Sampler Fill (if configured in the system). Signal to fill the BioTector sampler. To test the Sampler Fill signal, press the ENTER key, set the device to ON/OFF, and press the ENTER key again. If the device is on, it will be marked with an “*”. This signal remains on until turned off. 22.

  • Page 90: Signal Simulate

    8.1.3 Signal Simulate S I G N A L S I M U L A T E 0 9 : 1 7 : 2 8 1 2 - 0 9 - 0 2 1 < * C H A N N E L 1 - 6 4 .
  • Page 91 32. Cal Signal (if configured in the system). Use this function to test the Calibration Signal output. To change the state of the device, press the ENTER key, set the device to ON/OFF, and press the ENTER key again. If the device is on, it will be marked with an “*”. See Section 8.3.5 Output Devices for details.

  • Page 92: Data Output

    8.1.4 Data Output D A T A O U T P U T 0 9 : 1 7 : 2 8 1 2 - 0 9 - 0 2 1 < O U T P U T D E V I C E M M C / S D C A R D S E N D...

  • Page 93: Send Reaction Archive

    8.1.4.1 Send Reaction Archive S E N D R E A C T I O N A R C H I V E 0 9 : 1 7 : 2 8 1 2 - 0 9 - 0 2 1 < S T A R T D A T E 0 1 - 0 9 - 0 2...

  • Page 94: Standard Mode

    Standard mode: TIC & TOC Analysis: TIME The time the reaction started. DATE The date the reaction started. S1:2 Stream type and analysis range. TIC [mgC/l] The calibrated TIC value in mgC/l. TOC [mgC/l] The calibrated TOC value in mgC/l (TOC represents NPOC). COD/BOD[mgO/l] The calculated COD and/or BOD value in mgO/l (if activated in COD/BOD Program menu).
  • Page 95 Engineering mode (VOC Analysis): TIME The time the reaction started. DATE The date the reaction started. S1:2 Stream type and analysis range. CO2z analyzer zero adjust for the current reaction. TCmgu The un-calibrated TC value in mgC/l (measured value from the TC analysis). TCmgc The calibrated TC value in mgC/l (measured value from the TC analysis).

  • Page 96: Send Fault Archive

    8.1.4.2 Send Fault Archive This menu is used to download the fault archive. The communication port parameters used are those set up in the Data Program menu. All items in the fault archive will be downloaded unless the user interrupts the downloading with the Pause Sending or Stop Sending functions.

  • Page 97: Input/Output Status

    8.1.5 Input/Output Status Input/Output Status menus are used for monitoring the analog and digital inputs and outputs for advanced diagnostics purposes. Digital Input The Digital Input menu allows the engineer to monitor the system digital inputs. This feature is useful for the system trouble-shooting or diagnostics.

  • Page 98: Oxygen Controller Status

    8.1.6 Oxygen Controller Status O 2 - C T R L S T A T U S 0 9 : 1 7 : 2 8 1 2 - 0 9 - 0 2 1 < I D E N T I F I C A T I O N # c 3 0 0 0 0 1 9 V E R S I O N 0 3 .

  • Page 99: Service

    8.1.7 Service S E R V I C E 0 9 : 1 7 : 2 8 1 2 - 0 9 - 0 2 1 < R E A C T I O N C O U N T E R 5 2 3 8 S E R V I C E R E Q U I R E D...

  • Page 100: Commissioning Menu

    COMMISSIONING MENU The Commissioning menus are used during the commissioning and startup of the analyzer. The functions in the menus are used to program system site specific settings. Commissioning Menu Diagram 8.2.1 Reaction Time REACTION TIME 6m52s  REACTION TIME displays the total reaction time (in minutes and seconds) for range 1, based on all programmed settings in System Program, System Program 1 menu.

  • Page 101: Sample Pump

    8.2.2 Sample Pump SAMPLER FORWARD REVERSE  BioTector Sample Pump runs forward for the FORWARD time to STREAM 1 100s bring a fresh sample from the STREAM, MANUAL and/or STREAM 2 100s CALIBRATION points to the Sample (ARS) Valve. This time STREAM 3 should be long enough to guarantee a fresh sample is injected ……………………...

