Inficon HAPSITE ER Portable GC/MS Manuals

Manuals and User Guides for Inficon HAPSITE ER Portable GC/MS. We have 2 Inficon HAPSITE ER Portable GC/MS manuals available for free PDF download: Operating Manual

Inficon HAPSITE ER Operating Manual (432 pages)

chemical identification system

Brand: Inficon | Category: Measuring Instruments | Size: 41.25 MB

Operating Manual Style Conventions

4
- Table of Contents
  5
- Customer Support
  14
Chapter 1

14
- How to Contact Customer Support
  14
- Returning Your Instrument to INFICON
  15
  - Introduction
    16
Chapter 2 HAPSITE er System

16
- HAPSITE er and Accessories
  16
  - Specifications
    17
  - Instrument Overview
    18
  - Description of Subsystems
    18
- Gas Chromatograph
  18
- Membrane Isolation Valve
  19
  - Mass Spectrometer
    20
  - Vacuum System
    21
  - Electronic Systems
    22
- Mass Spectrometer Control
  22
- Gas Chromatograph Control
  22
- Main Processor
  22
- Interfaces
  23
  - Software Systems
    23
    
    HAPSITE Components and Assemblies
    24
Chapter 3 Ship Kit Packing Lists

24
- 930-850-G9, G12 Ship Kit Contents
  24
- 930-850-G10, G11 Ship Kit Contents
  26
- Ship Kits Box 3 and 4
  28
  - Basic Assembly
    28
- Attaching the Probe
  29
- Installing the Gas Canisters
  30
- How to Remove a Gas Canister
  34
  - Connect the Power Supply
    36
    
    Connecting the Laptop
    37
  - Connect Laptop with Black Crossover Cable
    37
  - Connect Laptop with Wireless Connection
    39
    
    Battery
    39
    
    Battery Charger
    39
    
    Battery Charger Connections and Startup
    39
    
    Loading the Battery Charger
    40
    
    Understanding the Battery Charger Indicators
    41
  - Testing Battery
    42
    
    Installing the Battery
    42
    
    Removing the Battery
    43
    
    Replacing the Concentrator
    44
    
    Probe Nut Assembly
    52
    
    Attaching a Bag Sample
    53
    
    VX/R-33 Conversion Tube
    56
- Air Probe Sampling
  56
- Thermal Desorption Tube Sampling
  58
  - Helpful Guidelines
    60
    
    Operating HAPSITE er in Portable Mode
    61
Chapter 4 Starting HAPSITE er in Portable Mode

61
- Emergency Mode (EMER MODE)
  66
- Concentrator Options (CONC OPTIONS)
  68
- Concentrator Cleanout
  68
- Skip Cleanout
  70
  - Concentrator Cleanout Failure
    71
  - Quick Reference SOP - Heat-Up and Tune
    72
    
    Selecting a Different Method Using the SELECT METHOD Icon
    73
    
    Changing the Default Method
    76
    
    Show All
    77
    
    Survey Mode
    77
    
    Quick Reference SOP - Survey Method
    84
    
    ANALYZE (GC/MS) Mode with the Concentrator
    85
    
    Procedure for Running Concentrator Methods
    85
    
    Tenax Concentrator
    85
    
    Tri-Bed Concentrator
    85
    
    Detecting Hazardous Chemicals
    90
    
    Quick Reference SOP - Concentrator Methods
    90
    
    View Results/View Reports
    91
    
    Help Icon
    100
    
    Info Icon
    101
  - HAPSITE er Icon
    109
- Battery Icon
  110
- Carrier Gas Icon
  110
- Internal Standard Icon
  111
- HEATERS Icon
  111
- HEATERS Button
  112
- NEG Button
  112
- CONC Button
  113
  - TUNE STATUS Icon
    113
- Tune Reports
  114
  - GPS Icon
    115
  - HAPSITE SYSTEM Icon
    116
- HAPS Button
  116
- FIRMWARE Button
  117
- DATE TIME Button
  117
- NET Button
  118
  - Attachments
    118
  - Info
    119
    
