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810 Sample Processor
Manual
8.810.8001EN / 2019-12-06

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Summary of Contents for Metrohm 810

  • Page 1 810 Sample Processor Manual 8.810.8001EN / 2019-12-06...
  • Page 3 Metrohm AG CH-9100 Herisau Switzerland Phone +41 71 353 85 85 Fax +41 71 353 89 01 info@metrohm.com www.metrohm.com 810 Sample Processor Manual 8.810.8001EN / 2019-12-06...
  • Page 4 Technical Communication Metrohm AG CH-9100 Herisau techcom@metrohm.com This documentation is protected by copyright. All rights reserved. This documentation has been prepared with great care. However, errors can never be entirely ruled out. Please send comments regarding possible errors to the address above.
  • Page 5: Table Of Contents

    ■■■■■■■■■■■■■■■■■■■■■■ Table of contents Table of contents 1 Introduction The 810 Sample Processor with operating instru- ments ..................1 Instrument description ............2 1.2.1 Instrument components ............3 1.2.2 Intended use ................3 About the documentation ........... 3 1.3.1 Symbols and conventions ............4 Safety instructions ..............
  • Page 6 7 Technical specifications Lift and turntable ............... 38 Membrane pump with valve ..........38 Interfaces and connectors ..........38 Power connection ............... 39 Ambient temperature ............39 Reference conditions ............39 Dimensions ................39 8 Accessories Index ■■■■■■■■ 810 Sample Processor...
  • Page 7 ■■■■■■■■■■■■■■■■■■■■■■ Table of figures Table of figures Figure 1 A complete system consisting of operating instrument with 810 Sam- ple Processor ..................1 Figure 2 810 Sample Processor Front .............. 9 Figure 3 810 Sample Processor rear .............. 10 Figure 4 Connector strip ................
  • Page 9: Introduction

    ■■■■■■■■■■■■■■■■■■■■■■ 1 Introduction 1 Introduction The 810 Sample Processor with operating instru- ments The 810 Sample Processor is a sample changer for the following operating instruments : 915 KF Ti-Touch ■ 916 Ti-Touch ■ Operation is carried out by an operating instrument with a corresponding software.
  • Page 10: Instrument Description

    12 Operating instrument 13 810 Sample Processor 14 USB RS adapter (6.2148.050) NOTICE It is possible to connect one 810 Sample Processor per operating instru- ment. Updating the device software is described in the manual of the operating instrument. Instrument description The 810 Sample Processor is a versatile instrument.
  • Page 11: Instrument Components

    Remote Boxes. 1.2.2 Intended use The 810 Sample Processor is designed for usage as a sample changer in analytical laboratories. It is not suitable for usage in biochemical, biologi- cal or medical environments in its basic equipment version.
  • Page 12: Symbols And Conventions

    Warning This symbol draws attention to a possible biological hazard. Caution This symbol draws attention to a possible damage of instruments or instrument parts. Note This symbol marks additional information and tips. ■■■■■■■■ 810 Sample Processor...
  • Page 13: Safety Instructions

    The electrical safety when working with the instrument is ensured as part of the international standard IEC 61010. WARNING Only personnel qualified by Metrohm are authorized to carry out service work on electronic components. WARNING Never open the housing of the instrument. The instrument could be damaged by this.
  • Page 14: Tubing And Capillary Connections

    Personnel safety WARNING Wear protective goggles and working clothes suitable for laboratory work while operating the 810 Sample Processor. It is also advisable to wear gloves when caustic liquids are used or in situations where glass vessels could break. WARNING Always install the safety shield supplied with the equipment before using the instrument for the first time.
  • Page 15: Flammable Solvents And Chemicals

    WARNING The 810 Sample Processor is not suitable for utilization in biochemical, biological or medical environments in its basic equipment version. Appropriate protective measures must be implemented in the event that potentially infectious samples or reagents are being processed.
  • Page 16 ■■■■■■■■■■■■■■■■■■■■■■ 1.4 Safety instructions More details about the disposal of your old instrument can be obtained from your local authorities, from waste disposal companies or from your local dealer. ■■■■■■■■ 810 Sample Processor...
  • Page 17: Overview Of The Instrument

    ■■■■■■■■■■■■■■■■■■■■■■ 2 Overview of the instrument 2 Overview of the instrument Front and rear Figure 2 810 Sample Processor Front Safety shield (6.2751.080) Sample rack (6.2041.310) Other models, see chap. Accessories. Other models, see chap. Accessories. Assembly rail Guide chain For magnetic stirrer (741 Stirrer).
  • Page 18: Figure 3 810 Sample Processor Rear

    ■■■■■■■■■■■■■■■■■■■■■■ 2.1 Front and rear US B 2 Figure 3 810 Sample Processor rear Distributor Membrane pump For rinsing equipment. Pump 1. Pump connector Pump valve Pump 2. For the external pump. Swing Head connector (optional) Stirrer connector Mini DIN socket (9-pin).
  • Page 19: Back Panel