  • Page 102: Stream Program

    8.2.3 Stream Program SAMPLER  If a sampler is used with the BioTector, SAMPLER is programmed (YES). When activated in this menu, the programmable Sampler time will be displayed automatically in the Sample Pump menu above.  In multi-stream systems, CONTROL determines the multi-stream CONTROL BIOTECTOR valve sequence to be controlled by either BIOTECTOR, or by an...

  • Page 103: Cod/Bod/Lpi/Flow Program

    8.2.4 COD/BOD/LPI/FLOW Program DISPLAY  DISPLAY function, which is programmed as “NO” by default, allows the user to program COD, BOD, LPI and/or FLOW & e.g. TOC in kg/h parameter results to be displayed by the system with the “YES” setting. When activated, the system sends the relevant 4-20mA signals for COD, BOD (in mgO/l), LPI (in %), and/or FLOW (in m /h) &...
  • Page 104 FLOW PROGRAM  HEADING function determines the label for the total product loss, total waste, etc. result based on the externally measured HEADING TOC kg/h sample flow input value, which is sent to the BioTector as an DET. TIME analog input signal, if this option is installed into the system. This STREAM 1 0.00m3/h, 1.00 parameter is an editable text with a maximum size of 8...

  • Page 105: New Reagents Program

    8.2.5 New Reagents Program SPAN CALIBRATION  SPAN CALIBRATION (NO by default) defines if the Span Calibration reactions are part of the Install New Reagents procedure in Reagents Setup menu.  If SPAN CALIBRATION is activated (YES), the standard solution needs to be connected to the Calibration/Manual port of the BioTector as part of the Install New Reagents procedure.

  • Page 106: Reagents Monitor

    8.2.6 Reagents Monitor REAGENTS MONITOR  When REAGENTS MONITOR is activated (YES), the system creates a new Reagent Status screen which displays the amount of reagents and the estimated number of days left for each reagent to last. The Reagent Status screen is displayed for a period of 15 minutes and the system automatically reverts back to the default Reaction Result screen.

  • Page 107: Autocal Program

    8.2.7 Autocal Program TIME 00:00  TIME (00:00 by default) schedules the Zero & Span Calibration or Check reactions time (in HR:MIN) for the weekdays if any is programmed below. MONDAY CHECK  In this menu, Zero and/or Span Calibration reactions and/or TUESDAY Check reactions are scheduled if programmed on a particular WEDNESDAY...
  • Page 108 CHANNEL 1 STREAM 1  In CHANNEL 1 STREAM 1 TOC setting, the first parameter CHANNEL 1 500mgC/l INST defines the type of 4-20mA output which can be programmed as: CHANNEL 2 STREAM 1 STREAM and MANUAL reaction results, CAL (zero & span CHANNEL 2 100mgC/l INST...

  • Page 109: Alarm Program

    8.2.9 Alarm Program ALARM 1 STREAM 1  If ALARM 1-6 is not programmed in Output Devices menu, this 20.0mgC/l option will not be available in this menu. See section 8.3.5 ALARM 2 STREAM 2 Output Devices for details. 10.0mgC/l ...

  • Page 110: Data Program

    8.2.10 Data Program PRINTER, PC, MMC/SD CARD  These menus allow the user to program three separate output device communication port configuration profiles, which are PRINTER, PC and MMC/SD flash card.  The functions described below covers all programming options for each device.

  • Page 111: System Configuration Menu

    SYSTEM CONFIGURATION MENU System Configuration menus are used to configure the system in the factory. The user should avoid any modifications in these menu settings unless it is absolutely necessary. System Configuration Menu Diagram Page 111...

  • Page 112: Analysis Mode

    8.3.1 Analysis Mode ANALYSIS TYPE TIC+TOC_D  ANALYSIS TYPE defines BioTector’s analysis modes, which are TIC+TOC, TC, VOC, TIC+TOC_D, TC_D and VOC_D. TIC+TOC (TIC&TOC) and VOC systems can be programmed to run in TIC+TOC, TC and VOC analysis types, including the “_D” analysis types.

