Metrohm 930 Compact IC Flex Short Instructions
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Metrohm 930 Compact IC Flex Short Instructions

Oven ses/pp/deg
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930 Compact IC Flex
930 Compact IC Flex Oven SeS/PP/Deg
Manual – Short Instructions
8.930.8120EN / 2017-07-31

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  • Page 1 930 Compact IC Flex 930 Compact IC Flex Oven SeS/PP/Deg Manual – Short Instructions 8.930.8120EN / 2017-07-31...
  • Page 3 Metrohm AG CH-9100 Herisau Switzerland Phone +41 71 353 85 85 Fax +41 71 353 89 01 info@metrohm.com www.metrohm.com 930 Compact IC Flex 930 Compact IC Flex Oven SeS/PP/Deg 2.930.2560 Manual – Short Instructions 8.930.8120EN / 2017-07-31...
  • Page 4 Technical Communication Metrohm AG CH-9100 Herisau techcom@metrohm.com This documentation is protected by copyright. All rights reserved. This documentation has been prepared with great care. However, errors can never be entirely ruled out. Please send comments regarding possible errors to the address above.

  • Page 5: Table Of Contents

    4.10 Installing the pulsation absorber ........19 4.11 Injection valve ..............19 4.12 Metrohm Suppressor Module (MSM) ....... 19 4.12.1 Inserting the rotors ..............20 4.12.2 Connecting the Metrohm Suppressor Module (MSM) ..... 21 ￭￭￭￭￭￭￭￭ 930 Compact IC Flex Oven SeS/PP/Deg (2.930.2560)
  • Page 6 4.19 Connecting the instrument to the power grid ....31 4.20 Initial start-up ..............32 4.21 Connecting and rinsing the guard column ....... 34 4.22 Connecting the separation column ........35 4.23 Conditioning ................ 37 5 Operation 6 Accessories Index ￭￭￭￭￭￭￭￭ 930 Compact IC Flex Oven SeS/PP/Deg (2.930.2560)
  • Page 7 Removing the transport locking screws ..........13 Figure 4 Installing tubing weighting and aspiration filter ........ 18 Figure 5 Metrohm Suppressor Module (MSM) – Connection capillaries ..22 Figure 6 Connecting the MCS ............... 26 ￭￭￭￭￭￭￭￭ 930 Compact IC Flex Oven SeS/PP/Deg (2.930.2560)

  • Page 9: About These Short Instructions

    In addition to an introduction, safety instructions and an overview of the instrument, you will also find information about instal- ling and operating the 930 Compact IC Flex Oven SeS/PP/Deg as well as information regarding the warranty. You can download the comprehen- sive manual as a PDF file from the Internet.

  • Page 10: Introduction

    2.1 Instrument description 2 Introduction Instrument description The 930 Compact IC Flex is a robust ion chromatograph. It is distinguished Its intelligence: All of the functions are monitored, optimized and docu- ￭ mented in an FDA-compatible manner. Intelligent components, such as iColumns, save important data onto a chip.
  • Page 11 The rotor required for the application and any adapter that is required must be ordered separately. Peristaltic pump The peristaltic pump is used for pumping sample and auxiliary solutions. It can rotate in both directions. ￭￭￭￭￭￭￭￭ 930 Compact IC Flex Oven SeS/PP/Deg (2.930.2560)

  • Page 12: Intended Use

    This instrument is suitable for processing chemicals and flammable sam- ples. Therefore, the use of the 930 Compact IC Flex requires the user to have basic knowledge and experience in handling toxic and caustic sub- stances.

  • Page 13: Safety Instructions

    The electrical safety when working with the instrument is ensured as part of the international standard IEC 61010. WARNING Only personnel qualified by Metrohm are authorized to carry out service work on electronic components. WARNING Never open the housing of the instrument. The instrument could be damaged by this.