    EXIT Menu
    119
    
    Extended Standby
    121
  - End Standby
    123
    
    Communications and Touch Screen Options
    125
Chapter 5 Communications

125
- Wireless Range
  125
- Turning on the Radio
  125
- Wireless Module Indicator Lights
  127
- FCC Statement
  143
- FCC RF Exposure Statement
  144
  - Regulatory Compliance Information for CANADIAN Users
    144
- Industry Canada (IC) Notices
  144
  - Regulatory Compliance Information for EUROPEAN Users
    145
- European Usage Restrictions
  145
- European EMC Compliance Statement
  146
- European Safety Compliance Statement
  147
  - Laptop Operation
    148
Chapter 6 Sampling Procedure

148
- Survey Mode
  149
- Sampling Procedure
  149
- Quick Reference SOP - Running Survey Mode
  153
  - ANALYZE (GC/MS) Mode with the Concentrator
    153
  - Tri- Bed Concentrator
    153
  - Tenax Concentrator
    154
  - Quick Reference SOP - Tri-Bed Concentrator Method
    158
    
    Selecting a New Method
    158
    
    ER IQ Software
    162
Chapter 7 HAPSITE Software - er IQ

162
- Computer System Requirements
  162
  - Software Installation
    162
  - System Setup Screen
    163
    
    Introduction
    163
  - System Setup Menu
    163
- File Menu
  164
- View Log
  165
- Log File Toolbar
  166
  - Functions Menu
    167
  - System
    167
  - Port Settings Tab
    168
  - Display Tab
    168
  - Miscellaneous Tab
    169
    
    Tools Menu
    174
  - Set Access Level
    174
- Changing Access Levels
  175
- Setting or Changing the Access Level Password
  176
  - View Menu
    177
  - Window Menu
    178
  - Help Menu
    179
    
    Safety DB
    179
    
    Manage Files
    182
    
    Status Icon
    186
  - Status Properties
    186
  - HAPSITE er Time Zone
    187
  - HAPSITE er Information
    191
  - Pressure Flows and Temperatures
    192
  - NEG Status
    193
  - Functions
    196
  - Parameters
    197
  - Service Module
    198
    
    Front Panel Display Icon
    198
    
    HAPSITE Sensor Icon
    199
  - Update HAPSITE Software
    200
  - Bring Online
    200
- Communication Messages
  200
  - Disconnect
    200
    
    HAPSITE Icons
    201
    
    Data Review
    204
Chapter 8

204
- Introduction
  204
- Data Review Toolbar
  204
- Accessing the Data Review Feature
  205
- Reports
  208
- Using the Zoom Function in the TIC/RIC Window
  213
- Zooming out
  216
- Using the Zoom Spectrum Function
  217
  - Analyzing Data Using AMDIS
    219
- Setting the AMDIS Pathway
  221
- View Function in AMDIS
  224
- Confirm Screen in AMDIS
  225
  - NIST Library Searches
    227
  - Show/Update Current Peaks
    231
- Show/Update Current Peaks Window Description
  234
- Peak Search Parameters
  236
- NIST Search Setup
  236
- Report Preview
  239
  - Background Subtract
    241
  - Background Subtraction Using a Range of Points
    243
    
    Range Tool
    245
  - Additional Features of the Range Tool
    247
    
    Displaying Reconstructed Ion Chromatograms (RIC)
    247
    
    Chromatogram Overlay
    252
    
    Chromatogram Subtract
    255
    
    Right-Click Menus Within Data Review
    257
    
    Right-Clicking in the TIC Window
    257
- Properties Menu
  259
  - Spectrum Window
    260
  - Analyzing Data Using NIST
    262
  - NIST Database Program
    263
  - Grab Spectra for NIST
    264
    
    Tune
    266
Chapter 9

266
- Introduction to Autotune and Manual Tune
  266
- Autotune
  266
- Starting Autotune from the Manual Tune Screen on Laptop Computer
  266
  - Viewing a Tune Report
    268
  - Tune Reports Options
    270
    
