Oakton 35616-00 Instruction Manual

Ph/mv/rel mv/° c benchtop meters and ph/mv/ion/° c benchtop meters

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pH/mV/Rel mV/° C Benchtop Meters
and
pH/mV/Ion/° C Benchtop Meters
Model numbers:
35616-00
35620-10
35616-03
35620-13
35616-05
35620-15
35616-08
35620-18
35616-01
35620-11
35616-02
35620-12
35616-06
35620-16
35616-07
35620-17
1200 ©2000
70149

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Summary of Contents for Oakton 35616-00

  • Page 1 C Benchtop Meters pH/mV/Ion/° C Benchtop Meters Model numbers: 35616-00 35620-10 35616-03 35620-13 35616-05 35620-15 35616-08 35620-18 35616-01 35620-11 35616-02 35620-12 35616-06 35620-16 35616-07 35620-17 1200 ©2000 70149...
  • Page 3: Table Of Contents

    Table of contents 1. Introduction ....................................4 2. Keypad functions ................................5–8 • Primary keys • Secondary keys • Numeric keys 3. Starting up the meter..............................9–10 • Back panel connections • Turning the meter on and off 4. pH calibration..................................11–12 • 1-point calibration • 2-point calibration (up to 5-point) introduction 5.
  • Page 4: Introduction

    1. Introduction Thank you for selecting the OAKTON ® pH/mV°C meter or OAKTON pH/mV/Ion/°C meter. This manual provides instructions for the 35616- and 35620-series meters. Each section includes illustrations that show you which but- ton to press for each major function.
  • Page 5: Keypad Functions

    2. Keypad functions MEAS The large membrane keypad makes the instrument easy to use. Each button, when pressed, has a corresponding graphic indicator on the display. While in the measurement function, the primary display shows the readings for pH, rel- °C ative mV, mV and Ion Concentration.
  • Page 6 Primary function: Enter numeric values, con- firm calibration points, or confirm and scroll the SETUP MODE HOLD REL MV BASE program options in setup mode. Secondary function: None. SET TEMP MEAS OFFSET RESLN SLOPE Numeric value: None. ACTIVATE CAL EDIT ALARM ON/OFF BEEP...
  • Page 7 SET TEMP/OFFSET Primary function: Press to calibrate ATC temperature probe or to set manual temperature. Enter desired temperature value with numeric keys. Then press YES to confirm the value, or NO to reenter the value. Press CAL/MEAS to exit Set Temp mode. NOTE: This key is active only in the Measurement mode.
  • Page 8 MR/OPTIONS Primary function: Recall stored values, in last-in-first-out sequence. The meter displays recalled values according to the current mode. If there are no stored values in memory, the ERR annunciator appears. To recall all stored values, press MR repeatedly. To exit from MR mode, press CAL/MEAS. In the MR mode, you can also select PRINT to send recalled values to the RS-232 output.
  • Page 9: Starting Up The Meter

    INPUT RS232 3. Starting up the meter Figure 2 above shows the back panel introduction connections of the pH meter. From left to right: • ATC input jack Back panel connections keypad • input for BNC connector functions See Figure 2 above. •...
  • Page 10 Turning on and off the meter SETUP MEAS READY HOLD As soon as you attach your DC power adapter to the meter, the meter will beep. Then, the display will show a diagnostic test of all the readouts for a few °C seconds(Figure 3).
  • Page 11: Ph Calibration

    4. pH calibration This instrument stores up to 5 calibration points to ensure accuracy. You can perform 5-point calibration in any order with standard pH buffers: 1.68, 4.01, 7.00, 10.01, and 12.45. This meter features auto buffer recognition at these 5 values for faster calibration. Or, you can enter your own custom pH buffer introduction values (see step 5 below for instructions).
  • Page 12: Ph Calibration

    7. Press YES to confirm calibration. The CON indicator blinks for one second and disappears (Figure 6). SETUP MODE HOLD REL MV BASE The meter is now calibrated at the buffer indicated in the primary display. SET TEMP MEAS OFFSET RESLN SLOPE ACTIVATE...
  • Page 13: Relative Mv Calibration

    5. Relative mV Calibration MEAS 1. While in the measurement function, press MODE to enter relative mV mode. The primary display indicator shows “Rel mV”. If you have never calibrated mV or if the meter has been reset, the value shown is the same °C as the absolute mV value.
  • Page 14: Ion Calibration

    6. Ion Calibration MEAS READY This calibration is for models with direct concentration mode only. For best accuracy, calibrate your meter to AT LEAST two points with similar concentrations to the solutions you want to test. You can calibrate up to five points. 1.
  • Page 15: Measurement: Ready, Continuous, Hold

