Thermo Scientific F30400 Installation And Operation Manual
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Thermo Scientific F30400 Installation And Operation Manual

Thermo Scientific F30400 Installation And Operation Manual

Thermolyne furnace large tabletop muffle/ atmosphere controlled ashing
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Thermo Scientific
Thermolyne Furnace
Large Tabletop Muffle/
Atmosphere Controlled Ashing
Model Type: F30400
Installation and Operation Manual
LT1262X1
Revision. J
August, 2022

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  • Page 1 Thermo Scientific Thermolyne Furnace Large Tabletop Muffle/ Atmosphere Controlled Ashing Model Type: F30400 Installation and Operation Manual LT1262X1 Revision. J August, 2022...
  • Page 2 © 2022 Thermo Fisher Scientific Inc. All rights reserved. Thermo Fisher Scientific Inc. provides this document to its customers with a product purchase to use in the product operation. This document is copyright protected and any reproduction of the whole or any part of this document is strictly prohibited, except with the written authorization of Thermo Fisher Scientific Inc.

  • Page 3: Table Of Contents

    Tuning ............25 Thermo Scientific...
  • Page 4 To Replace Door Switch (Microswitch) ......67 Small Benchtop Muffle Thermo Scientific...
  • Page 5 WEEE Compliance ..........84 Thermo Scientific...
  • Page 6 Contents Small Benchtop Muffle Thermo Scientific...

  • Page 7: Safety Information

    Safety Information Contents • “Alert Signals” on page 6 • “Important Information” on page 6 • “Warnings” on page 6 • “Warning” on page 7 Thermo Scientific Large Tabletop Muffle...

  • Page 8: Alert Signals

    Important Information Your Thermo Scientific Thermolyne F30400 Model Furnace has been designed with function, reliability and safety in mind. It is your responsibility to install it in conformance with local electrical codes.

  • Page 9: Warning

    Refer to the appropriate Material Safety Data Sheets (MSDS) for information regarding proper handling and recommended protective equipment. For additional MSDS copies, or additional information concerning the handling of refractory ceramic products, please contact the Customer Service Department at 1-800-438-4851. Thermo Scientific Large Tabletop Muffle...
  • Page 10 Safety Information Warning Large Tabletop Muffle Thermo Scientific...

  • Page 11: Introduction

    Introduction Contents • “Intended Use” on page 10 • “General Usage” on page 10 • “Principles of Operation” on page 11 Thermo Scientific Large Tabletop Muffle...

  • Page 12: Intended Use

    General Usage Do not use this product for anything other than its intended usage. TOTAL NUMBER OF DIGITAL NUMBER OF STORED MODEL NUMBER PROGRAMMABLE COMMUM. PROGRAMS SEGMENTS F30420C-33-80 F30420-33-60-80 F30420C-60-80 F30420C-80 F30428C-60-80 F30428C-80 Large Tabletop Muffle Thermo Scientific...

  • Page 13: Principles Of Operation

    The control is located under the furnace chamber and is well insulated from the heat generated in the furnace chamber. The temperature is controlled by one of three types of controllers. Thermo Scientific Large Tabletop Muffle...
  • Page 14 Introduction Principles of Operation Large Tabletop Muffle Thermo Scientific...

  • Page 15: Chapter 3 General Specification

    Electrical Ratings Watts 5500 5500 Freq. 50/60 50/60 Phase 400°F-1800°F* 400°F-1800°F* Cont. (204°C)-(982°C) (204°C)-(982°C) Temperature Ratings °F (°C) 1800°F-2000°F 1800°F-2000°F Intermittent (982°C)-(1093°C) (982°C)-(1093°C) * The maximum continuous temperature for ashing furnaces (-60 models) is 1787°F (975°C). Thermo Scientific Large Tabletop Muffle...

  • Page 16: Environmental Conditions

    17°C to 27°C; 20% to 80% relative humidity, non-condensing. Installation Category II (overvoltage) in accordance with IEC 664. Pollution degree 2 in accordance with IEC 664. 2,000 meters. Altitude Limit: Storage: -25°C to 65°C; 10% to 85% relative humidity. Voltage 240VAC +/- 10% Tolerance Large Tabletop Muffle Thermo Scientific...