  • Page 113: System Program

    8.3.2 System Program SYSTEM PROGRAM 1  SYSTEM PROGRAM 1 TIC + TOC_D defines the system SYSTEM PROGRAM 1 TIC + TOC_D parameters for Oxidation Phase operation in TIC & TOC_D analysis mode. In TIC & TOC_D analysis mode, the TIC and TOC contents of a sample are measured consecutively by means of a single sample injection into a single reactor.
  • Page 114 TOC ACID  TOC ACID states the amount of acid (in pulses) to be injected into the reactor for the TOC SPARGE phase at range 1. TOC SPARGE TIME 135s 20l/h  BioTector sparges and measures the TOC content of the sample for the TOC SPARGE TIME (135s by default) with the oxygen flow (20 l/h) settings.
  • Page 115 SYSTEM PROGRAM 1 TC_D  SYSTEM PROGRAM 1 TC_D defines the system parameters for Oxidation Phase operation in TC_D analysis mode. In TC_D analysis mode, the TC_D content of a sample is measured by means of a single sample injection into the reactor. ...
  • Page 116 SYSTEM PROGRAM 2 SYSTEM PROGRAM 2 TIC + TOC_D RANGE CHANGE 1-2 50.0mgC/l  RANGE CHANGE 1-2 defines the concentration levels for the BioTector to change its range automatically from range 1 to range 2.  The RANGE CHANGE 1-2 is typically the top concentration point of TOC RANGE 1 in System Range Data menu by default.
  • Page 117 SYSTEM PROGRAM 3 SYSTEM PROGRAM 3 TIC + TOC_D  RANGE CHANGE 2-3 defines the concentration level for the RANGE CHANGE 2-3 150.0 mgC/l BioTector to change its range automatically from range 2 to range 3.  The RANGE CHANGE 2-3 is typically the top concentration point of TOC RANGE 2 in System Range Data menu by default.

  • Page 118: Calibration Data

    8.3.3 Calibration Data DECIMAL PLACES  DECIMAL PLACES setting defines the number of decimal places (0, 1, 2 or 3) system displays in the reaction results and in the relevant system menus. TOC/TC CALIBRATION 1  Calibration menus are used to install the calibration data and TOC/TC CALIBRATION 2 thus to calibrate the BioTector in factory.

  • Page 119: Cleaning Program

    8.3.4.2 Cleaning Program The parameters in Cleaning Program menu identifies the operation of the specific cleaning cycle built and programmed for each specific analyzer. CLEANING TYPE BASE WASH  Systems, programmed to operate with the BASE WASH cleaning type, carries out sample tubing wash cycle at a programmable frequency, and if necessary a reactor wash cycle using the base reagent.
  • Page 120 CLEANING VALVE  When the CLEANING VALVE is programmed with the SPF “Sample Pump Forward” setting or SPF/SAMPLER setting in systems operating with BioTector sampler, cleaning valve is powered just before and while the sample pump is running in forward direction. ...
  • Page 121 TUBING WASH BASE 1  In systems programmed with BASE WASH cleaning cycle, TUBING WASH ACID TUBING WASH BASE 1, ACID and BASE 2 settings define the TUBING WASH BASE 2 quantity of acid and base reagents (in pulses) used to wash the sample lines which include tubing located between the Sample (ARS) Valve and the Bypass port, and each stream specific tubing.

  • Page 122: Zero Program

    8.3.4.3 Zero Program ZERO PROGRAM  In ZERO PROGRAM 5, 3, 3 setting, the first, second and third inputs define the minimum number of reactions to be carried out at Range 1, Range 2 and Range 3 respectively during the Zero Calibration and Zero Check cycles.

  • Page 123: Span Program

    SERVICE ZERO 20 , 5  SERVICE ZERO specifies the number of zero calibration cycles to be repeated after a defined number of reactions between each zero calibration cycle. The first setting “20” is the number of reactions between each zero calibration cycle, and the second setting “5”...
  • Page 124 TC CAL STD 250.0mgC/l  In VOC systems, the sum of the TIC and TOC Calibration Standard solution is displayed as TC Calibration Standard. When TOC Calibration Standard is programmed as 0.0mgC/l above, and when a concentration of TIC Calibration Standard is programmed above, BioTector displays the TC Calibration Standard as 0.0mgC/l on purpose.