    7. Measurement: Ready, Continuous, and Hold functions introduction keypad functions starting up Measuring with READY indicator on. MEAS READY The READY indicator appears on the top left corner of calibration the display when the reading is stable. NOTE: see page 16 for directions on how to activate or deactivate the ready indicator.
  • Page 16 Measuring in the continuous mode SETUP MODE HOLD REL MV While the READY indicator assures stable readings, the BASE continuous mode provides instantaneous readings for SET TEMP MEAS OFFSET SLOPE RESLN faster operation. Continuous mode readings, however, are not as stable. To turn off the READY indicator: ACTIVATE CAL EDIT ALARM...
  • Page 17: Measuring Ph

    8. Measuring pH SETUP MODE HOLD REL MV BASE When you first turn on the instrument, the meter enters directly into pH measurement mode. SET TEMP MEAS OFFSET RESLN SLOPE 1. After calibration, press CAL/MEAS to enter the measurement function. The MEAS indicator shows on ACTIVATE CAL EDIT ALARM...
  • Page 18: Measuring Relative Mv

    10. Measuring relative mV SETUP MODE HOLD REL MV BASE SET TEMP MEAS OFFSET RESLN SLOPE ACTIVATE CAL EDIT ALARM ON/OFF BEEP READY TIMER • ± PRINT SHIFT OPTIONS OPTIONS OPTIONS introduction Measuring relative mV: A. press CAL/MEAS button to enter measurement function (if necessary).
  • Page 19: Measuring Ion Concentration

    11. Measuring Ion Concentration SETUP MODE HOLD REL MV BASE 1. After calibration, press CAL/MEAS to enter the SET TEMP Measurement function. The MEAS indicator shows on MEAS OFFSET RESLN SLOPE the top center of the LCD. ACTIVATE CAL EDIT ALARM ON/OFF BEEP...
  • Page 20: Automatic Temperature Compensation (Atc) And Manual Temperature Compensation

    12. Automatic Temperature Compensation (ATC) MEAS READY and Manual Temperature Compensation Automatic temperature compensation °C Automatic temperature compensation only functions in the pH measurement mode when the temperature probe is plugged into the meter. introduction 1. For automatic temperature compensation (ATC), simply plug in the temperature probe in the phone jack (Figure 12).
  • Page 21: Setup Functions And Setup Keys

    13. Setup function SETUP function The SETUP function lets you view and customize meter parameters. Press the SETUP key to enter SETUP mode. SETUP mode has four main programs: • viewing previous pH calibration data: introduction last time calibrated; SETUP last calibrated buffer points;...
  • Page 22 Setup functions at a glance Press YES to confirm and scroll to each setup function. Press CAL/MEAS to exit at any time. Activation Default Program Function Keys Options Setting Viewing previous pH calibration data P1.0 Last calibration time — Indication only —...
  • Page 23 Program 1: SETUP Viewing previous pH calibration data Program 1 tells you the time and date of your last pH calibration. It also lets you see the calibrated buffer values and the calibration temperature of your last pH calibration. P1.0 Time of last pH calibration. Indication only.
  • Page 24 Program 2: SETUP Selecting meter operations (memory reset; auto-off) Program 2 has two options for customizing: P2.0 Memory reset: The Memory Reset feature is useful if you want to recali- brate to a different electrode and select entirely new SETUP options. Selecting ON resets all stored meter data: previous pH, mV and relative mV memory introduction P 2.0: Memory reset...
  • Page 25 P3.3 Display and set year: SETUP use numeric keys to set year. Press YES to confirm. Meter will continue on to Program 4 on meters with RS-232 option, or return to measurement mode on meters without RS-232. introduction P 3.,3: Display and set year Program 4: Selecting communication data keypad...
  • Page 26: Switching The Ph Resolution

    14. Switching the pH resolution 1. Be sure you are in the pH measurement function (MEAS). 2. Press SHIFT then RESLN. The display will show the last set resolution (Figure 15). 3. Each time you press SHIFT and RESLN, the meter automatically toggles to the opposite setting.
  • Page 27: Setting The Ready Indicator

    15. Setting the Ready indicator The READY indicator shows on the display when a reading stabilizes. Select YES to turn READY indicator on. Select NO during titration or when you need to detect instantaneous pH, mV, or ion concentration changes. 1.
  • Page 28: Setting The Audible Beep

