vacuubrand ME 16C NT-ME 16C NT+EK Instructions For Use Manual

vacuubrand ME 16C NT-ME 16C NT+EK Instructions For Use Manual

Chemistry diaphragm pumps, chemistry vacuum systems

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Technology for Vacuum Systems
Instructions for use
ME 16C NT - ME 16C NT + EK
MD 12C NT - MD 12C NT + EK
MD 12C NT + AK + EK
MV 10C NT - MV 10C NT + EK
Chemistry diaphragm pumps
Chemistry vacuum systems
Original instructions EN

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Summary of Contents for vacuubrand ME 16C NT-ME 16C NT+EK

  • Page 1 page 1 of 88 Technology for Vacuum Systems Instructions for use ME 16C NT - ME 16C NT + EK MD 12C NT - MD 12C NT + EK MD 12C NT + AK + EK MV 10C NT - MV 10C NT + EK Chemistry diaphragm pumps Chemistry vacuum systems Original instructions EN...
  • Page 2 ® (US-Reg.No 3,833,788), VACUUBRAND (US-Reg.No 3,733,388), ® VACUU·VIEW , GREEN VAC (US-Reg.No. 4,924,553), VACUU·PURE ® ® ® (US-Reg No. 5,559,614) and also the shown company logos are registered trademarks of VACUUBRAND GMBH + CO KG in Germany and/or other countries.
  • Page 3 page 3 of 88 Achtung: Die vorliegende Betriebsanleitung ist nicht in allen EU-Sprachen verfügbar. Der Anwen- der darf die beschriebenen Geräte nur dann in Betrieb nehmen, wenn er die vorliegende Anleitung versteht oder eine fachlich korrekte Übersetzung der vollständigen Anleitung vorliegen hat. Die Betriebsanleitung muss vor Inbetriebnahme der Geräte vollständig gelesen und verstanden wer- den, und alle geforderten Maßnahmen müssen eingehalten werden.
  • Page 4 page 4 of 88 Tähelepanu! Käesolev kasutusjuhend ei ole kõigis EL keeltes saadaval. Kasutaja ei tohi seadet käsitseda, kui ta ei saa kasutusjuhendist aru. Sel juhul peab saadaval olema kogu kasutusjuhen- di tehniliselt korrektne tõlge. Enne seadme kasutamist tuleb kogu juhend läbi lugeda, see peab olema arusaadav ning kõik nõutud meetmed peavad olema rakendatud.
  • Page 5 page 5 of 88 注意:この取扱説明書はすべての言語で利用可能ではありません。 もしこの取扱説明書を理解 できないならば、ユーザーは装置を操作してはなりません。 この場合、技術的に正しい翻訳が なされた完全なマニュアルを用意しなければなりません。 装置を作動する前にマニュアルを完 全に読み、そして理解されなくてはなりません。そして、すべての要求される対策を講じなけ ればなりません。 真空装置を安全に取り扱うために 주의 : 이 매뉴얼은 모든 언어로 번역되지는 않습니다. 만약 이 매뉴얼의 내용을 충분히 인지하지 못했다면 기기를 작동하지 마십시오. 매뉴얼의 내용을 기술적으로 정확하게 번역한 경우에 이용 하십시오. 기기를 사용하기 전에 이 매뉴얼을 충분히 읽고 이해하고 모든 요구되는 사항들을 적용 해야...
  • Page 6 page 6 of 88 Atentie: Acest manual nu este disponibil in toate limbile EU. Utilizatorul nu trebuie sa lucreze cu aparatul daca daca nu intelege manualul. Astfel, va fi disponibile o traducere corecta si completa a manualului. Manualul trebuie citit si inteles in intregime inainte de a lucra cu aparatul si a luat toate masurile care se impun.
  • Page 7: Table Of Contents

    page 7 of 88 Contents Safety information! ............. 9 Important information! ................. 9 General information ................11 Intended use..................11 Setting up and installing the equipment ..........12 Ambient conditions ................14 Operating conditions ................. 15 Safety during operation ..............17 Maintenance and repair..............19 Important information: Equipment marking (ATEX) ....
  • Page 8 page 8 of 88 Assembling the pump housing ............71 Replacing the overpressure safety relief device ......78 Repair - Maintenance - Return - Calibration ....81 Warranty ................82 Health and safety clearance form ........83 EC Declaration of Conformity of the Machinery ....84 China RoHS ...............
  • Page 9: Safety Information