  • Page 14: Tubing And Capillary Connections

    This product is covered by European Directive 2012/19/EU, WEEE – Waste Electrical and Electronic Equipment. The correct disposal of your old instrument will help to prevent negative effects on the environment and public health. ￭￭￭￭￭￭￭￭ 930 Compact IC Flex Oven SeS/PP/Deg (2.930.2560)

  • Page 15: Symbols And Conventions

    WARNING This symbol draws attention to a possible biological hazard. CAUTION This symbol draws attention to possible damage to instruments or instrument parts. NOTE This symbol highlights additional information and tips. ￭￭￭￭￭￭￭￭ 930 Compact IC Flex Oven SeS/PP/Deg (2.930.2560)

  • Page 16: Overview Of The Instrument

    Bottle holder Column holder For hanging the separation column (iCol- umn). With column recognition. Column oven Metrohm Suppressor Module (MSM) Sample degasser Inline filter Injection valve Purge valve Pulsation absorber 10 Base tray ￭￭￭￭￭￭￭￭ 930 Compact IC Flex Oven SeS/PP/Deg (2.930.2560)

  • Page 17: Rear

    Room for the detector and the adsorption cartridge for the MCS. Rear Figure 2 Rear Bottle holder Drainage tubing connection For connecting the drainage tubing, which guides escaped fluids away from the bottle holder. ￭￭￭￭￭￭￭￭ 930 Compact IC Flex Oven SeS/PP/Deg (2.930.2560)
  • Page 18 For connecting the instrument to the com- Plugged with a stopper. puter with the USB cable (6.2151.020). 21 Power socket Power socket for connecting the power cable and power switch for switching the instrument on and off. ￭￭￭￭￭￭￭￭ 930 Compact IC Flex Oven SeS/PP/Deg (2.930.2560)

  • Page 19: Installation

    (6.2739.000). ￭ In order to achieve optimum analysis results, capillary connections in an IC system must be absolutely tight and free of dead volume. Dead volume ￭￭￭￭￭￭￭￭ 930 Compact IC Flex Oven SeS/PP/Deg (2.930.2560)

  • Page 20: Removing Transport Locking Screws

    These are located at the rear of the instrument and labeled with Transport security screws. Remove these transport locking screws before the initial start-up. Accessories For this step you need: 4 mm hex key (6.2621.030) ￭ ￭￭￭￭￭￭￭￭ 930 Compact IC Flex Oven SeS/PP/Deg (2.930.2560)

  • Page 21: Figure 3 Removing The Transport Locking Screws

    Store the transport locking screws in a safe place. Reinsert the transport locking screws each time you transport the instrument a significant dis- tance. CAUTION The pumps may be damaged if you transport the instrument without inserting the transport locking screws. ￭￭￭￭￭￭￭￭ 930 Compact IC Flex Oven SeS/PP/Deg (2.930.2560)

  • Page 22: Connecting The Drainage Tubing And Leak Sensor

    The drainage tubing is connected. ￭ The leak sensor connection cable is inserted into the leak sensor con- ￭ nection socket. The 930 Compact IC Flex is switched on. ￭ The leak sensor is switched to active in the software. ￭ 4.4.1...

  • Page 23: Connecting The Leak Sensor

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 4 Installation Connecting the drainage tubing 4.4.2 Connecting the leak sensor Plugging in the leak sensor connection cable The leak sensor connection cable is coiled up in the base tray. ￭￭￭￭￭￭￭￭ 930 Compact IC Flex Oven SeS/PP/Deg (2.930.2560)

  • Page 24: Column Oven

    The tubing adapter for aspiration filter accessory set (6.2744.210) ￭ This accessory set contains a filter holder, a clamping screw and tubing weighting. An aspiration filter (6.2821.090) ￭ The adsorber tube (6.1609.000) ￭ The SGJ clip (6.2023.020) ￭ ￭￭￭￭￭￭￭￭ 930 Compact IC Flex Oven SeS/PP/Deg (2.930.2560)
  • Page 25 Always wear gloves when handling the aspiration filter. In order to avoid air bubbles after the installation of the aspiration fil- ter, we recommend pre-rinsing the aspiration filter with water or elu- ent. ￭￭￭￭￭￭￭￭ 930 Compact IC Flex Oven SeS/PP/Deg (2.930.2560)