    A sample rack is a turntable that acts as a receptacle for sample vessels. Various types of sample racks are available for different numbers and types of sample vessels. The 810 Sample Processor requires sample racks with up to a maximum of 42 cm diameter. Figure 5 Sample rack 6.2041.470...
  • Page 20 This will enable an unambiguous recognition of the rack and thus the cor- rect positioning of the beaker. A positioning table is assigned to each rack type in which each rack position is defined. ■■■■■■■■ 810 Sample Processor...
  • Page 21: Setting Up The Instrument

    Unplug the power plug immediately if you suspect that moisture has ■ gotten inside the instrument. Only personnel who have been issued Metrohm qualifications may ■ perform service and repair work on electrical and electronic parts. ■■■■■■■■...
  • Page 22: Connecting An Operating Instrument

    ■ Connecting an operating instrument The 810 Sample Processor requires a USB connection to the operating instrument in order for it to be controlled. Using a 6.2151.000 controller cable, the instrument can be connected directly, either to a USB socket on the operating instrument or to a connected USB hub.
  • Page 23: Installing The Rinsing And Aspiration Equipment

    M6 bore holes of the distributor. Place the tubings into the guide chain . These are the feed lines for the spray nozzles. 2 Mounting the aspiration tubing Manually tighten the 6.1805.510 FEP aspiration tubing (60 ■ cm) in the M8 bore hole of the distributor. ■■■■■■■■ 810 Sample Processor...
  • Page 24: Guide Chain For Cables And Tubing

    This could lead to overloading of and possible damage to the drive. Do not place rigid tubings, as for example aspiration tubings made of PTFE, into the guide chain. ■■■■■■■■ 810 Sample Processor...
  • Page 25: Installing The Titration Head

    Installing the titration head Mounting the titration head 6.1458.010 Figure 7 Mounting the titration head 1 Place the titration head (e.g. 6.1458.010) into the opening of the titration head holder and screw tight with the enclosed screws. ■■■■■■■■ 810 Sample Processor...
  • Page 26: Figure 8 Installing Accessories For The Titration

    Installing accessories for the titration 1 Insert three spray nozzles (6.2740.020) or rinsing nozzles (6.2740.030) into the oblique bore holes of the titration head, see figure. 2 Insert two 6.2709.070 guide sleeves into the titration head, see figure. ■■■■■■■■ 810 Sample Processor...
  • Page 27: Figure 9 Connecting The Tubings

    6.1543.170 6.2740.020 Figure 9 Connecting the tubings 1 Tighten the 6.1805.420 rinsing tubings which have been fas- tened to the distributor on the rear of the tower to the spray or rinsing nozzles (6.2740.020 or 6.2740.030). ■■■■■■■■ 810 Sample Processor...
  • Page 28: Figure 10 Rod Stirrer 802 Stirrer

    Connecting a stirrer to the tower NOTICE If an MSB stirrer is connected to the MSB1 socket, then the stirrer con- nector on tower 1 cannot be used, because both sockets are controlled internally via MSB1. ■■■■■■■■ 810 Sample Processor...
  • Page 29: Figure 13 Inserting The Rod Stirrer

    Installing the 741 Stirrer A magnetic stirrer (741 Stirrer) can be used as an alternative to a rod stir- rer. 1 Hang the magnetic stirrer to the assembly rail between the tower and the turntable. ■■■■■■■■ 810 Sample Processor...
  • Page 30: Connecting An External Pump

    Ext. Pump 2 on the rear of the tower. Pay attention to the orientation of the three contact pins. Tighten the knurled screw at the front end of the plug by hand in ■ clockwise direction. This secures the plug. ■■■■■■■■ 810 Sample Processor...
  • Page 31: Connecting Msb Devices

    In order to connect MSB devices, e.g. stirrers or dosing devices, Metrohm instruments are equipped with up to a maximum of four connectors on what is referred to as the Metrohm Serial Bus (MSB). Various kinds of peripheral devices can be connected in sequence (in series, as a "Daisy Chain") at a single MSB connector (8-pin Mini DIN socket) and con-...
  • Page 32: Connecting A Dosing Device

    805 Dosimat ■ WARNING If a Dosino is connected to the 810 Sample Processor, then the connec- tion cable must be equipped with a T.2400.102 ferrite core. The ferrite core diminishes any interference voltages and thus ensures compliance with the strict EMC standards in accordance with the applicable techni- cal standards, see EU declaration of conformity of the instrument.
  • Page 33: Connecting A Stirrer Or Titration Stand

    804 Ti Stand only: Connect the rod stirrer to the stirrer connector ■ (socket with stirrer symbol) of the titration stand. Switch on the operating instrument. ■ US B 1 Co ntr . MS B 2 MS B 3 Figure 17 Connecting an MSB stirrer ■■■■■■■■ 810 Sample Processor...
  • Page 34: Connecting A Remote Box