  • Page 125: Reagents Purge

    8.3.4.5 Reagents Purge ACID PURGE 23s , 4  ACID/BASE PURGE defines the operation time (23 seconds by BASE PURGE 23s , 4 default) of the acid and base pumps to prime the reagents during the Install New Reagent cycle. The reagent priming and the subsequent reactor purge operation is repeated 4 times by default.
  • Page 126 PRESSURE CHCK FAULT 6.0l/h  At the end of each reaction during operation, BioTector automatically pressurizes the system with oxygen gas and uses its mass flow controller to detect any gas leak in the system. If the measured flow is less than or equal to the programmed PRESSURE CHECK FAULT flow level (6.0 l/h by default) during the test, the pressure check passes.

  • Page 127: Output Devices

    8.3.5 Output Devices POWERED ALL TIME  POWERED ALL TIME parameter specifies if the relays are powered all the time even if the system is stopped or paused with the YES setting, or if the relay is powered only when required with the default NO setting.
  • Page 128 RELAY 18 DEFAULT STATE DEFAULT STATE defines the idle state of the relay. N/D stands for “Normally De- energized” relay by default and N/E stands for “Normally Energized” relay. STOP Output set to operate when the BioTector is stopped condition. Note that remote stand- by is not considered as a stop condition.
  • Page 129 OUTPUT 1-8  OUTPUT1-8 menus contain system optional output relay settings. Relay terminals 1-8 are located on the stream expansion board (auxiliary board), which is an optional feature of the system.  OUTPUT1-8 relays can be programmed to a single output function or to multiple output functions as described for RELAY 17-20 above.

  • Page 130: Reaction Check

    8.3.6 Reaction Check CO2 LEVEL 100ppm, AUTO  Due to the organic and inorganic contamination in the BioTector reagents, every TOC/TC reaction will generate a small level of from the reagents alone even if there is no sample present. The first setting (100ppm by default) of CO2 LEVEL specifies the reaction check CO level, which is the minimum expected CO reading in ppm measured by the CO...

  • Page 131: Result Integration

    8.3.7 Result Integration RESULT INTEGRATION  RESULT INTEGRATION (3 by default) defines the number of reaction results to be averaged to get the actual TOC result.  INTEGRATION LIMITS controls the averaging function defined INTEGRATION LIMITS 10% , 5.00 in RESULT INTEGRATION above. The first parameter “10%” defines the % band variation and the second parameter “5.00”...
  • Page 132 SERVICE COUNTER 180 DAYS  SERVICE COUNTER (180 days by default) specifies the number of days the system operates before triggering an “83_SERVICE TIME” warning.  Note that the service counter keeps operating and decreases the count by a day if system is powered up during the same day even though system was not running.

  • Page 133: Fault Status

    8.3.9 Fault Status This menu gives a short status history of several system devices before a fault is registered. The default 0.0 values indicate that there are no faults detected for the specific device. O2 FLOW  The O2 FLOW menu consists of 120 entries for the MFC setpoint value (first column) and MFC flow value (second column).

  • Page 134: Co2 Analyzer

    8.3.10 CO2 Analyzer ANALYSIS GRAPH SCALE 10000ppm  ANALYSIS GRAPH SCALE determines the scale of the y-axis “CO analyzer’s ppm-CO readings” on the Analysis Graph Screen (see Section 2.1.4 Analysis Graph Screen details). This function allows the system to display CO data peaks in optimal resolution on the LCD screen.

  • Page 135: Cooler Program

    8.3.11 Cooler Program COOLER 16.0C DIFF  COOLER 16.0C DIFF, defines the programmed cooler temperature setpoint (16°C by default) and the operation mode DIFF (DIFFERENTIAL temperature mode by default). Other available operation modes are F (FIXED temperature mode) and B (BACKUP mode). ...

  • Page 136: Ozone Destructor Program

    8.3.12 Ozone Destructor Program PURGE CYCLE MODE AUTO  PURGE CYCLE MODE, which is automatically controlled (AUTO by default), specifies how the purging of the Ozone Destructor is carried out. In AUTO (Automatic) mode, the Ozone Destructor heater and the BioTector Cooler are controlled by the PURGE CYCLE FLOW and AUTO PURGE CYCLE parameters defined below.

  • Page 137: Software Update

    8.3.13 Software Update LOAD FACTORY CONFIG.  Each BioTector system contains a configuration which is installed and protected by system flash memory. When any modification is carried out in system configuration, LOAD FACTORY CONFIGURATION function allows the user to revert back to the original system settings programmed in the factory.