    Performing Manual Tune
    272
    
    Outputs
    273
    
    Inputs
    274
    
    Other Inputs
    277
    
    Set Access Level to Advanced
    278
    
    Manual Tune
    279
    
    Save Tune
    280
    
    Tool Bar
    281
    
    Tune Drop-Down Menu
    282
    
    Tune Control Panel
    285
- Tune Parameters
  286
  - Peak Scan Window
    288
- Peak Scan Window Controls
  288
  - Setting the Full Scan Range
    289
  - Tune and Mass Calibration Status
    290
  - Mass Calibration Status
    291
  - Scan Window Menu
    292
  - Tune Status Window Menu
    293
    
    Method Editor
    294
Chapter 10

294
- The Method Editor
  294
- Reloading Default HAPSITE Methods
  296
- Loading Default Methods
  296
  - Default Methods
    299
  - Description Page
    300
  - Startup Page
    304
  - Inlet Page
    306
- Inlet States
  307
- GC Temperature Profile
  311
- Scan Events
  312
- Headspace Flow Parameter
  313
- Situprobe Flow Parameter
  313
- Scan Events for SIM Methods
  314
  - Tune Page
    314
- Param Page
  315
- Report Page
  317
  - Full Scan Page
    318
  - SIM Page
    319
- SIM for Analyze
  319
- SIM for Survey
  322
- Creating a SIM Method
  323
  - Search Page
    330
- Setting up a Qualitative Search
  331
- Setting up a Quantitative Search
  336
- Peak Search
  337
- Alarm
  340
- Edit Options
  343
- Template/Calibration Files
  350
- View Reports
  350
  - Data Page
    353
- Data File Information
  353
- Date and Time Appendix
  354
- Data Display
  356
  - Summary Page
    357
  - Method Sequence
    357
Chapter 11

362
- Introduction to Quantitative Analysis
  362
- Calibrating a Method
  362
- Definition of Terms in the Calibrate Window
  380
- Method
  380
- Data Files
  380
- Peak Search
  381
- Analytes
  382
- Reports
  382
- Extracted Mass Peaks
  384
- Calibration
  385
  - Build/Edit Template Menu
    385
  - ID Unknowns
    385
  - Definition of Terms in the ID Unknowns Window
    389
- Method
  389
- Data Files
  390
- Peak Search
  390
- Analytes
  390
- Reports
  390
  - Display Function
    392
Chapter 12

393
- Introduction
  393
- HAPSITE Symptom - Cause - Remedy Chart
  393
- Saturation of the Probe and Probe Line
  397
- Symptoms
  397
- Decontaminate Saturation
  397
Chapter 13

407
- HAPSITE Part Number
  407
- HAPSITE er Accessories
  408
- HAPSITE er Spare Parts
  408
- HAPSITE Consumables
  409
- Headspace Spare Parts
  410
- Service Module Spare Parts
  411
- HAPSITE Situprobe Spare Parts
  411
Chapter 14

412
- Glossary
  412
- HAPSITE Target Compounds
  419
- Compounds in Order of Elution
  419
  - Calibrating Gas Mixtures
    420
Appendix B Acquisition, Preparation, and Handling

420
Appendix C

426
- Introduction
  426
- Shipping the Canisters
  426
- Empty Canisters
  428

Inficon HAPSITE ER Operating Manual (436 pages)