  • Page 17: Unpacking

    3. Open the furnace door and remove the packing material from inside the furnace chamber. 4. Vacuum the chamber prior to use to remove the insulation dust due to shipment. 5. Retain the original packaging material if reshipment is foreseen or required. Thermo Scientific Large Tabletop Muffle...
  • Page 18 Unpacking Large Tabletop Muffle Thermo Scientific...

  • Page 19: Installation

    Installation Contents • “Site Selection” on page 18 • “Electrical Connections” on page 18 • “Electrical Conditions in the EU” on page 18 Thermo Scientific Large Tabletop Muffle...

  • Page 20: Site Selection

    Zmax= 0.0229 ohm at the point of connection, according to EN 61000-3-11 clause 6.2.2. The user has to ensure that the device is operated on a network supply that meets these requirements. If necessary, the system impedance can be confirmed by the energy supplier. Large Tabletop Muffle Thermo Scientific...

  • Page 21: Operation, All Models

    Operation, All Models Contents • “Power Switch” on page 20 • “Cycle Light shown on the display” on page 20 • “Door Safety Switch” on page 20 Thermo Scientific Large Tabletop Muffle...

  • Page 22: Power Switch

    Note an acoustic click of the switch during opening and closing of the door. If this condition is not true, consult the Troubleshooting section before proceeding. This check must be done when the furnace is heating and the cycle light on the display is illuminated. Large Tabletop Muffle Thermo Scientific...

  • Page 23: Chapter 7 Single Setpoint Models W/Otp

    • “Running the Program” on page 28 • “Holding the Program” on page 28 • “Stopping the Program” on page 28 • “Clearing the Flashing End” on page 28 • “Verifying a Running Program” on page 28 Thermo Scientific Large Tabletop Muffle...

  • Page 24: Eurotherm 3216 Controller Operation

    Process Value (PV) Display SetPoint (SP) PAGE Button Display and Scolling Text Messages UP ARROW Button SCROLL Button DOWN ARROW Button If at any time you want to return to the HOME DISPLAY, press PAGE button. Large Tabletop Muffle Thermo Scientific...

  • Page 25: Buttons And Indicators

    SP.RAT: Ramp Rate Setpoint (default units is minutes). RAMPU: Ramp Unit of measure (seconds, minutes and hours). DWELL: Time for dwell or delay (default units is minutes). T.STAT: Timer Status. Active only when timer is active. Thermo Scientific Large Tabletop Muffle...

  • Page 26: Alarms

    In addition to over-temperature protection, units containing a single setpoint controller w/OTP feature a mechanical OTP relay device, which disconnects power from the elements in an alarm condition. Large Tabletop Muffle Thermo Scientific...

  • Page 27: Tuning

    8. Normal control function will resume after the controller calculates tuning parameters. Furnace must be at ambient temperature before starting a tune. “Stat” and “Sp.rr” must be set to OFF or “tunE” will not initiate. Tune has completed when “tunE” stops flashing on display. Thermo Scientific Large Tabletop Muffle...

  • Page 28: Functions

    The instrument remains in standby until the time has elapsed. After the time has elapsed, the instrument controls up to setpoint. These instructions are used with the Single Setpoint models with OTP only (See models listed on front page). Large Tabletop Muffle Thermo Scientific...

  • Page 29: Program Overview

    For example, if it is desired for the controller to stop doing anything at all once the timer is finished, set End.T to OFF. If it is desired to revert back to the ambient temp setpoint at which the program started, set END.T to rES. Thermo Scientific Large Tabletop Muffle...

  • Page 30: Setpoint Rate Limit Setup

    Press the SCROLL button until “T.SAT” is displayed. The display will show “run” if the program is running, “hold” if it is paused or “res” if it is not running. Press the PAGE button to display Actual temperature. Large Tabletop Muffle Thermo Scientific...

