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Inficon 3000 Micro GC Gas Analyzer Manuals
Manuals and User Guides for Inficon 3000 Micro GC Gas Analyzer. We have
2
Inficon 3000 Micro GC Gas Analyzer manuals available for free PDF download: Operating Manual, Reference Manual
Inficon 3000 Micro GC Operating Manual (268 pages)
Gas Analyzer
Brand:
Inficon
| Category:
Measuring Instruments
| Size: 16.72 MB
Table of Contents
Table of Contents
9
Introduction
19
Chapter 1
19
About the Instrument
19
Definition of Notes, Warnings and Cautions
21
Safety Overview
22
Cleaning 3000 Micro GC
24
Electromagnetic Compatibility
25
Sound Emission Certification for Federal Republic of Germany
25
Specifications
27
Chapter 2
27
3000 Micro GC Specifications
27
Environmental Conditions
28
Instrument Specifications
28
Sample Inlet Specifications
28
Sample Injector Specifications
28
Column Heater Specification
28
TCD Specifications
28
Repeatability
29
Carrier Gas Specifications
29
Portable 3000 Micro GC Carrier Gas Specifications
29
External Input/Output
29
Portable 3000 Micro GC Onboard Battery
29
Safety and Regulatory Standards
30
Overview
31
Chapter 3
31
Overview of 3000 Micro GC Instrument and Accessories
31
3000 Micro GC Chassis
32
1,2-Channel Chassis
32
3,4-Channel Chassis
33
Portable Chassis
34
The 3000 Micro GC Module
35
Principle of 3000 Micro GC Module Operation
35
Injector Flow Assembly
37
Injectors
38
Variable Injector (Timed)
38
Variable Large Volume Injector (Timed)
38
Fixed Injector
39
Backflush Injector
40
Columns
41
Detector
42
D-Board
42
Enhanced D-Board
42
Standard D-Board
42
Module Cases
43
Standard Module Case
43
Modbox Module Case
43
3000 Micro GC Chassis Components
44
Inlet Tubing
44
C-Board
45
OBC Board
45
Sample Pump
46
Carrier Gas Weldment
47
Carrier Gas Inlet
48
Vents
49
Remote Control Module
50
Sample Conditioners
51
EZ IQ Chromatography Software
52
Product Identification
53
1,2-Channel and Portable 3000 Micro GC Part Numbering
54
3,4-Channel 3000 Micro GC Part Numbering
55
Serial Number
55
Identification Number
56
Installation
57
Chapter 4 Site Preparation
57
List of Required Tools
57
Tubing and Fitting Requirements
57
Site Requirements
58
Electrical Requirements
58
Space and Venting Requirements
58
Computer Requirements
58
Gas and Regulator Requirements
59
Carrier Gas and Regulator Requirements
59
Calibration Gas and Regulator Requirements
59
Instrument Hardware Setup
60
Unpacking the Instrument
60
Shipping Kit Contents
60
Shipped with Every Instrument
60
Configuration Dependent Parts
61
1,2-Channel and 3,4-Channel 3000 Micro GC Specific Parts
61
Portable 3000 Micro GC Specific Parts
61
Sample Inlet Parts
61
Gas Inlet Parts
61
GC Module Parts
61
Power Cords - Country Dependent
61
Making Carrier Gas and Sample Inlet Connectors
62
Connecting the Carrier Gas
64
Gas Safety
64
Connecting the Carrier Gas Particulate Filter
65
Setting the Gas Pressure
66
Purge the Carrier Gas Line
66
Connecting the Carrier Gas to the 3000 Micro GC
67
Using the Onboard Carrier Gas Cylinder
67
Installing the Sample Inlet Filter
68
Sample Inlet Filter Parts List
68
Tools Required
69
Sample Inlet Filter Assembly Installation
69
Power and Communication Cable Setup
70
Instrument Configuration Setup
71
Turn on 3000 Micro GC
71
IP Address Configuration
72
Carrier Gas Configuration
73
Ping the Instrument
73
Chromatography Software Installation
74
Accessory Installation
75
Chapter 5 Sample Conditioners
75
List of Sample Conditioners and Ipns
75
Installing the 10 Micron Sample Inlet Filter
77
Installing the Genie Filter Assembly
77
Tools Required
77
User Supplied Parts
78
Installation Instructions for the Genie Filter Assembly
78
Installing the Pressure Reducer
82
Tools Required
82
User Supplied Parts
82
Installation Instructions for the Pressure Reducer
83
Installing the Pressure Reducer and Genie Filter Assembly
86
Tools Required
86
User Supplied Parts
86
Genie Filter Assembly
86
Installing Heated Sample Introduction Accessories
91
Heated Regulator
92
Target Analytes
93
Heated Regulator Accessory Contents
93