  • Page 26: Connecting The Eluent Degasser

    Tighten the aspiration filter to the filter holder. ￭ Figure 4 Installing tubing weighting and aspiration filter Connecting the eluent degasser The eluent degasser is completely connected. No installation work is required. ￭￭￭￭￭￭￭￭ 930 Compact IC Flex Oven SeS/PP/Deg (2.930.2560)

  • Page 27: Installing The High-Pressure Pump

    4.12 Metrohm Suppressor Module (MSM) The suppressor drive of the 930 Compact IC Flex can hold various rotors. The large rotors, such as the MSM‑HC Rotor A (6.2842.000) and the MSM-HC Rotor C (6.2842.200) can be inserted directly. The small rotors, such as the MSM Rotor A (6.2832.000) and the MSM-LC Rotor A (6.2844.000), must first be fitted into the adapter (6.2842.020),...

  • Page 28: Inserting The Rotors

    Connecting piece (6.2835.010) ￭ Large rotors can be inserted directly into the rotor housing. CAUTION The rotor may be destroyed during start-up if not inserted correctly. Therefore, follow the following instructions exactly. ￭￭￭￭￭￭￭￭ 930 Compact IC Flex Oven SeS/PP/Deg (2.930.2560)

  • Page 29: Connecting The Metrohm Suppressor Module (Msm)

    Connecting the Metrohm Suppressor Module (MSM) The three entries and exits of the suppressor units, numbered 1, 2 and 3 on the connecting piece, each have two permanently installed PTFE capil- laries. ￭￭￭￭￭￭￭￭ 930 Compact IC Flex Oven SeS/PP/Deg (2.930.2560)

  • Page 30: Figure 5 Metrohm Suppressor Module (Msm) - Connection Capillaries

    Outlet capillary for the regeneration solu- tion; to the waste container. waste rins. rinsing solution Outlet capillary for the rinsing solution; to Inlet capillary for the rinsing solution. the waste container. Recommended installation ￭￭￭￭￭￭￭￭ 930 Compact IC Flex Oven SeS/PP/Deg (2.930.2560)
  • Page 31 4.12.2.1 Installing bottles with auxiliary solutions Accessories To connect the bottles of the auxiliary solutions, you will need the follow- ing accessories: Accessories from the accessory kit: IC Vario/Flex SeS (6.5000.020) ￭ ￭￭￭￭￭￭￭￭ 930 Compact IC Flex Oven SeS/PP/Deg (2.930.2560)

  • Page 32: Peristaltic Pump

    Coupling olive/UNF 10/32 (6.2744.034) ￭ Pump tubing connection with locking nut and filter (6.2744.180): ￭ Includes a locknut, 3 adapters and a tubing olive with filter holder. 2 × pressure screw, short (6.2744.070) ￭ ￭￭￭￭￭￭￭￭ 930 Compact IC Flex Oven SeS/PP/Deg (2.930.2560)
  • Page 33 Raise the contact pressure lever one step at a time until liquid ￭ flows. When liquid starts flowing, raise the contact pressure lever by an ￭ additional two ratchet increments. The contact pressure is now set optimally. ￭￭￭￭￭￭￭￭ 930 Compact IC Flex Oven SeS/PP/Deg (2.930.2560)

  • Page 34: Metrohm Co Suppressor (Mcs)

    Suppressor (MCS) 4.14 Metrohm CO Suppressor (MCS) 4.14.1 Connecting the MCS The MCS is connected between the Metrohm Suppressor Module (MSM) and the conductivity detector. Connecting the MCS Figure 6 Connecting the MCS Air aspiration capillary Pressure screw, short (6.2744.070)
  • Page 35 CW, through which air is aspirated. The CO adsorption cartridge CW is now ready for installation. NOTE The new CO adsorption cartridge CW (6.2837.100) works without attached H O adsorption cartridge. ￭￭￭￭￭￭￭￭ 930 Compact IC Flex Oven SeS/PP/Deg (2.930.2560)

  • Page 36: Installing The Conductivity Detector

    CW as follows: 4.15 Installing the conductivity detector The 930 Compact IC Flex provides enough space for one detector and additional accessories in the detector chamber. The detector is available as separate device and is supplied with a separate manual.

