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CEM Discover SP-D 10/35 Cleaning And Maintenance Tips

CEM Discover SP-D 10/35 Cleaning And Maintenance Tips

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Cleaning and Maintenance Tips for
Discover® SP-D 10/35 and 80
Discover SP-D Cleaning with Tap Water – to be done DAILY
Note: Complete procedure each day after running samples. The sample will vent 4 to 6 times
and lose 2 to 3 mL of water
1. Create the following method using the document, CEM Synergy–D Software Operating
Procedures in the section "Create New Methods."
Microwave Power Application: Ramp to Temperature
Pressure Stages: Custom,
Stage 1: PressureSP = 125 PSI, Times at SP = 4,
Stage 2: PressureSP = 250 PSI, Times at SP = 10,
Remove Stages 3 – 5.
Vessel: 80 mL Quartz or 35 mL or 10 mL Pyrex without Liner
Stage
1
2. Add tap water to vessel
10 mL to the 35 mL and 80 mL vessel, OR
3 mL and 15 – 20 grains of NaCl to the 10 mL vessel
3. Add stir bar and cap
4. Place in Explorer rack or Discover SP–D
5. Add sample to queue using the document,
Procedures
in the section "Set-up and Start a Sample Queue with the Explorer" OR
"Set-up and Start a Sample Queue without the Explorer"
6. Press Play
ActiVent cleaning – to be done WEEKLY
1. Press the HOME key to display the "Discover Home" screen.
2. Press the "+/-" keys to highlight "System Setup".
3. Press the ENTER key.
4. Press the right ARROW key 3 times to display the "Setup 4" screen.
5. Press the "+/-" keys to highlight "APM Cleaning".
6. Press the ENTER key. A new screen will appear:
7. Remove the attenuator (microwave door) from the cavity.
8. Press the ENTER key. A new screen will appear:
www.cem.com
Temp
Ramp
Hold
Time
Time
200
4:00
2:00
info@cem.com
Pressure Power
Stirring
400
300
Med
CEM Synergy–D Software Operating
704-821-7015
Sept 2014
800-726-3331

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Summary of Contents for CEM Discover SP-D 10/35

  • Page 1 Note: Complete procedure each day after running samples. The sample will vent 4 to 6 times and lose 2 to 3 mL of water 1. Create the following method using the document, CEM Synergy–D Software Operating Procedures in the section “Create New Methods.”...
  • Page 2 NOTE: If stirring does not occur, try using a larger/stronger stir bar. NOTE: The prepared sample can be used to determine adequate stirring speed for each sample. NOTE: If stirring does not work properly, contact CEM Service: service@cem.com. IR Temperature Verification with Water – to be done MONTHLY 1.
  • Page 3 The temperature should be within 6°C of 200°C. If the temperature is not within 6°C of 200°C, contact CEM service: service@cem.com Additional Tips The ActiVent vapor seal should be checked on a weekly basis •...

This manual is also suitable for:

Discover sp-d 80