    16. Setting the audible beep If the beep function is set to ON, the instrument will beep every time you press a function key. 1. Be sure you are in the Measurement mode (MEAS). 2. Press SHIFT and then press BEEP. The display will show the last setting (Figure 17).
  • Page 29: Checking Offset

    17. Offset The offset reading shows how much the meter has to compensate electronically for the efficiency of the pH electrode. The offset function shows the pH electrode offset value in mV. The offset is based on the 7.00 pH buffer calibration. If you did not calibrate the 7.00 buffer, the primary display shows a ±20 mV offset from a base of 0.00 mV.
  • Page 30: Setting The High And Low Ph Setpoint Alarm

    19. Setting the high and low setpoint alarm 1. Press MODE to select the Measurement mode for the setpoint, i.e. pH, rel mV, or mV. NOTE: Ion concentration mode does not have high and low alarms. 2. Press ALARM. If high setpoint has not been entered, the display will show “- - - -”...
  • Page 31: Setting And Activating The Timer

    20. Setting and activating the timer The instrument provides an internal timer that counts down from 23 hours 59 minutes, and then gives an audible beep. This function is a timer only and does not activate any other functions. 1. Be sure you are in the measurement function (MEAS).
  • Page 32: Memory Input Functions And Options

    19. Memory input function and options SETUP MODE HOLD REL MV BASE Data is stored in sets: • pH and temperature; SET TEMP MEAS OFFSET SLOPE RESLN • mV and temperature (includes ion concentration measurements) ACTIVATE CAL EDIT ALARM ON/OFF BEEP READY TIMER...
  • Page 33 2nd option: Memory input on time interval. This option allows you to input data into memory at a selected time interval; for example, if you want to maintain a record of reading every hour. 1. To access the second MI option, press SHIFT, then MI/OPT, then YES.
  • Page 34: Memory Recall Functions And Options

    22. Memory recall function and options SETUP MODE HOLD REL MV BASE This function recalls the previous readings stored in the memory. SET TEMP MEAS OFFSET SLOPE RESLN ACTIVATE CAL EDIT ALARM ON/OFF BEEP READY TIMER • ± PRINT SHIFT OPTIONS OPTIONS OPTIONS...
  • Page 35: Setting Up The Optional Printer And Rs-232 Output

    23. Setting up the optional printer and RS-232 output RS-232 provides an output for transmitting displayed readings to a printer or computer. The data is supplied in RS232 ASCII format. ASCII format lets you import data to most popular software programs, and to most printers. Figure 24 introduction Using the meter with a printer...
  • Page 36 Using the meter with a printer to download SETUP MODE HOLD REL MV stored memory BASE SET TEMP MEAS OFFSET Use the first MR key option to download all memory to a RESLN SLOPE printer. ACTIVATE CAL EDIT ALARM ON/OFF BEEP READY TIMER...
  • Page 37 Print function and options SETUP MODE HOLD REL MV BASE 1. Press PRINT to send currently displayed data to printer or computer. The PRINT icon will appear (Figure 25). SET TEMP MEAS OFFSET RESLN SLOPE 2. “Error” symbol blinks if cable is incorrectly attached or setup does not match the PC requirements.
  • Page 38 Introduction measurement The OAKTON DAS is the NEXT GENERATION in easy to use Data Acquisition Software. The features offered are: temperature • Bi-directional communications so you can monitor, control, and operate virtually all the meter functions...
  • Page 39 Use this feature when you want to go to another appli- care and maintenance cation software and still keep the OAKTON DAS ready for use. Single Clicking on the ICON lets you edit the trouble shooting/error name under the ICON. Hold the click on the ICON to messages move the ICON to new positions on the screen.
  • Page 40 Options under “FILE” menu A. Settings: 1. Click on FILE and select SETTINGS (Figure 27). A window labeled COM PORT SETTINGS will appear (Figure 28). This lets you select the RS-232 commu- nications port number (1 or 2), communications baud rate, parity and stop bit.
  • Page 41: Ready/Offset/ Slope