    Instruments that are controlled via remote lines and/or that send control signals via remote lines can be connected via the 6.2148.010 Remote Box. In addition to Metrohm, other instrument manufacturers also use similar connectors that make it possible to connect different instruments together.
  • Page 35: Connecting Usb Devices

    Connecting USB devices Two USB connectors (type A sockets) are available for connecting instru- ments with an USB interface. The 810 Sample Processor then functions as USB hub (distributor). If you wish to connect more than two USB devices, you can also use an additional, commercially available USB hub.
  • Page 36: Mounting The Drip Pan

    1 Fasten the enclosed tubing to the drainage nipple on the drip pan and then guide the free end of the tubing into a waste container. 2 Place the drip pan on the assembly rail of the turntable as shown in the figure. ■■■■■■■■ 810 Sample Processor...
  • Page 37: Attaching A Sample Rack

    NOTICE Hold the rack in such a way that the printed Metrohm logo is legi- ble horizontally. 2 Carry out the [Rack reset] or [Initialize rack] function in the man- ual control of the control software.
  • Page 38: Figure 22 Mounting The Safety Shield

    You can adjust the vertical position of the safety shield at any time by loosening the screws. The optimum vertical position meets the following criteria: The rack can rotate freely. ■ Nobody can access the working area of the lift while the instru- ■ ment is in operation. ■■■■■■■■ 810 Sample Processor...
  • Page 39: Maintenance

    Maintenance The electronic and mechanical functional groups of Metrohm instruments can and should be checked by specialist personnel from Metrohm as part of a regular preventive maintenance schedule. Please ask your local Metrohm representative regarding the precise terms and conditions involved in concluding a corresponding maintenance agreement.
  • Page 40: Troubleshooting

    "System / rectly configured. Device manager / Sample Processor / Swing Head / Robotic arm". Sample Processor – The Initialize the rack using the function [Reset wrong rack table is being rack] in the "Manual control". used. ■■■■■■■■ 810 Sample Processor...
  • Page 41: Pump

    Make sure that the canisters are not placed ■ much pressure on the on a higher level than the pump. pump valve. Check the fill level of the canisters. ■ Make sure that the canisters are not com- ■ pletely sealed (overpressure). ■■■■■■■■ 810 Sample Processor...
  • Page 42: Appendix

    6.2740.030 rinsing nozzle (optionally available) ■ The rinsing liquid is applied as a fine jet for optimal removal of layers on electrodes and on titration accessories. ■■■■■■■■ 810 Sample Processor...
  • Page 43: Remote Interface

    MSB interface of the Sample Processor. Figure 25 Connectors of the Remote Box Cables MSB connector For connecting to an MSB connector of the Metrohm Serial Bus. For connecting external Sample Processor. dosing devices or stirrers. Remote connector For connecting instruments with a remote interface.
  • Page 44: Pin Assignment Of The Remote Interfaces

    Pin assignment of remote socket and remote plug The above figure of the pin assignment of a Metrohm remote interface does not only apply for the Remote Box, but also for all Metrohm devices with 25-pin D-Sub remote connectors. Inputs +5 V approx.
  • Page 45 Assignment Pin no. Assignment Pin no. Input 6 Output 6 Input 7 Output 7 0 volts / GND Output 8 +5 volt Output 9 0 volts / GND Output 10 Output 11 Output 12 Output 13 ■■■■■■■■ 810 Sample Processor...
  • Page 46: Technical Specifications

    15 steps each in both rotation directions. Pump connectors A socket with M8 thread for 772 Pump Unit or 823 Membrane Pump Unit. U = 16 ± 1 V, I = ≤ 0.8 A Swing Head con- 9-pin Mini DIN socket nector ■■■■■■■■ 810 Sample Processor...
  • Page 47: Power Connection

    –40 - 60 °C Reference conditions Ambient tempera- 25 °C (±3 °C) ture ≤ 60 % Relative humidity Dimensions Width 0.28 m Height 0.73 m Depth 0.50 m Weight (without 14.52 kg accessories) Material Housing Metal housing, surface-treated ■■■■■■■■ 810 Sample Processor...
  • Page 48: Accessories

    Downloading the accessories list 1 Enter https://www.metrohm.com/ into your Internet browser. 2 Enter the article number (e.g. 810) into the search field. The search result is displayed. 3 Click on the product. Detailed information regarding the product is shown on various tabs.
  • Page 49: Index

    Sample rack ......11 Magnetic stirrer Serial number ......11 Mount ........ 20 Connect Service ........5 Metrohm Serial Bus MSB, see also Barcode reader ....27 Stirrer "MSB" ........23 Dosing device ..... 24 Connect ....... 20, 25 Mount MSB devices .......

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