    Make operating personnel aware of dangers arising from the pump and the pumped substances. VACUUBRAND disclaims any liability for inappropri- ate use of these pumps and for damage from failure to follow instructions contained in this manual.
  • Page 10 page 10 of 88 ➨ DANGER indicates a hazardous situation which, if not avoided, will result in death or serious injury. + WARNING indicates a hazardous situation which, if not avoided, could result in death or serious injury. • CAUTION indicates a hazardous situation which, if not avoided, could result in minor or moderate injury.
  • Page 11: General Information

    page 11 of 88 General information Remove all packing material from the packing box. Re- NOTICE move the product from its packing-box and retain all pack- aging until the equipment is inspected and tested. Re- move the protective caps from the inlet and outlet ports and retain for future use.
  • Page 12: Setting Up And Installing The Equipment

    page 12 of 88 + The pumps are designed for ambient temperatures during operation between +50°F and +104°F (+10°C and +40°C). Periodically check maximum tempera- tures if installing the pump in a cabinet or a housing. Make sure ventilation is adequate to maintain recom- mended operating temperature.
  • Page 13 page 13 of 88 patibility with system components (e.g., exhaust pipe- line or exhaust valve) at the outlet. + Do not permit any uncontrolled pressurizing. Make sure that the exhaust tubing cannot become blocked to avoid a risk of bursting! + Keep the electrical power cord away from heated sur- faces.
  • Page 14: Ambient Conditions

    page 14 of 88 2 in (5 cm) between the cooling fan and surrounding items (e.g., housing, walls, etc.), or else install an external au- tomatic ventilation system. Do not place the pump on soft surfaces (e.g., rubber foam) during operation. This may reduce the air circulation in the pump housing and affect the fan’s cooling effect.
  • Page 15: Operating Conditions

    page 15 of 88 • This product may only be used indoors in a non-explo- sive atmosphere, and in a dry environment. Adopt suitable measures in case of differences from recommended conditions, e.g., installation in higher altitudes (risk of insufficient cooling), conductive pollu- tion or external condensation on the pump.
  • Page 16 page 16 of 88 Do not pump: - unstable substances - substances which react explosively under impact (mechanical stress) without air - substances which react explosively when being ex- posed to elevated temperatures without air, - substances subject to auto-ignition, - substances which are inflammable without air - explosive substances.
  • Page 17: Safety During Operation

    page 17 of 88 Safety during operation ➨ Adopt suitable measures to prevent the release of dan- gerous, toxic, explosive, corrosive, noxious or pollut- ing fluids, vapors and gases. To prevent any emission of such substances from the pump outlet, install an appropriate collecting and disposal system and take protective action for pump and environment.
  • Page 18 page 18 of 88 (chemicals, thermal decomposition products of fluoro- elastomers). Use appropriate protective clothing and safety goggles. + Interruption of the pump (e.g., due to power failure), failure of connected components or of parts of the sup- ply, or change in parameters must not be allowed to lead to dangerous conditions.
  • Page 19: Maintenance And Repair

    page 19 of 88 the exhaust waste vapor condenser in particular might be elevated in case of permanent high gas flow. The temperatures that are produced during operation may cause burns. Avoid direct contact with the surface. Provide a suitable contact guard if necessary. •...
  • Page 20 For details and for the online ”Instructions for repair” man- ual see www.vacuubrand.com. In normal use, the lifetime of the diaphragms and valves is typically 15,000 operating hours. Bearings have a typi- cal durability of 40000 h.
  • Page 21 page 21 of 88 + Vent the pump before starting maintenance. Isolate the pump and other components from the vacuum system. Allow sufficient cooling of the pump. Drain condensate, if applicable. Clean polluted surface with a clean, slightly moistened cloth. NOTICE To moisten the cloth we recommend water or mild soap.
  • Page 22: Important Information: Equipment Marking (Atex)

    Important information: Equipment marking (ATEX) Only valid for products with ATEX marking. If the ATEX marking is shown on the rating plate of the respective product, VACUUBRAND GMBH + CO KG assures, that the device complies with the provi- sions of the directive 2014/34/EU. The applied harmonized stand- ards are indicated in the EC Declaration of Conformity of the Ma- chinery (see instructions for use).
  • Page 23 page 23 of 88 • The equipment is designated for a low degree of mechanical stress and has to be installed in a way so that it cannot be damaged from outside. Pumping units have to be installed so that they are protected against shocks from the outside and against glass splinters in the event of breakage (implosion).
  • Page 24: Technical Data

    page 24 of 88 Technical data General technical data valid for all pumps II 3/- G Ex h IIC T3 Gc X ATEX approval if the ATEX marking Internal Atm. only is shown on the rating plate Inner part (pumped gases) Tech.File: VAC-EX02 Maximum permissible inlet pressure (absolute)
  • Page 25: General Technical Data Valid For All Pumps