    SETTINGS. Or, reset the meter’s RS 232 parameters to RS-232 match the selections in the COM PORT SETTINGS win- dow. Select RUN under the FILE options and continue. electrode care and If you still have error messages, call your OAKTON maintenance Distributor for advice. trouble shooting/error messages...
  • Page 42 DATA FILE MANAGEMENT The OAKTON DAS software lets you log data directly to your computer or to download readings that have been stored in your meter's memory. Logging data directly to your computer allows faster logging rates and unlimited file sizes—-see“Storing Directly to Computer File”...
  • Page 43 • If you used an existing file name or a new file name, you will see a window that reads, “For continuous logging, set auto shut off option off.” This is a reminder to disable the automatic shutoff feature that shuts meter down after 30 minutes. Use the A-O/Reset button to disable Auto-off.
  • Page 44 Downloading memory from meter To download readings stored in the meter’s memory, click the MEMORY OPTIONS button on the bottom of the computer screen. NOTE: You can store readings to memory either through the MEM IN button located on the meter keypad, or from the MEM IN button located at the bottom of the computer screen.
  • Page 45 B. Memory Release Opt: CLEAR ALL MEMORY This window lets you select ON or OFF to clear all memory and erase the readings stored in the meter’s memory (Figure 35). 1. Select ON or OFF to select whether to clear all mem- ory data from the meter .
  • Page 46 OAKTON DAS FUNCTIONS CAL PARAM Select CAL PARAM at the top of the screen to view a window that shows all the calibration data (Figure 38). NOTE: Although you can view calibration data from the screen, you need to perform calibration functions from your benchtop meter.
  • Page 47 DAS CONTROL BUTTONS The DAS control buttons are located along the bottom of the screen. OFF button: Careful: this causes the DAS to stop running and return to the main screen of the DAS. To return to the DAS run- ning mode, select RUN under the FILE menu.
  • Page 48 ALARM button This button opens a series of two windows that let you select the high and low alarm set points. (Figure 40). The measurement mode that the meter and DAS system are in determines the alarm type shown in the window. For example: the pH measurement mode lets you Figure 40 set pH alarms, the mV measurement mode lets...
  • Page 49 ACTIVATE button Starts the timer countdown. NOTE: If there is no time interval set for the timer, an error message “METER TIMER NOT SET. GO SET TIMER’ is displayed with an OK button. Press the OK button to close the message window. When a time interval is set, you will see a brief message, “please wait meter is enabling the timer”.
  • Page 50 DRIFT/MIN button Opens a window that displays the electrode’s drift per minute. This is a view only window. This window dis- plays the electrode drift in the current measurement mode. For example: if the meter is set for the pH mode Figure 45 electrode drift is displayed in pH/min;...
  • Page 51 The last two buttons in the lower right hand corner are read only displays of the date and time. setup functions EXITING OAKTON DAS resolution/ CLOSE (under FILE options) READY/offset/ slope Select CLOSE in FILE options. The display window and buttons will close.
  • Page 52: Ph Electrode Care And Maintenance

    24. pH Electrode care and maintenance Because your pH electrode is susceptible to dirt and conta- mination, clean it every one to three months depending on the extent and condition of use. NOTE: for Ion Selective Electrode care, consult the instruction manual included with your electrode.
  • Page 53 3 through 6 up to three times for bet- ter response. If the response does not improve, then memory input/recall your electrode is no longer functioning—replace with a new electrode. Call your OAKTON Distributor. printing/ RS-232 electrode care and...
  • Page 54: Error Messages

    25. Error messages LCD display Indicates Cause Solution Memory write Unit too old Turn meter off Err. 1 (on primary error. (> 10 years) and then on. display) or hardware Return if needed. + 2 short beeps. failure. Memory Hardware Turn meter off Err.
  • Page 55: Ph Buffer/Temperature Table

    27. pH buffer/temperature table. Temperature pH buffer values °C °F 4.01 7.00 10.00 4.01 7.12 10.33 4.01 7.09 10.25 4.00 7.06 10.18 4.00 7.04 10.11 introduction 4.00 7.02 10.05 4.01 7.00 10.00 keypad 4.01 6.99 9.95 functions 4.02 6.98 9.92 4.03 6.98 9.88...
  • Page 56: Specifications

    28. Specifications Mode Temperature –1999 to 1999 mV 0 to 9999 Range -2.00 to 15.99 0.0 to 100.0°C (same for rel mV) concentration units 0.1mV up to ±399.9mV ±1 least Resolution 0.01 or 0.1 pH 0.1°C 1mV beyond ±399.9mV significant digit ±0.2mV up to ±399.9mV ±0.5% of Accuracy...
  • Page 57: Accessories

    NOTE: Remember to check the temperature calibration when replacing the ATC probe or functions when using with an OAKTON ® “All-in-One” combined pH and temperature probe. resolution/ See section 12, page 20, “Automatic Temperature Compensation (ATC) and Manual READY/offset/ Temperature Compensation.”...
  • Page 58: Warranty

    31. Return of items keypad functions Authorization must be obtained from your OAKTON Distributor before returning items for any reason. When starting up applying for authorization, please include data regarding the reason the items are to be returned.

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