Inficon HAPSITE Smart Manuals

Inficon HAPSITE Smart Manuals

Manuals and User Guides for Inficon HAPSITE Smart. We have 1 Inficon HAPSITE Smart manual available for free PDF download: Operating Manual

Inficon HAPSITE Smart Operating Manual

Inficon HAPSITE Smart Operating Manual (554 pages)

Chemical Identification System

Brand: Inficon | Category: Measuring Instruments | Size: 42.11 MB

Table of Contents

Operating Manual Style Conventions
14
Table of Contents
15
Chapter 1

29
- Introduction
  29
- The HAPSITE Smart System
  29
- Performance Specifications
  30
- Serial Number Location
  30
- Theory of Operation
  31
- Description of Subsystems
  32
- Gas Chromatograph
  32
- Instrument Overview
  32
- Membrane Isolation Valve
  34
  - Mass Spectrometer
    34
  - Vacuum System
    36
  - Electronic Systems
    37
- Gas Chromatograph Control
  37
- Interfaces
  37
  - Software Systems
    37
    
    HAPSITE Components and Assemblies
    39
- Main Processor
  37
- Mass Spectrometer Control
  37
Chapter 2

39
Chapter 3 Starting the HAPSITE in Portable Mode

89
- Quick Reference SOP - Heat-Up and Tune
  94
- Extended Standby
  134
- Cold Standby
  136
- Shutdown System
  138
- Rebooting the HAPSITE
  140
- Restart Program
  141
  - Wireless and USB
    143
Chapter 4

143
- Introduction
  143
- FCC Compliance Information
  143
- FCC Information - Information for U.S.A. Users
  144
- FCC Statement
  144
  - FCC RF Exposure Statement
    144
  - IC Notice - Information for Canadian Users
    145
    
    Wireless Range
    145
    
    Turning the Radio on
    146
    
    Establishing Communication
    147
  - Setting the User Access Level
    147
  - Configuring the HAPSITE for Wireless Communication
    148
- Setting up Smart IQ for Communication with the HAPSITE
  148
- Setting the IP Address
  150
  - Configuring the Laptop for Wireless Communication
    153
    
    Wireless Module Indicator Lights
    153
    
    Turning the Radio off
    154
    
    Saving Files to the USB
    155
    
    Retrieving Files from the USB Drive
    157
    
    Reviewing the Data Retrieved from the USB
    159
    
    Operating HAPSITE in Laptop Mode
    161
Chapter 5 Starting the HAPSITE in Laptop Mode

161
Chapter 6 Introduction to Methods

203
- Sensitivity
  203
  - Survey Method
    203
- Building a Survey Method Library File
  205
- Building a Survey Target Compound Library
  205
  - GC/MS Methods
    208
  - Building a GC/MS Method and Target Compound Library File
    210
    
    Tune
    211
- Creating Survey Methods for Target Compounds
  205
Chapter 7

211
- Introduction to Autotune and Manual Tune
  211
- Autotune
  212
- Starting Autotune from the Manual Tune Screen
  214
  - Viewing a Tune Report
    215
  - Autotune Failure
    217
  - Manual Tune Settings and Controls
    219
- Tool Bar
  221
- Tune Drop down Menu
  222
- Tune Properties Window
  223
  - Tune Control Panel
    224
- Tune Parameters
  225
  - Peak Scan Window
    227
- Peak Scan Window Controls
  227
  - Full Scan Window
    229
  - Tune and Mass Calibration Status
    230
  - Mass Calibration Status
    232
  - Right Mouse Button (RMB) Menus
    233
- RMB in Scan Window
  233
- RMB in Tune Status Window
  234
- RMB on y Axis
  235
  - Performing Manual Tune
    235
  - Adjusting Base Peak Gain
    236
  - Adjusting Resolution
    239
  - Adjusting the Ion Energy
    241
    