  • Page 31: Segment & 5X16 Segment Programmable Models W/Otp

    40 • “Over-Temperature Protection (OTP)” page 40 • “1-Program 8-Segment Controller Operation” page 42 • “Soft Start Timer” page 44 • “Delayed Switch On Timer” page 45 • “5-Program 16-Segment Controller Operation” page 50 Thermo Scientific Large Tabletop Muffle...

  • Page 32: Eurotherm 3216 Controller

    The furnace temperature controller is configured and tuned at the factory to function well for most applications. Occasionally, it may be advisable to configure the temperature controller differently to suit a particular working environment or process. Large Tabletop Muffle Thermo Scientific...

  • Page 33: Operator Interface & Home Display

    Alternative set point in use (SP2) Alarm active (Red) Remote set point or communication active Timer running for 3216c or Program running for 3216p RUN (flashing) Timer hold for 3216c or Program hold for 3216p Thermo Scientific Large Tabletop Muffle...

  • Page 34: Operator Buttons

    A few seconds after the button is released, the controller will accept the new value and is indicated by a brief flash of the display. 3. Press PAGE button to return to the HOME display. Large Tabletop Muffle Thermo Scientific...

  • Page 35: Alternate Set Point Selection (Sp2)

    4. The new ramp rate unit is applied when the button is released and is indicated by a brief flash of the display. 5. Press PAGE button to return to HOME display. Thermo Scientific Large Tabletop Muffle...

  • Page 36: View Or Change The Display Units

    “UNITS” is shown in the lower display. The current unit is shown in the upper display. 2. Press UP or DOWN button to change the display unit. a. (°C): Degrees Celsius b. (°F): Degrees Fahrenheit c. (°K): Kelvin Large Tabletop Muffle Thermo Scientific...

  • Page 37: Auto Tuning

    2. Set the temperature as per requirement; refer to section “Single Set Point Operation” on setting SP1 or SP2. 3. Press SCROLL button to scroll through the list of parameters until A.TUNE is displayed. Thermo Scientific Large Tabletop Muffle...

  • Page 38: Parameter List

    The scrolling text can be interrupted at any time by a single press of any of the buttons, but will not scroll again until the parameter is returned to. Large Tabletop Muffle Thermo Scientific...
  • Page 39 DOWN button to choose LEv2 (Level 2). 5. Press UP or DOWN button to enter the password. The default code is ‘25’. If an incorrect code is entered the display reverts to Level 1. Thermo Scientific Large Tabletop Muffle...

  • Page 40: Offset Procedure

    PV Offset applies a single offset to the temperature or process value over the full display range of the controller and can be adjusted in Level 2. It has the effect of moving the curve up or down about a central point as shown in the example below:- Large Tabletop Muffle Thermo Scientific...

  • Page 41: Alarms & Diagnostics

    • Press PAGE button and SCROLL button together to acknowledge an alarm. If the alarm is still present the ALM beacon lights continuously. The action which takes place depends on the type of alarm configured: Thermo Scientific Large Tabletop Muffle...

  • Page 42: Sensor Break & Loop Break Protection

    To Configure Deviation High Alarm 1. Press SCROLL button until “A1.DHi” appears on the display. 2. Press UP or DOWN button to select the OTP value you desire. We recommend a value of 50. Large Tabletop Muffle Thermo Scientific...
  • Page 43 The set point changes instantaneously from its current value of the measured temperature to a new value at the beginning of a segment. Step can be achieved by turning off Ramp rate. A Step segment has a minimum duration of 1 second. Thermo Scientific Large Tabletop Muffle...

  • Page 44: 1-Program 8-Segment Controller Operation

    • Soft Start timer. Starts automatically on power up. It applies a power limit until the temperature reaches a threshold value or the timer times-out after the dwell period. • 8-Segment programmable controller (4 ramps & 4 soaks). Large Tabletop Muffle Thermo Scientific...
  • Page 45 OFF (0) OFF (0) OFF (0) OFF (0) TIMER.TimerDwell3 Timer Dwell 3 Duration Level 2 Read/Write TIMER.TimerSP4 Timer Target Setpoint 4 Level 2 Read/Write OFF (0) OFF (0) TIMER.TimerRamp4 Timer Ramp Rate 4 Level 2 Read/Write Thermo Scientific Large Tabletop Muffle...