    page 25 of 88 General technical data valid for all pumps Outlet hose nozzle for tubing I.D. 5/8” (hose nozzle DN 15 mm) + EK hose nozzle for tubing I.D. 3/8” (hose nozzle DN 10 mm) hose nozzle for tubing Coolant connection I.D.
  • Page 26 page 26 of 88 MD 12C NT Type MD 12C NT + EK MD 12C NT + AK + EK Maximum pumping speed* (ISO 21360) (12.0) Ultimate vacuum (absolute) Torr without gas ballast (mbar) Ultimate vacuum (absolute) Torr with gas ballast (mbar) A-weighted emission sound pressure dB(A)
  • Page 27: Gas Inlet Temperatures

    page 27 of 88 Gas inlet temperatures Permitted range of gas Operating condition Inlet pressure temperatures at inlet > 75 Torr (100 mbar) ➨ 50 °F to 104 °F Continuous operation (high gas load) (+10°C to +40°C) < 75 Torr (100 mbar) ➨...
  • Page 28: Abbreviations

    page 28 of 88 Abbreviations ECTFE: Ethylene/Chlorotrifluoroethylene ETFE: Ethylene/Tetrafluoroethylene FEP: Perfluoroethylene perfluoropropylene copolymer FFKM: Perfluoro elastomer FPM: Fluoroelastomer Polyethylene PET: Polyethylene terephthalate Polypropylene PTFE: Polytetrafluoroethylene separator for condensates, catchpot at inlet or outlet exhaust vapor condenser Pump parts Position Component Inlet Outlet ON/OFF switch...
  • Page 29 page 29 of 88 ME 16C NT, MD 12C NT, MV 10C NT...
  • Page 30 page 30 of 88 ME 16C NT + EK, MD 12C NT + EK, MV 10C NT + EK MD 12C NT + AK + EK...
  • Page 31: Use And Operation

    page 31 of 88 Use and operation Installation Remove the product from its packing-box. Read the document ”Safety information for Safety information for vacuum equipment vacuum equipment” and observe the in- structions contained therein! Sicherheitshinweise für Vakuumgeräte Safety information for vacuum equipment Avis de sécurité...
  • Page 32: Vacuum Connection (Inlet)

    page 32 of 88 Vacuum connection (inlet) Inlet: Small flange connection KF DN 25 with clamping ring and centring ring. Connect the vacuum line (e.g., metal hose (stainless steel) KF DN 25) at the inlet of the pump. • Reduce the transmission of vibration. Pre- vent mechanical load due to rigid pipelines.
  • Page 33: Separator (Ak) At The Inlet

    page 33 of 88 Use a suitable valve (see “Accessories / Spare parts”, pg. 43) to isolate the pump from the vacuum application. This is to allow the pump to warm up before pumping condensable va- pors and to clean the pump after use before it is switched off.
  • Page 34: Connecting The Outlet

    page 34 of 88 Connecting the outlet Outlet via hose nozzle DN 15 mm or via hose outlet nozzle DN 10 mm (exhaust waste vapor con- denser EK). In case, install a small flange connection in- stead (thread G1/2”, see “Accessories / Spare parts”, pg.
  • Page 35: Exhaust Waste Vapor Condenser (Ek) At The Outlet

    page 35 of 88 ✘ ✘ Always install outlet tubing descending from the pump or provide other measures to avoid backflow of condensate towards the pump. ✔ ✔ Exhaust waste vapor condenser (EK) at the outlet The exhaust waste vapor condenser enables an effi- cient condensation of the pumped vapors at the outlet.
  • Page 36 page 36 of 88 Check all hose connections prior to starting operation of the cooling system. Secure coolant hoses at the hose nozzles (e.g., with hose clamps) to prevent their acci- dentally slipping off. ➨ Prevent the discharge of dangerous gases and vapors to the surrounding atmosphere.
  • Page 37: Electrical Connection

    page 37 of 88 Permissible range of coolant temperature at the exhaust NOTICE waste vapor condenser: 5°F to 68°F (-15°C to +20°C) Check hose connections prior to starting operation of the cooling system. Check coolant hoses regularly during operation. Electrical connection Plug in the power cord.
  • Page 38 page 38 of 88 • If the pump is installed at an altitude of more max. 6500 ft than 6500 ft (2000 m) above mean sea lev- (2000 m) el, check compatibility with applicable safety requirements, and adopt suitable measures. There is a risk of the motor overheating due to insufficient cooling.
  • Page 39 page 39 of 88 A temperature sensor in the winding protects I ➨ O the pump motor. In case of excess tempera- ture or if the motor is blocked, the motor is shut down. °C / °F If the vacuum pump is switched off due to this safety precaution, the error must be cleared manually: Unplug pump from the power supply ...
  • Page 40: Important Notes Regarding The Use Of Gas Ballast