    Smart IQ Software
    245
Chapter 8

245
- The HAPSITE Software - Smart IQ
  245
- Computer System Requirements
  246
- Installing and Updating the HAPSITE Smart
  246
- Changing Access Levels
  278
- Setting or Changing the Access Level Password
  279
  - Smart IQ Controls
    280
- System Setup Main Menu
  281
- File
  281
- Functions
  281
- System
  281
- Help Menu
  282
  - Software Versions for the HAPSITE and Laptop
    282
  - HAPSITE Icons
    283
    
    Data Review
    287
- Tools Menu
  282
- View Menu
  282
- Window Menu
  282
Chapter 9

287
- Introduction to Data Review
  287
- Accessing the Data Review Feature
  288
- Data Review Toolbar
  291
- RMB Menus Within Data Review
  292
- RMB in the TIC/RIC Window
  292
- RMB in the Spectrum Display Window
  294
- Steps Required to Perform a One Point Background Subtraction
  297
- Background Subtraction Using a Range of Points
  299
- Additional Features of the Background Tool
  300
  - Utilizing the Range Tool
    300
- Steps Required to Range Acquisition
  301
- Additional Features of the Range Tool
  302
  - Using the Zoom Function
    302
  - Using the Zoom Function in the TIC/RIC Window
    302
  - Using the Zoom Spectrum Function
    304
    
    Displaying Reconstructed Ion Chromatograms (RIC)
    305
    
    RIC Plot to Locate Specific Compounds
    306
    
    NIST Library Searches
    309
    
    Searching Peaks
    311
    
    Analyzing Data Using AMDIS
    315
    
    How to Access AMDIS
    315
- Accessing NIST from AMDIS
  317
  - Analyzing Data Using NIST
    318
  - How to Grab Spectra/Utilize the Full NIST Program
    319
    
    Method Generated Reports
    320
    
    Reporting and Printing Data
    320
    
    Reports Generated from Peaks Menu
    322
    
    Smart IQ Hot Keys
    323
    
    Saving and Managing Files
    325
Chapter 10 Saving Files on the HAPSITE

325
- Method Files
  325
- Event Log Files
  327
- Data Files
  327
- Tune Files
  328
- Data Review
  330
  - Saving Files to the PC
    332
- Method Files
  333
- Event Log Files
  334
- Data Files
  335
- Tune Files
  335
- Report Files
  335
  - Transferring Files between the HAPSITE and PC
    335
  - Saving, Retrieving and Reviewing Files Using the USB Drive
    337
    
    Method Editor
    339
Chapter 11

339
- The Method Editor
  339
- Description Page
  341
- Full Scan Method
  343
- SIM Method
  344
  - Startup Page
    345
- Headspace
  347
- Situprobe
  348
  - Inlet Page
    348
- Inlet States
  350
- GC Temperature Profile
  355
- Use Internal Standard
  356
- Scan Events
  356
- Concentrator Selection
  357
- Headspace Flow Parameter
  357
- Situprobe Flow Parameter
  358
  - Tune Page
    358
- Param Page
  358
- Report Page
  358
  - Full Scan Page
    361
  - SIM Page
    363
- SIM for GC/MS
  364
- SIM for Survey
  366
  - Search Page
    368
- Setting up a Qualitative Search
  369
- Setting up a Quantitative Search
  374
  - Data Page
    379
  - Summary Page
    382
  - How to Create a Method
    383
- Creating a New Custom Method from an Existing Method
  383
  - How to Sequence Methods
    386
    
    Target Compound Methods
    391
Chapter 12

391
- Introduction to Quantitative Analysis
  391
- Definition of Terms in the Calibrate Window
  392
- Method
  392
- Data Files
  392
- Peak Search
  393
- Analytes
  394
- Reports
  394
- Extracted Mass Peaks
  396
- Calibration
  396
  - Definition of Terms in the ID Unknowns Control Panel
    396
- Method
  396
- Data Files
  397
- Peak Search
  397
- Analytes
  398
- Reports
  398
- Extracted Mass Peaks
  399
- Calibration
  399
  - Display Function
    400
  - The Quantitation
    402
  - Using the Calibrate Function
    402
  - Using the ID Unknown Function
    410
    