  • Page 46: Soft Start Timer

    SS.SP is exceeded. If the PV is already greater than SS.SP the reduced power limit is not applied and the timer times out. When the timer status = reset, the control output is controlling at a level limited by the output high and low limits. Large Tabletop Muffle Thermo Scientific...

  • Page 47: Delayed Switch On Timer

    • Setting the parameter T.STAT to run; • A command through serial communications; • A logic input suitably configured. When the timer status = run, the control output is off. When the timer status = reset, the control output is controlling. Thermo Scientific Large Tabletop Muffle...
  • Page 48 Each ramp consists of a controlled rate of change of set point to a target level. Each ramp is followed by a dwell at that level. The ramp rate, target level and dwell time are set by the user. Large Tabletop Muffle Thermo Scientific...
  • Page 49 ‘PROG’. 2. To set the resolution, press SCROLL button to select ‘TM.RES’. Press DOWN or UP button to set ‘Hour or ‘min’ (In this example, the ramp rate and dwell period are set in hours). Thermo Scientific Large Tabletop Muffle...
  • Page 50 2:11. (In this example the set point will dwell at 45 for 2 hours 11 minutes). 8. Now repeat the above three steps (5, 6 & 7) to set remaining all segments. Large Tabletop Muffle Thermo Scientific...
  • Page 51 SP2 is achieved. It is more usual to use a DWELL (default) or RESET end type. • The program will start from the measured temperature. On recovery from power failure, the program will automatically run at the last ramp rate from the current measured temperature. Thermo Scientific Large Tabletop Muffle...

  • Page 52: 5-Program 16-Segment Controller Operation

    A program is stored as a series of segments and can be run once. This 16 segment digital model can enable 16 segments in each program. Some of the commonly used parameters in operator Level 1 and Level 2 of 3216p controller are: Large Tabletop Muffle Thermo Scientific...
  • Page 53 Level 2 Read/Write OFF (0) OFF (0) PROGRAMMER.Dwell4 Program Dwell 4 Duration Level 2 Read/Write PROGRAMMER.SP5 Program Target Setpoint 5 Level 2 Read/Write PROGRAMMER.Ramp5 Program Ramp Rate 5 Level 2 Read/Write OFF (0) OFF (0) Thermo Scientific Large Tabletop Muffle...
  • Page 54 Each program can have its own Holdback value assigned to it. H.BACK can be accessed from Level 1 or Level 2. To set the holdback value: Large Tabletop Muffle Thermo Scientific...
  • Page 55 2. The setpoint 2 may be a lower or a higher temperature). rES : Reset on completion and reverts to SP1 or SP2, based on the Setpoint selection. Scroll through parameters in Level 2 and set the required ‘END.T’ by pressing Thermo Scientific Large Tabletop Muffle...
  • Page 56 7. To set the first Ramp rate, press SCROLL button to select ‘RMP.1’. Press DOWN button to set the value. 8. To set the first Dwell, press SCROLL button to select ‘DWEL.1’. Press DOWN or UP button to set the value. Large Tabletop Muffle Thermo Scientific...
  • Page 57 Press and hold ‘PROGRAM END’ will be displayed at for more than 1 second the end of the program Programs can also be operated from the ‘P.STAT’ parameter found in the level 1 parameter list. Thermo Scientific Large Tabletop Muffle...
  • Page 58 • END TYPE - when the end type is SP2, Timer END does not occur until the ramp is complete or SP2 is achieved. It is more usual to use a DWELL (default) or RESET end type. Large Tabletop Muffle Thermo Scientific...