    page 40 of 88 Important notes regarding the use of gas ballast Gas ballast is a continuous purge to keep the pump’s in- terior as clean as possible and to reduce the possibility of condensation inside the pump. ➨ Air and pumped media might react inside the pump or at the outlet of the pump and form hazardous or explo- sive mixtures, when you use air rather than inert gas for the gas ballast.
  • Page 41: In Case Of Condensation

    ✔ in time to avoid overflow. Install a level sensor (see “Accessories / Spare parts”, pg. 43) for monitoring, if necessary (VACUUBRAND con- troller CVC 3000 or VNC 2 is required). The maximum liquid level is at approximately 80% of the total filling level to avoid problems when removing the catchpots.
  • Page 42: Shutdown & Storage

    page 42 of 88 Drain catchpots. + Important: Comply with regulations when disposing of solvents/condensates. Recy- cle if possible; purify if contaminated. NOTICE Reattach drained catchpots. Shutdown & storage The pump can be switched off under vacuum. Short-term: Condensate? - Has the pump been exposed to conden- sate? O ➨...
  • Page 43: Accessories / Spare Parts

    page 43 of 88 Accessories / Spare parts Exhaust waste vapor condenser with catchpot 0.52 qt (500 ml) ....20699948 (Upgrade kit including holder and front cover) Separator (inlet) ........20699979 small flange KF DN 25 (adapter to hose nozzle DN 15 mm at inlet included) Vacuum gauge DVR 2pro ......20682906 Vacuum gauge DCP 3000 with gauge head VSK 3000 ......20683170...
  • Page 44 Vacuum hose (caoutchouc) 15 mm ID (sold by meter) ......20686003 Adapter for gas ballast connection via small flange KF DN 16 ....20636193 Level sensor for catchpots.................20699908 (VACUUBRAND controller CVC 3000 or VNC 2 is required). At the inlet: Metal hose (stainless steel) KF DN 25 (1000mm) ........20673337 PTFE hose KF DN 25 (1000mm) ..............20686033...
  • Page 45: Troubleshooting

    page 45 of 88 Set of seals for MD 12C NT, MV 10C NT (diaphragms, valves and O-rings) ............20696839 Overpressures safety relief device at exhaust waste vapor condenser ..............20638821 Centring ring KF DN 25, FEP coated ............20635722 Diaphragm key (w/f 66) ................20636554 Troubleshooting Fault Possible cause...
  • Page 46: Replacing The Device Fuse

    page 46 of 88 Fault Possible cause Remedy ❑ Pump too noisy. ➨ Atmospheric or high ✔ Connect hose or silencer pressure at the pump to pump outlet. Be careful inlet? not to cause outlet over- pressure, especially with condensable vapors. ➨...
  • Page 47: Replacing Diaphragms And Valves

    page 47 of 88 Replacing diaphragms and valves + Please read section ”Replacing diaphragms and valves” com- pletely before starting maintenance. The pictures may show other versions of pumps. This does not change the method of replacing diaphragms and valves. ➨...
  • Page 48 page 48 of 88 + Allow sufficient cooling of the pump before starting maintenance. °C / °F + Vent the pump and isolate it from the vacuum system before you start mainte- nance. Ensure that maintenance is done only by suitably NOTICE trained and supervised technicians.
  • Page 49: Disassembling The Pump Housing

    page 49 of 88 Disassembling the pump housing...
  • Page 50 page 50 of 88 2.5 mm 2.5 mm...
  • Page 51 page 51 of 88 without ”EK”:...
  • Page 52 page 52 of 88 + Don’t loosen this screw!
  • Page 53 page 53 of 88...
  • Page 54 page 54 of 88 2.5 mm...
  • Page 55: Checking Diaphragms And Valves

    page 55 of 88 Checking diaphragms and valves Position Component Position Component Clamping bracket Diaphragm support disc Disc spring Washers Valve head Connecting rod O-rings Housing Valves Distributor Head cover Hose clip Diaphragm clamping disc PTFE tube with square head screw Diaphragm...
  • Page 56: Replacing The Diaphragms

    page 56 of 88 Replacing the diaphragms + Clean. 20696867 / 20696839...
  • Page 57 page 57 of 88 + Pay attention to number of washers!
  • Page 58 page 58 of 88...
  • Page 59 page 59 of 88 + Pay attention to number of washers! + 4.4 ft.lbf (6 Nm) It is recommended to use a torque wrench. Attach torque wrench to diaphragm key (hexagonal bolt 6 mm wide).
  • Page 60: Replacing The Valves