Heated Vaporizer
94
Heated Vaporizer Accessory Contents
95
Installation
95
Tools and Supplies Required
95
User Supplied Parts
96
Prepare the 3000 Micro GC and Sample Introduction Accessory
96
Installing the Transfer Line
97
Mounting the Heated Sample Conditioners
98
Install the Vent Tubing and Connect to Power
100
Installation for 3,4-Channel 3000 Micro Gcs
101
Heated Regulator/Vaporizer Part Numbers
102
The Remote Connector
104
EZ IQ Operation to Activate Remote Start/Cancel Function
106
Multi-Position Valve Installation and Setup
107
Valve Hardware/Software Requirements
107
Valve Configuration
108
Valve Hardware Connections
108
Embedded Web Page Operation
109
Instrument Setup through
109
Chapter 6 Overview
109
Determine Basic 3000 Micro GC Configuration
109
Determining 3000 Micro GC Advanced Configuration
111
Status
114
Check GC Module Parameters
114
Check the Duty Cycle
114
Utilities
115
Set Date/Time
115
Restart
116
Shutdown
116
Support
116
Remove or Replace a GC Module
116
Change GC Module Address
116
Change Carrier Gas Configuration
117
Change IP Address
121
IP Configuration
121
Access the Embedded Web Page Via a Fixed IP Address
124
Basic EZ IQ Operation
129
Chapter 7
129
Introduction
129
Connecting EZ IQ with 3000 Micro GC
129
Configuring EZ IQ to Use a Valco (VICI) Valve
132
Configuring a Valco (VICI) Switching Valve
133
Configuring a Valco (VICI) Sampling Valve
135
Navigating EZ IQ
137
EZ IQ Workflow
139
Basic Method Development
140
Creating a New Method
141
Opening a Method
144
Downloading a Method
145
View Instrument Status
146
Run a Sample
147
Basic Sequencing
148
Scheduling Runs
148
Integrating the Chromatogram
149
About Integration Events
149
Common Integration Events
150
Width
150
Threshold
150
Integration off
151
Add or Edit Integration Events
151
Manually Add or Edit Integration Events
151
Graphically Programming Integration Events
153
Annotate a Chromatogram
154
Qualify Peaks
154
Adding Peak and Group Information
156
Manually Add Peak Information
156
Define Peaks Graphically
157
Adding Groups
161
Adjust Peak Windows
162
Calibration
164
Enter Concentration Amounts in the Peaks/Groups Table
164
Obtain Preliminary Data for Calibration
164
Perform a Single Level Calibration
165
Perform a Multiple Level Calibration
168
Review Calibration
169
Generate Standard Reports
170
Method Reports
170
Customize a Method Report
170
Custom Method Report Features
171
Importing a Template File
172
Save a Custom Method Report
173
View or Print a Custom Method Report
174
External Standard (ESTD) Reports
175
Customize an ESTD Report
175
Save a Customized ESTD Report
175
View and Print an ESTD Report
176
EZ IQ Operation to Activate Remote Start/Cancel Function
177
Apply the Valco Valve Program to EZ IQ Method
180
Valco Valve Setup in EZ IQ
180
Running a Sample with a Valco Valve
181
Running a Sequence with a Valco Valve
182
Chapter 8 Routine Operation
183
System Bakeout
183
Shutdown/Restart
185
Standby
186
Remove and Replace a 3000 Micro GC Module
187
Types of Replacement Modules
187
Performance Enhanced GC Module Vs. Standard GC Module
187
Update the Instrument Firmware
188
Decommission a Standard GC Module
189
Remove a GC Module
193
Install a GC Module
198
Commission a New Standard GC Module
202
Enable the Instrument in EZ IQ
204
Sample Conditioners
205
Sample Conditioner Connections
205
Connections for Sample Inlet Filter (PN G2801-60900), Pressure Reducer (PN G2815A), Pressure Reducer and Genie Filter Assembly (PN G2816A), and Genie Filter Assembly (PN G2817A)
205
Connections for the Heated Regulator (PN G2818A-X/G2845A-X/G2857A-X)
205
Connections for the Heated Vaporizer (PN G2819A-X/G2846A-X/G2858A-X)
205
Running a Low Pressure, Clean Gas Sample
206
Running a Low Pressure, Liquid/Particulate Containing Gas Sample
207
Running a High Pressure Gas Sample Without Liquids/Particulates
208
Running a High Pressure Gas Sample with Liquids/Particulates
209
Running a High Pressure Gas Sample Containing C6+ Components
210
Using a Sample Vessel
210
Using a Transfer Line or Other Continuous Sample Source