  • Page 59: Communication Option

    NOTE Please ensure the adapter is compatible with the operating system of your PC/Laptop. Some adapter needs driver softwares & port access privileges on your PC/Laptop for proper functioning. Please contact your local IT for assistance. Thermo Scientific Large Tabletop Muffle...

  • Page 60: Rs 485 Pinout & Connections

    Verify DB-9 pin connections as shown in wiring diagram, interchange 2 & 3 connections if communication is not working. d. Verify the configuration values in the controller, listed in the Table 4, “Controller Parameters for Communication”. Large Tabletop Muffle Thermo Scientific...

  • Page 61: Chapter 10 Installation And Operation Of Air Control

    This exhaust system must be capable of handling smoke and gases produced in an ashing procedure. Coal ashing furnaces -60 models contain a feature to provide air (or inert gas) flow within the furnace chamber. Thermo Scientific Large Tabletop Muffle...
  • Page 62 Failure to connect the exhaust port to an appropriate exhaust system will result in smoke and gases filling the work area. Without the connection, gases and smoke will escape around the door seal and at the rear of the furnace. Large Tabletop Muffle Thermo Scientific...

  • Page 63: Chapter 11 Furnace Loading

    • If you are heating a number of small parts, spread them throughout the center of the furnace chamber. • Keep objects away from thermocouple. • Use insulated tongs and mittens when loading and unloading furnace. • Always wear safety glasses. Thermo Scientific Large Tabletop Muffle...
  • Page 64 Furnace Loading Large Tabletop Muffle Thermo Scientific...

  • Page 65: Chapter 12 Preventive Maintenance

    (500°F). We highly recommend that you replace the thermocouple periodically (once every six months) to ensure temperature accuracy. General Cleaning Instructions Wipe exterior surfaces with lightly dampened cloth containing mild soap solution. The Troubleshooting section is intended to aid in defining and correcting possible service problems. Thermo Scientific Large Tabletop Muffle...
  • Page 66 Preventive Maintenance General Cleaning Instructions Large Tabletop Muffle Thermo Scientific...

  • Page 67: Chapter 13 Maintenance And Servicing

    • “To Replace a Platinel II Thermocouple” on page 66 • “To Replace Solid State Relay:” on page 67 • “To Replace Door Switch (Microswitch)” on page 67 • “To Realign Door Strike” on page 68 • “To Replace Control Module” on page 68 Thermo Scientific Large Tabletop Muffle...

  • Page 68: To Replace A Heating Element

    1. Disconnect furnace from power supply. 2. Remove the back terminal cover of the furnace. (Note placement and connection of T/C lead wires). 3. Remove the screws on the thermocouple terminals and pull the thermocouple straight out. Large Tabletop Muffle Thermo Scientific...

  • Page 69: To Replace Solid State Relay

    8. Remove the two screws and nuts from the Microswitch. 9. Insert new Microswitch and secure with screws and nuts removed in Step 8. 10. Slide control section back and replace the wires on the door switch. Thermo Scientific Large Tabletop Muffle...

  • Page 70: To Realign Door Strike

    To Replace Control Module Gently pry the retaining tabs on both sides out, and then pull the control straight out of the sleeves. Install the new controller to the sleeve. Large Tabletop Muffle Thermo Scientific...

  • Page 71: Chapter 14 Troubleshooting

    Lighten load in chamber to allow heat to circulate. Slow heatup. Wrong heating element. Install proper element. One or more heating elements are burned out. Replace burned out elements. Wired improperly. Check wiring diagram for correct wiring of your furnace. Thermo Scientific Large Tabletop Muffle...
  • Page 72 If you find the breaker tripped first try to reset it by pressing the button in. If the breaker is not tripped and will not reset it should be replaced. Ensure both breakers are reset. Large Tabletop Muffle Thermo Scientific...

  • Page 73: Chapter 15 Replacement Parts List

    All models RYX62 Mechanical relay All models SWX103 Circuit breaker All models SWX143 Power switch All models SWX163 Door switch All models TC412X1A Thermocouple All models TRX96 Terminal block All models TRX178 Terminal block All models Thermo Scientific Large Tabletop Muffle...