Chemical Identification System

Brand: Inficon | Category: Measuring Instruments | Size: 16.9 MB

Table of Contents
3
Declaration of Conformity
12
Two Year Warranty
14
Disclaimer and Copyright
16
Definition of Note, Hint, Danger, Warning and Caution Paragraphs
17
Operating Manual Style Conventions
18
Customer Support
19
How to Contact Customer Support
19
Returning Your Instrument to INFICON
19
Introduction
21
System Description
21
Instrument and Accessories
21
Specifications
22
Instrument Overview
22
Description of Subsystems
23
Gas Chromatograph
23
Membrane Isolation Valve
24
Mass Spectrometer
24
Vacuum System
26
Electronic Systems
27
Software Systems
27
HAPSITE Components and Assemblies
28
Ship Kit Packing Lists
28
930-850-G5, G6, G7, G8 Ship Kit Contents
28
Basic Assembly
30
Attaching the Probe
30
Installing the Gas Canisters
32
How to Remove a Gas Canister
37
Connect the Power Supply
40
Connecting the Laptop
42
Connect the Laptop with the Black Crossover Cable
42
Connect Laptop with Wireless Connection
44
Battery
45
Battery Charger
45
Battery Charger Connections and Startup
45
Loading the Battery Charger
46
Understanding the Battery Charger Indicators
47
Testing Battery
47
Installing the Battery
48
Removing the Battery
48
Helpful Guidelines
50
Operate the Instrument in Portable Mode
51
Start HAPSITE er in Portable Mode
51
Emergency Mode (EMER MODE)
59
Concentrator Options (CONC OPTIONS)
63
Concentrator Cleanout
63
Skip Cleanout
67
Concentrator Cleanout Failure
69
Quick Reference SOP- Heat-Up and Tune
71
Select a Different Method Using the SELECT METHOD Icon
71
Change the Default Method
75
Show All
77
Survey Mode
77
Quick Reference SOP - Survey Method
85
ANALYZE (GC/MS) Mode with the Concentrator
86
Tri-Bed Concentrator
86
Tenax Concentrator
86
Procedure for Running Concentrator Methods
86
Quick Reference SOP - Concentrator Methods
92
Detecting Hazardous Chemicals
92
Help Icon
93
Info Icon
94
EXIT Menu
103
Extended Standby
105
End Standby
108
Communications and Touch Screen Options
110
Communications
110
Wireless Range
110
Turning on the Radio
110
Wireless Module Indicator Lights
112
Setting up Communications
112
Configuring the Instrument for Communications
119
Turning off the Radio
130
Wireless Information
132
Regulatory Compliance Information for UNITED STATES Users
132
FCC Statement
133
FCC RF Exposure Statement
133
Regulatory Compliance Information for CANADIAN Users
134
Industry Canada (IC) Notes
134
Regulatory Compliance Information for EUROPEAN Users
134
European Usage Restrictions
135
European EMC Compliance Statement
136
European Safety Compliance Statement
138
Laptop Operation
139
Sampling Procedure
139
Survey Mode
139
Sampling Procedure
140
Quick Reference SOP - Running Survey Mode
143
ANALYZE (GC/MS) Mode with the Concentrator
143
Tri-Bed Concentrator
143
Tenax Concentrator
144
Quick Reference SOP - Tri-Bed Concentrator Method
148
Selecting a New Method
149
ER IQ Software
152
HAPSITE Software - er IQ
152
Computer System Requirements
152
Software Installation
152
System Setup Screen
152
Introduction
153
System Startup Menu
153
File Menu
153
Functions Menu
157
System
157
Port Setting Tab
158
Display Tab
159
Miscellaneous Tab
160
Tools Menu
167
Set Access Level
168
View Menu
170
Window Menu
171
Help Menu
171
Safety Database
172
Manage File
175
Status Icon
180
Status Properties
180
HAPSITE Time Zone
181
HAPSITE Information
189
Pressure Flows and Temperatures
190
NEG Status
191
Functions
195
Parameters
196
Service Module
197
Front Panel Display Icon
198
HAPSITE Sensor Icon
199
Update HAPSITE Software
200
Bring Online
200
Communication Messages
200
Disconnect
201
HAPSITE Icons
201
Data Review
203
Chromatogram Overlay
203
Introduction
205
Data Review Toolbar
205
Accessing the Data Review Feature
206
Reports
210
Using the Zoom Function in the TIC/RIC Window
215
Zooming out
219
Using the Zoom Spectrum Function
220
Analyzing Data Using AMDIS
222
Setting the AMDIS Pathway
224
View Function in AMDIS
227
Confirm Screen in AMDIS
228
NIST Library Searches
230