212
Running a High Pressure Liquid Petroleum Gas Sample
214
Consumable Replacement Procedures
217
Replacing the External 10 Micron Sample Inlet Filter Disk
217
Replacing the 2 Micron Filter in the Heated Vaporizer (PN G2819A-X/G2846A-X/G2858A-X)
218
Replacing the 7 Micron Filter in the Heated Regulator (PN G2818A-X/G2845A/G2857A)
219
Battery Usage Information
220
General Information and Cautions of the Portable 3000 Micro GC
220
Portable 3000 Micro GC Operation
220
To View the Battery Status
221
Charging the Battery
221
Replace the Battery
222
Onboard Carrier Gas Supply
224
Refill Onboard Carrier Gas Cylinder
225
Before Turning off the Carrier Gas
228
Troubleshooting
229
Chapter 9 Symptom, Cause, and Remedy Tables
229
Common Chromatographic Problems
229
Common Software Problems
233
Common Connection Problems
236
Common Hardware Problems
237
Common Chromatographic and Method Problems
238
Chromatographic Problems
238
Baseline Symptoms
238
Baseline Position
238
Baseline Wander and Drift
239
Baseline Noise
240
Baseline Spiking
240
Retention Time Symptoms
241
Retention Time Drift
241
Retention Time Wander (Reproducibility)
241
Peak Symptoms
242
No Peaks
242
Inverted Peaks
242
Extra Peaks
243
Deformed Peaks
244
Peak Fronting
244
Peak Tailing
244
Deformed Peak Apex
245
Split Peak Apex
245
Method Problems
246
Column and Detector Bakeout
246
Correcting Instrument Parameter Settings
246
Adjusting Column Head Pressure
246
Recalibrating
246
Service and Technical Support
247
Chapter 10
247
How to Contact Customer Support
247
Returning 3000 Micro GC to INFICON
247
Warranty Extension
247
Service Contract
248
Replacement Parts and Gases
249
Chapter 11
249
Power Cables and Converters
249
GC Modules
251
Description of GC Module Numbers
251
Reference Number on Top of GC Module
251
New Module Part Number
251
Refurbished Module Part Number
251
New Module Replacement Part Number
251
Standard Modules
252
Standard Modules Table
253
Performance Enhanced Modules
257
Performance Enhanced Modules Table
258
Discontinued Module Replacement Ipns
262
Sample Accessories and Filters
263
Sample Conditioners
263
Filters
264
Other Support Parts
264
Checkout Gases
265
Universal Checkout Gas
265
NGA Checkout Gas
266
RGA Checkout Gas
267
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Inficon 3000 Micro GC Reference Manual (108 pages)
gas analyzer
Brand:
Inficon
| Category:
Measuring Instruments
| Size: 9.45 MB
Table of Contents
Title Page
3
Trademarks
4
Copyright
4
Purpose of this Reference Guide
5
How to Contact Customer Support
7
Table of Contents
9
3000 Micro GC Guide 1
11
Configuring a PC for a Direct Connection to 3000 Micro GC Via the Crossover Cable
11
3000 Micro GC Guide 2
15
Connecting to 3000 Micro GC Via the Static IP Address
15
3000 Micro GC Guide 3
19
Changing the Instrument IP Address
19
3000 Micro GC Guide 4
23
Changing the Carrier Gas Configuration
23
3000 Micro GC Guide 5
27
Installing EZ IQ
27
Configuring a 3000 Micro GC with EZ IQ
31
3000 Micro GC Guide 6
31
3000 Micro GC Method Setup
33
3000 Micro GC Guide 8
37
Running a Sample
37
3000 Micro GC Guide 9
39
Integrating Chromatograms
39
3000 Micro GC Guide 10
41
Setting Annotations
41
Qualifying Peaks and Groups
43
3000 Micro GC Guide 11
43
Adjusting Retention Time Windows
45
3000 Micro GC Guide 12
45
Conducting a Single Level Calibration
47
3000 Micro GC Guide 13
47
Conducting a Multiple Level Calibration
51
3000 Micro GC Guide 14
51
Calibration with Average Replicates
55
3000 Micro GC Guide 15
55
Customizing a Method Report
59
3000 Micro GC Guide 16
59
Customizing an ESTD Report
63
3000 Micro GC Guide 17
63
Changing a Standard Module
67
3000 Micro GC Guide 18
67
Changing a Performance Enhanced Module
79
3000 Micro GC Guide 19
79
Replacing a Standard Module with a Performance Enhanced Module
87
3000 Micro GC Guide 20
87
Testing Instrument Flow Rates
97
3000 Micro GC Guide 21
97
Installing the Digital I/O Module
99
3000 Micro GC Guide 22
99
Replacing the Battery Cable Fuse on a Portable Instrument
105
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