    page 60 of 88 + Screw in diagonally at first slightly, then tighten. + 8.9 ft.lbf (12 Nm) Replacing the valves...
  • Page 61 page 61 of 88 + Clean. 20696867 / 20696839...
  • Page 62 page 62 of 88...
  • Page 63 page 63 of 88 + 2.2 ft.lbf (3 Nm)
  • Page 64 page 64 of 88 + Maintain all pump heads in the same way. MD 12C NT...
  • Page 65 page 65 of 88 ME 16C NT MV 10C NT ME 16C NT MD 12C NT MV 10C NT...
  • Page 66: Replacing The Valve At The Distributor

    page 66 of 88 Replacing the valve at the distributor (only MD 12C NT / MV 10C NT) 2.5 mm without ”EK”: 2.5 mm without ”EK”: size 2...
  • Page 67 page 67 of 88 size 2 Version A (valve: Ø 24,4 mm):...
  • Page 68 page 68 of 88 20696839 Ø 24,4 mm Ø 26 mm Version B (valve: Ø 37 mm): 20696839 Ø 37 mm Ø 40 mm...
  • Page 69 page 69 of 88 size 2 without ”EK”: size 2...
  • Page 70 page 70 of 88 + Do not operate the pump without pump housing! Danger due to freely rotating fan! Risk of overheating due to missing cooling air guide.
  • Page 71: Assembling The Pump Housing

    page 71 of 88 Assembling the pump housing + 8.9 ft.lbf (12 Nm)
  • Page 72 page 72 of 88 + 8.9 ft.lbf (12 Nm)
  • Page 73 page 73 of 88 + 3.7 ft.lbf (5 Nm) + 3.7 ft.lbf (5 Nm)
  • Page 74 page 74 of 88 + 3.7 ft.lbf (5 Nm)
  • Page 75 page 75 of 88 + 3.7 ft.lbf (5 Nm)
  • Page 76 page 76 of 88...
  • Page 77 page 77 of 88 Checking the ultimate vacuum ➨ A fter any intervention at the equipment (e.g., repair / maintenance) the ultimate vacuum of the pump has to be checked. Only if the pump achieves its specified ultimate vacuum, the pump’s leak rate is low enough to ensure that no explosive atmospheres will occur in the inte- rior of the equipment.
  • Page 78: Replacing The Overpressure Safety Relief Device

    page 78 of 88 Replacing the overpressure safety relief device at the exhaust waste vapor condenser size 1...
  • Page 79 page 79 of 88 20638821 20638821...
  • Page 80 page 80 of 88 size 1...
  • Page 81: Repair - Maintenance - Return - Calibration

    3 or 4. These devices cannot be checked, maintained or repaired. Also decontaminat- ed devices must not returned to VACUUBRAND due to a residual risk. The same conditions apply to on-site work.
  • Page 82: Warranty

    Warranty VACUUBRAND shall be liable for insuring that this product, including any agreed installation, has been free of defects at the time of the transfer of risk. VACUUBRAND shall not be liable for the consequences of improper han-...
  • Page 83 page 83 of 88 Declarations and certificates...
  • Page 84: Ec Declaration Of Conformity Of The Machinery

    page 84 of 88...
  • Page 85 85 of 88 DECLARATION OF CONFORMITY – China RoHS 2 VACUUBRAND GMBH + CO KG has made reasonable efforts to ensure that hazardous materials and substances may not be used in its products. In order to determine the concentration of hazardous substances in all homogeneous materials of the subassemblies, a “Product Conformity Assessment”...
  • Page 86: China Rohs

    (Pb), mercury (Hg), cadmium (Cd), hexavalent chromium (Cr+VI), polybrominated biphenyls (PBB), and polybrominated diphenyl ethers (PBDE). Products manufactured by VACUUBRAND may enter into further devices (e.g., rotary evaporator) or can be used together with other appliances (e.g., usage as booster pumps).
  • Page 87 page 87 of 88...
  • Page 88 Seitenzahl Technology for Vacuum Systems VACUUBRAND > Support > Manuals Manufacturer: VACUUBRAND GMBH + CO KG VACUUBRAND GMBH + CO KG Alfred-Zippe-Str. 4 Alfred-Zippe-Str. 4 97877 Wertheim 97877 Wertheim GERMANY GERMANY Phone: Head office +49 9342 808-0 Sales +49 9342 808-5550...

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