Current Peaks
235
Show/Update Current Peaks
236
Show/Update Current Peaks Window Description
241
Peak Search Parameters
243
NIST Search Setup
243
Report Preview
247
Background Subtract
251
Background Subtraction Using a Range of Points
254
Additional Features of the Background Tool
255
Range Tool
256
Additional Features of the Range Tool
258
Displaying Reconstructed Ion Chromatograms (RIC)
259
Chromatogram Subtract
263
Right-Click Menus Within Data Review
267
Right-Clicking in the TIC Window
267
1Properties Menu
269
Spectrum Window
270
Analyzing Data Using NIST
271
NIST Database Program
272
Grab Spectra for NIST
273
Tune
276
Introduction to Autotune and Manual Tune
276
Autotune
276
Viewing a Tune Report
277
Tune Report Options
280
Performing Manual Tune
283
Manual Tune Variables
283
Outputs
284
Inputs
285
Other Inputs
287
Set Access Level to Advanced
288
Manual Tune
288
Save Tune
289
Tool Bar
289
Tune Drop-Down Menu
290
Tune Control Panel
292
1Tune Parameters
293
Peak Scan Window
294
1Peak Scan Window Control
295
Setting the Full Scan Range
296
Tune and Mass Calibration Status
297
Mass Calibration Status
298
Scan Window Menu
299
Tune Status Window Menu
299
Method Editor
301
The Method Editor
301
Reloading Default HAPSITE Methods
303
Loading Default Methods
303
Default Methods
306
Description Page
307
Startup Page
310
Inlet Page
313
Inlet States
313
GC Temperature Profile
318
Scan Events
319
Headspace Flow Parameter
320
Situprobe Flow Parameter
321
Scan Events for SIM Methods
322
Tune Page
322
Param Page
322
Report Page
324
Full Scan Page
325
SIM Page
327
SIM for Analyze
327
SIM for Survey
328
Creating a SIM Method
329
Search Page
336
Setting up a Qualitative Search
338
Setting up a Quantitative Search
342
Peak Search
344
Alarm
346
Edit Options
348
Template/Calibration Files
356
View Reports
356
Data Page
361
Data File Information
362
Date and Time Appendix
363
Data Display
364
Summary Page
365
Method Sequence
365
Calibration
370
Introduction to Quantitative Analysis
370
Calibrating a Method
370
Definition of Terms in the Calibrate Window
390
Method
391
Data Files
391
Peak Search
391
Analytes
392
Reports
392
Extracted Mass Peaks
394
Calibration
394
Build/Edit Template Menu
395
ID Unknowns
395
Definition of Terms in the ID Unknowns Window
399
Method
399
Data Files
399
Peak Search
400
Analytes
400
Reports
400
Display Function
401
Maintenance
402
Introduction
402
HAPSITE Symptom - Cause - Remedy Chart
402
Saturation of the Probe and Probe Line
405
Symptoms
405
Decontaminate Saturation
405
NEG Troubleshooting
405
Attaching HAPSITE to the Service Module
406
Bakeout Procedure
412
Reactivating the NEG Pump
414
Part Numbers
417
HAPSITE Part Numbers
417
HAPSITE Accessories
417
HAPSITE Spare Parts
418
HAPSITE Consumables
419
Service Module Spare Parts
419
Glossary
420
Appendix A: HAPSITE Target Compounds
424
Compounds in Order of Elution
424
Appendix B: Calibrating Gas Mixtures
426
Acquisition, Preparation, and Handling
426
How to Establish the Desired Concentrations
426
Using Cylinders Containing each Concentration
427
Diluting the Gas On-Site
428
Correct Delivery of the MIX to the Inlet of the HAPSITE
428
Free Flow of Gas
428
Inert Sample Bag
429
Appendix C: Shipping the HAPSITE and Consumables
432
Introduction
432
Shipping the Canisters
432
Empty Canisters
434

Inficon Categories

Security Sensors Measuring Instruments Controller Test Equipment Gas Detectors

More Inficon Manuals

Inficon HAPSITE ER Portable GC/MS Manuals

Inficon HAPSITE ER Operating Manual (432 pages)

Table of Contents

Operating Manual Style Conventions

Chapter 1

Chapter 2 HAPSITE er System

Chapter 3 Ship Kit Packing Lists

Chapter 4 Starting HAPSITE er in Portable Mode

Chapter 5 Communications

Chapter 6 Sampling Procedure

Chapter 7 HAPSITE Software - er IQ

Chapter 8

Chapter 9

Chapter 10

Chapter 11

Chapter 12

Chapter 13

Chapter 14

Appendix B Acquisition, Preparation, and Handling

Appendix C

Inficon HAPSITE ER Operating Manual (436 pages)

Table of Contents

Related Products

Inficon Categories