  • Page 138: Password

    8.3.14 Password OPERATION 0000  Password menu allows any number from 1 to 9999 to be set as CALIBRATION 0000 passwords for the Operation, Calibration, Diagnostics, DIAGNOSTICS 0000 Commissioning and System Configuration menus (levels). When COMMISSIONING 0000 the setting is 0000 (by default), the password is disabled. SYSTEM CONFIGURATION 0000 ...

  • Page 139: Troubleshooting Of System Fault, Warning And Notification Events

    Section 9 Troubleshooting of System Fault, Warning and Notification Events BioTector Fault Event Explanation and Remedial Action The following fault conditions activate the BioTector stop sequence, set all 4-20mA signals to the FAULT LEVEL (1mA by default) programmed in the 4-20mA Program menu, and activate the FAULT relay. When the system fault is rectified, acknowledge the fault by pressing the ENTER key in the Fault Archive menu.
  • Page 140 05_PRESSURE TEST FAIL MFC flow did not drop below the Gas/liquid leak in the BioTector. “PRESSURE TEST FAULT” level Valve leaking or not sealing. during the pressure test cycle. See Open Sample Out Valve, inspect Section 8.3.4.6 Pressure/Flow Test for dirt/damage. Program for details.
  • Page 141 analyzer’s ppm CO 11_CO2 ANALYZER FAULT Fault in CO Analyzer. Check CO Very dirty optics in CO Analyzer. response in Simulate menu. Open CO analyzer and clean the optics. Power down and power up the BioTector. If problem persists, check outgoing 24V DC power to CO analyzer on Motherboard at wires 101 and 102.
  • Page 142 17_SMPL VALVE NOT Correct sensor position for Sensor 1 Change Relay 4 on the Relay SYNC (SEN1) has not been detected in PCB. Sample Valve when Sample Pump is Check sensor signal looking at running. LED 12 on Signal PCB and DI01 in Digital Input menu.

  • Page 143: Biotector Warning Event Explanation And Remedial Action

    BioTector Warning Event Explanation and Remedial Action The following warning conditions do not activate the BioTector stop sequence and leave the 4-20mA signals un-changed and do not activate the fault relay. If there are multiple warnings in the system, check the fuses on the Relay PCB and Signal PCB.
  • Page 144 29_PRESSURE TEST OFF There are two pressure tests carried Activate the Pressure/Flow Test out in BioTector. One is a daily cycle by programming the factory pressure test and the other, called flow settings in Pressure/Flow pressure check, is carried out every Test Program menu.
  • Page 145 52_HIGH CO2 IN BASE level in the base reagent, which is Confirm the base reagent CO checked during the Zero Calibration or filter is serviced and in good Zero Check cycles, is higher than the condition, and the container is “BASE CO2 ALARM”...
  • Page 146 63_SMPL PUMP STOP OFF Sample Pump stopped with its rotation Run the Sample Pump and check sensor OFF or the sensor is faulty and the rotation. it is not sensing the rotation of the Change Relay 2 on Relay PCB. pump.
  • Page 147 84_SAMPLER ERROR Warning generated on the BioTector Check the LCD screen of the venturi/vacuum sampler due to no/low venturi/vacuum sampler for sample or low air pressure/vacuum in details. the sampler. See BioTector venturi/vacuum sampler user manual. 88_O2 CONTROLLER A problem has been found during Check LED 2 (L2) on the O2- WARN communication with the O2-Controller...
  • Page 148 94_LO AIR PRESSURE 2 Air pressure supply has been less than Extreme fluctuations in air supply 0.6 bar for longer than 5 seconds. pressure or faulty external air When the oxygen concentrator is regulator. running, the pressure typically cycles Increase air supply pressure to from 1.5 bar to 0.9 bar.
  • Page 149 100_ROTARY V STOP:ON Rotary Valve stopped with its rotation Go to Simulate menu, set MFC sensor on (sensor signal 1). flow to 20 l/h and check the The sensor is faulty and it is always rotation of the Rotary Valve. showing on (sensor signal 1).

  • Page 150: Biotector Notification Event Explanation And Remedial Action

    BioTector Notification Event Explanation and Remedial Action The following Notification conditions do not activate the BioTector stop sequence, leave the 4-20mA signal un-changed and do not activate the fault relay. Relevant notifications below can be acknowledged in the Fault Archive menu. NOTIFICATION CONDITION CAUSE/REMEDY...