  • Page 74: Segment Programmable Models With Otp

    All models RYX37 S.S. relay All models RYX62 Mechanical relay All models SWX143 Power switch All models SWX163 Door switch All models TC412X1A Thermocouple All models TRX96 Terminal block All models TRX178 Terminal block All models Large Tabletop Muffle Thermo Scientific...

  • Page 75: 5X16 Segment Programmable Models With Otp

    All models RYX37 S.S. relay All models RYX62 Mechanical relay All models SWX143 Power switch All models SWX163 Door switch All models TC412X1A Thermocouple All models TRX96 Terminal block All models TRX178 Terminal block All models Thermo Scientific Large Tabletop Muffle...
  • Page 76 Replacement Parts List 5X16 Segment Programmable Models with OTP Large Tabletop Muffle Thermo Scientific...

  • Page 77: Chapter 16 Ordering Procedures

    All parts listed herein may be ordered from the Thermo Scientific dealer from whom you purchased this unit or can be obtained promptly from the factory. When service or replacement parts are needed we ask that you check first with your dealer.
  • Page 78 Ordering Procedures Large Tabletop Muffle Thermo Scientific...

  • Page 79: Chapter 17 Wiring Diagrams

    Wiring Diagrams Contents • “Single setpoint control” on page 78 • “Segment programmable control” on page 79 • “5X16 segment programmable control” on page 80 Thermo Scientific Large Tabletop Muffle...

  • Page 80: Single Setpoint Control

    Wiring Diagrams Single setpoint control Single setpoint control Large Tabletop Muffle Thermo Scientific...

  • Page 81: Segment Programmable Control

    Wiring Diagrams Segment programmable control Segment programmable control Thermo Scientific Large Tabletop Muffle...

  • Page 82: 5X16 Segment Programmable Control

    Wiring Diagrams 5X16 segment programmable control 5X16 segment programmable control Large Tabletop Muffle Thermo Scientific...

  • Page 83: Chapter 18 Regulatory Compliance

    Canadian ISED IC Notice This ISM digital apparatus complies with Canadian ICES-001. Cet appareil ISM est conforme á la norme NMB-001 du Canada Thermo Scientific Small Benchtop Muffle...

  • Page 84: Additional Regulations & Markings

    • Polybrominated biphenyls (PBB) (0.1 %) • Polybrominated diphenyl ethers (PBDE) (0.1 %) 2015/863 Annex II (RoHS3, In effect after July 22, 2019) • Bis(2-ethylhexyl) phthalate (DEHP) (0.1 %) • Butyl benzyl phthalate (BBP) (0.1 %) Small Benchtop Muffle Thermo Scientific...
  • Page 85 Our compliance is witnessed by written declaration from our suppliers and/or component testing. This confirms that any potential trace contamination levels of the substances listed above are below the maximum level set by the latest regulations or are exempt due to their application. Thermo Scientific Small Benchtop Muffle...

  • Page 86: Weee Compliance

    Ulteriori informazioni sulla conformità di Thermo Fisher Scientific con queste Direttive, l’elenco delle ditte di riciclaggio nel Vostro paese e informazioni sui prodotti Thermo Scientific che possono essere utili alla rilevazione di sostanze soggette alla Direttiva RoHS sono disponibili sul sito www.thermofisher.com/WEEERoHS.
  • Page 87 Important For your future reference and when contacting the factory, please have the following information readily available: Model Number: Serial Number: Date Purchased: The above information can be found on the dataplate attached to the equipment. If available, please provide the date purchased, the source of purchase (manufacturer or specific agent/rep organization), and purchase order number.
  • Page 88 Thermo Fisher Scientific Inc. 275 Aiken Road Asheville, NC 28804 United States www.thermofisher.com LT1262X1 Rev. J Contact Us North America: 866-984-3766 Europe: France +33 2 2803 2180 Germany +49 9184 90 9640 UK/Ireland + 44 870 609 9203 Asia: China +86 21 6865 4588 India 1800 22 8374 Japan +81 45 453 9220...

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