    Headspace Sampling System
    413
Chapter 13 Introduction

413
- How the HSS Operates
  414
- Performance Specifications
  415
- HSS Indicators
  415
- Consumables Required
  416
- Connecting the HSS to the HAPSITE
  417
- Providing Power to the HSS
  417
- If AC Power Is Available
  417
- If AC Power Is Not Available
  417
  - Using the HAPSITE with HSS
    417
  - Powering on the HSS
    418
  - Loading the Vials
    418
  - Loading the Wells
    422
  - Cycling the Vials
    424
  - Making the Measurement
    425
    
    Maintenance of HSS
    425
  - Clean out after a High Concentration Sample
    425
- Purge Procedure
  425
  - Cleaning up a High Background
    425
- Flush Procedure
  426
  - Cleaning the HSS Wells
    427
  - Washing the HSS
    428
  - Replacing the HSS Battery
    429
  - Replacing the HSS Nitrogen Canister
    430
    
    Shipping the HSS
    430
    
    Charging the HAPSITE Battery Using the HSS
    431
    
    Service Module
    433
Chapter 14

433
- Introduction
  433
- Service Module Input Power
  434
- Service Module 110 / 220 V(Ac) Input
  434
- Service Module 24 V(DC) Input
  434
  - Components of the Service Module
    435
- Backup Batteries
  435
- Mdp/Turbo Pump
  435
- Manifold Vent Valve
  435
- Foreline Vent Valve
  436
- Roughing Pump
  436
- Vacuum Interconnect Valve Actuator
  436
- Battery Charger
  436
- Power Supply
  437
- Communications
  437
  - When to Use the Service Module
    438
  - Smart IQ Software for the Service Module
    439
- The Service Module Tab in Properties Window
  440
  - Starting up HAPSITE on the Service Module
    443
  - Attaching the HAPSITE to the Service Module
    444
- Attaching the HAPSITE to the Service Module Using the Smart IQ PC Software
  445
- Attaching the HAPSITE to the Service Module Using the HAPSITE Front Panel Controls
  447
  - Detaching the HAPSITE
    449
- Using the Smart IQ Software to Detach
  449
- Using the Front Panel Display to Detach
  450
Chapter 15

459
- Introduction
  459
- Safety Considerations
  460
- HAPSITE Symptom - Cause - Remedy Chart
  461
- Required Environment for General Maintenance
  465
- Contamination
  465
- Contamination of the Mass Spectrometer
  466
- Decontaminate
  466
  - Contamination of the Probe and Probe Line
    467
- Decontamination
  466
  - Contamination of the Gas Chromatograph
    466
- Symptoms
  466
- Decontaminate
  467
- Symptoms
  467
- If no Indicators Are Illuminated
  515
- If a Battery Does Not Accept a Charge
  516
- If the Red Indicator Is Flashing
  516
Chapter 16

517
- Glossary
  517
- Customer Support
  529
Chapter 17

529
- How to Contact Customer Support
  529
- Returning Your Instrument to INFICON
  529
  - Part Numbers
    531
Chapter 18

531
- HAPSITE Part Number
  531
- HAPSITE Smart Accessories
  531
- HAPSITE Smart Spare Parts
  532
- HAPSITE Smart Consumables
  533
- HAPSITE Upgrade (for 930-280-GX Series HAPSITE)
  534
- HAPSITE Smart Training
  534
- On-Site Training Course
  534
- Syracuse Training Course
  535
- Usage Fees
  535
  - Headspace Spare Parts
    535
  - Service Module Spare Parts
    536
  - HAPSITE Situprobe Spare Parts
    536
    
    HAPSITE Target Compounds
    537
Appendix A Compounds in Order of Elution

537
Appendix B Acquisition, Preparation, and Handling

539

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