  • Page 37: Installing The Amperometric Detector

    4 Installation 4.16 Installing the amperometric detector The 930 Compact IC Flex provides enough space for one detector and additional accessories in the detector chamber. The detector is available as separate device and is supplied with a separate manual. Placing the detector in the instrument Follow the instructions in the chapter Inserting the detector in the manual for the detector.

  • Page 38: Connecting The Instrument To A Computer

    If the instrument is connected to the computer, then it must be switched off. Accessories For this step, you need the following accessories: USB connection cable (6.2151.020) from the accessory kit: Vario/Flex ￭ Basic (6.5000.000) ￭￭￭￭￭￭￭￭ 930 Compact IC Flex Oven SeS/PP/Deg (2.930.2560)

  • Page 39: Connecting The Instrument To The Power Grid

    Unplug the power plug immediately if you suspect that moisture has ￭ gotten inside the instrument. Only personnel who have been issued Metrohm qualification may ￭ perform service and repair work on electrical and electronic parts. ￭￭￭￭￭￭￭￭...

  • Page 40: Initial Start-Up

    Also see: MagIC Net Tutorial and online help. 2 Preparing the instrument Ensure that the eluent aspiration tubing is immersed in the eluent ￭ and that there is enough eluent in the eluent bottle. ￭￭￭￭￭￭￭￭ 930 Compact IC Flex Oven SeS/PP/Deg (2.930.2560)
  • Page 41 Check whether the detector outlet capillary is connected to the Metrohm Suppressor Module (MSM)'s inlet capillary for rinsing solu- tion (labeled rinsing solution).

  • Page 42: Connecting And Rinsing The Guard Column

    (6.2744.040) until then. Accessories For this step, you need the following accessories: Guard column (suitable for separation column) ￭ ￭￭￭￭￭￭￭￭ 930 Compact IC Flex Oven SeS/PP/Deg (2.930.2560)

  • Page 43: Connecting The Separation Column

    NOTE Connect the separation column only after the initial start-up of the instrument. Until that point, insert a coupling (6.2744.040) instead of the guard column and separation column. ￭￭￭￭￭￭￭￭ 930 Compact IC Flex Oven SeS/PP/Deg (2.930.2560)
  • Page 44 Manual ▶ Manual control ▶ Pump – Flow: Increase gradually up to the flow rate recommended in the column leaflet. – On Rinse the separation column with eluent for approx. 10 minutes. ￭ ￭￭￭￭￭￭￭￭ 930 Compact IC Flex Oven SeS/PP/Deg (2.930.2560)

  • Page 45: Conditioning

    (arrow has to point in the direction of flow). Ensure that the eluent aspiration tubing is immersed in the eluent ￭ and that there is enough eluent in the eluent bottle. ￭￭￭￭￭￭￭￭ 930 Compact IC Flex Oven SeS/PP/Deg (2.930.2560)
  • Page 46 4 Conditioning the system Continue rinsing the system with eluent until the desired stability level for the baseline has been attained . The instrument is now ready for measuring samples. ￭￭￭￭￭￭￭￭ 930 Compact IC Flex Oven SeS/PP/Deg (2.930.2560)

  • Page 47: Operation

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 5 Operation 5 Operation The 930 Compact IC Flex Oven SeS/PP/Deg is operated solely using the MagIC Net software. You can find information on operating the software in the tutorial for MagIC Net or in the online help. ￭￭￭￭￭￭￭￭...

  • Page 48: Accessories

    The PDF file with the accessories data will be created. NOTE When you receive your new instrument, we recommend downloading the accessories list from the Internet, printing it out and keeping it together with the manual for reference purposes. ￭￭￭￭￭￭￭￭ 930 Compact IC Flex Oven SeS/PP/Deg (2.930.2560)

  • Page 49: Index

    Equilibration ....... 33, 38 Vacuum pump Capillary connection ... 26 Protection ......13 Cartridge connection ..26 Valve Filter Installation ......26 See also "Injection valve" ..19 see "Inline filter" ....19 ￭￭￭￭￭￭￭￭ 930 Compact IC Flex Oven SeS/PP/Deg (2.930.2560)

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