  • Page 151: Service And Maintenance

    Section 10 Service and Maintenance 10.1 Weekly Maintenance  Check the air supply pressure: A) An existing instrument air supply line B) BioTector Compressor  Check and confirm that the air pressure is 1.5 bar on the filter pack pressure regulator. ...

  • Page 152: Six Month Service

    10.2 Six Month Service Below procedure is a recommended check list for the 6 month service on the BioTector TOC analyzers, built with Mixer Reactor, using the 6 Month Service Kit. Please note that any special models and applications may require additional service items.
  • Page 153 Using the Simulate menu (see Section 8.1.2 Simulate for details) and referring to figure 1 and table 2 in Section 4.1.1 Analysis Enclosure, check and confirm that the valves are operating and there are no leaks: Check Sample (ARS) Valve, MV4 rotation from sensor 1 (SEN1) to sensor 2 (SEN2) to sensor 3 _____ (SEN3) and to (SEN4) positions.
  • Page 154 Clean CO analyzer optics by removing the 4x M4x60 Allen bolts on the detector section. If necessary, clean both lenses, which are located on the detector and the source section of the CO _____ Analyzer using the Lens Tissue (see item T in the service kits). Replace o-ring with the 72-0325-30 o-ring provided (see item P in the service kit).
  • Page 155 Confirm that the temperature of the ozone destructor has dropped to ambient temperature level. Open the ozone destructor. The ozone destructor should never be opened when it is hot as the threads may seize. Confirm that the PTFE filters (discs) in the ozone destructor are clean. If there is _____ any material build up (e.g.
  • Page 156 Program the concentration of the standard solution in the Span Calibration menu (2.3.2 Span Calibration). The concentration of the calibration standard used must be typically greater than 50% of the full scale of the RANGE the calibration is carried out. In order to see BioTector calibrated _____ ranges, see System Range Data screen (2.2.3 System Range Data...

  • Page 157: System Replacement And Spare Parts

    Section 11 System Replacement and Spare Parts Page 157...
  • Page 158 BioTector Parts and Spare Parts Part Number and Part Number and Description Description 19-KIT-132 19-PCB-046 B7000i Type D BioTector ARM Mainboard, Rev 4, TOC Analyzer 6 Month Including Processor and Service Kit 20-PCB-136 10-EMT-090 B7000i Oxygen Controller PEEK ARS Sample Valve Board, complete (2.5mm) 19-MAX-010...
  • Page 159 Part Number and Part Number and Description Description 10-SMR-001 19-EMC-001 Non return valve (check Type 6606 Burkert N/C valve), 1psi valve with plug 19-EMC-002 19-EMC-003 Type 6606 Burkert N/O Type 6606 Burkert C/O valve with plug valve with plug 12-BIO-001 19-PCB-003 B4M C/O Pinch Valve, Power PCB (Mains PCB)
  • Page 160 Part Number and Part Number and Description Description 10-SCA-002 10-SCA-003 PFA Tubing, 1/4" OD x PFA Tubing, 3/16" OD x 5/32" ID - 1 meter 1/8" ID - 1 meter 10-SCA-006 10-SCA-007 PFA Tubing, 1/4" OD x 1/8” PFA Tubing, 3/16" OD x 1/16”...

  • Page 161: General Information

    BioTector Analytical Systems Ltd., Raffeen House, Ringaskiddy, Co.Cork, Ireland Tel: (+353) 21 437 42 37, Fax: (+353) 21 437 42 36, e-mail: info@biotector.com. Product: Produkt: / producto: / produit: / prodotto: BioTector B7000i TOC. Manufacturer’s serial numbers: Hersteller Seriennummern/Fabricantes números de serie/Fabricants numéros de série/Numeri di serie Produttori: BAC xxxyyyy &...

  • Page 162: Declaration Of Compliance

    12.2 Declaration of Compliance Declaration of Compliance Manufacturer: BioTector Analytical Systems Ltd. Address: Raffeen House, Ringaskiddy, Co. Cork, Ireland. Declares that the BioTector TOC Analyzer is in compliance with the following European/Irish Standard: I.S. EN 1484:1998 Water Analysis – Guidelines for the Determination of Total Organic Carbon (TOC) and Dissolved Organic Carbon (DOC) David Horan...

  • Page 163: Warranty And Exclusions

    12.3 Warranty and Exclusions Coverage of BioTector Warranty The BioTector comes with a standard 1 year warranty for agreed applications. The BioTector warranty is against manufacturing defects only. The warranty does not cover service/consumable items and consequential damage. Validity of Warranty For the warranty to be valid, regular 6 Month servicing must be carried out using the Service Kit supplied by the manufacturer.

  • Page 164: Regional And Country Specific Documents

    12.4 Regional and Country Specific Documents BioTector B7000i液体分析仪 关于符合中国《电子信息产品污染控制管理办法》的声明 中国RoHS： 部信息产业订单＃39， “电子信息产品污染控制管理办法”。 中国RoHS有毒有害物质或元素控制： 铅 汞 镉 六价铬 联合国- 多溴联苯 多溴二苯醚 （参考：中国工业和信息化部订购＃39） BioTectors产品虽然没有具体列出为中国电子信息产品（EIP），一些使用的电子元件中列出的子部分（如组件下的电子设备 工业部分）。尽职调查的要求，我们必须确保我们的产品符合信息产业部令第39号，并在可预见的，面向未来的，对新兴的 中国工业和信息化部建议。 为了证明这一点符合我们作出的自愿声明，指出一些EIP列出的组件中使用的BioTector产品的环保使 用期限（EFUP）至少25年。该产品的生产日期可以发现在产品标签上显示主板上的机箱后面。 此外，我们还宣布我们的包装不包含任何在这六种受限物质。 中国RoHS声明表 部件名称 有毒有害物质或元素 (Pb) (Hg) (Cd) (Cr6) (PBB) (PBDE) 铅 汞 镉 六价铬...
  • Page 165 Page 165...

  • Page 166: Appendices

    Section 13 Appendices Appendix 1 Instructions for Connecting Printer to BioTector Protocol used by the BioTector Baud rate 9600 Data bits Stop bits Parity None Flow control None Note that these instructions refer to the Epson LX300 printer with the optional serial port fitted. If a printer cable provided by the BioTector manufacturer is used, the electrical connections are as follows: - Terminal TX on the microcontroller is connected to pin 3 on the D25 plug.

  • Page 167: Appendix 2 Setting Up Windows To Receive Data From Biotector

    Appendix 2 Setting up Windows to Receive Data from BioTector To set up Windows for receiving data from the BioTector, open the Hypertrm file found within the HyperTerminal folder. This may be carried out by selecting Start, Programs, Accessories, Communications, HyperTerminal.

  • Page 168: Appendix 3 Glossary Of Terms And Abbreviations

    Appendix 3 Glossary of Terms and Abbreviations - - - No function is programmed 4-20mA CHNG 4-20mA Change signal Amperes 24 hours average for stream 1 – 6 A1 - A6 ALLDAT All Data Amperes ARS Valve Automatic Range Selection Valve (Sample Valve) Atmospheric pressure Biochemical Oxygen Demand C-276...
  • Page 169 Not Applicable Normally de-energized Normally Energized NaOH Sodium Hydroxide NDIR Non-dispersive Infrared NOTE Notification NPOC Non-purgeable Organic Carbon Oxygen Ozone Outside Diameter Operating System 3 Printed Circuit Board PEEK Poly-ether-ether-ketone Per-fluoro-alkoxy Purgeable Organic Carbon Poly-propylene Parts per billion (g/l) Parts per million (mg/l) PTFE Poly-tetra-fluoro-ethylene PVDF...

  • Page 170: A 4 C I

    HACH Company Repair Service in the Repair Service in Canada: Repair Service in World Headquarters United States: Hach Sales & Service Latin America, the Canada Ltd. P.O. Box 389 HACH Company Caribbean, the Far East, 1313 Border Street, Unit 34...
  • Page 171 HACH LANGE MAROC SARLAU Villa 14 – Rue 2 Casa Plaisance Quartier Racine Extension MA-Casablanca 20000 Tél. +212 (0)522 97 95 75 Fax +212 (0)522 36 89 34 info-maroc@hach-lange.com www.hach-lange.ma Page 171...

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