Spectrasensors SS1000 Operator's Manual
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Spectrasensors SS1000 Operator's Manual

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SS1000
Gas Analyzers
Operator's Manual
Tel: +44 (0)1943 878877 Email: info@ima.co.uk Web: www.ima.co.uk
UK Distibution by IMA Ltd

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  • Page 1 SS1000 Gas Analyzers Operator’s Manual Tel: +44 (0)1943 878877 Email: info@ima.co.uk Web: www.ima.co.uk UK Distibution by IMA Ltd...
  • Page 2 SS1000 Operator’s Manual THIS PAGE INTENTIONALLY LEFT BLANK 49000-02079 rev. A 4-29-10 Tel: +44 (0)1943 878877 Email: info@ima.co.uk Web: www.ima.co.uk UK Distibution by IMA Ltd...
  • Page 3 Tel: +44 (0)1943 878877 Email: info@ima.co.uk Web: www.ima.co.uk UK Distibution by IMA Ltd...
  • Page 4 Fax: 909.948.4100 www.spectrasensors.com Copyright © 2010 SpectraSensors, Inc. No part of this manual may be reproduced in whole or in part without the express written permission of SpectraSensors, Inc. SpectraSensors reserves the right to change product design and specifications at any time without prior notice.
  • Page 5 THIS PAGE INTENTIONALLY LEFT BLANK Tel: +44 (0)1943 878877 Email: info@ima.co.uk Web: www.ima.co.uk UK Distibution by IMA Ltd...

  • Page 6: Table Of Contents

    SpectraSensors Overview ........
  • Page 7 SS1000 Operator’s Manual Pipeline Pressure (if applicable) ....... . 3-10 Modbus Address .

  • Page 8: Table Of Contents

    Table of Contents 49000-02079 rev. A 4-29-10 Tel: +44 (0)1943 878877 Email: info@ima.co.uk Web: www.ima.co.uk UK Distibution by IMA Ltd...
  • Page 9 SS1000 Operator’s Manual THIS PAGE INTENTIONALLY LEFT BLANK 49000-02079 rev. A 4-29-10 Tel: +44 (0)1943 878877 Email: info@ima.co.uk Web: www.ima.co.uk UK Distibution by IMA Ltd...
  • Page 10 1-6 Figure 1–4: Typical normalized 2 signal where the species concentration is propor- tional to the peak height. 1-7 Figure 3–1: SS1000 keypad. 3-3 Figure 4–1: Connection Description window. 4-2 Figure 4–2: Connect To window. 4-2 Figure 4–3: COM Properties window. 4-3 Figure 4–4:...
  • Page 11 Potential instrument problems and solutions . A-10 Table B–1: SS1000 moisture in natural gas analyzer specifications. B-1 Table B–2: SS1000 carbon dioxide in natural gas analyzer specifications. B-2 Table B–3: Replacement parts for SS1000 SS1000 Operator’s Manual analyzers. B-5 SS1000 Operator’s Manual Tel: +44 (0)1943 878877 Email: info@ima.co.uk Web: www.ima.co.uk...
  • Page 12 SS1000 Operator’s Manual THIS PAGE INTENTIONALLY LEFT BLANK i i i Tel: +44 (0)1943 878877 Email: info@ima.co.uk Web: www.ima.co.uk UK Distibution by IMA Ltd...

  • Page 13: Who Should Read This Manual

    Take a moment to familiarize yourself with this Operator’s Manual by reading the Table of Contents. There are a number of options and accessories available for the SS1000 analyzers. This manual has been written to address the most common options and accessories.

  • Page 14: Special Symbols Used In This Manual

    SS1000 Operator’s Manual Special Symbols Used in This Manual This manual uses the following symbols to represent potential hazards, caution alerts, and important information associated with the analyzer. Every symbol has significant meaning that should be heeded. This icon denotes a warning statement. Warning statements indicate a potentially hazardous situation which, if not avoided, may result in serious injury or death.
  • Page 15 When selecting an analyzer, the total system design must be considered to ensure safe, trouble-free performance. Function, sizing, proper installation, operation, and maintenance are beyond the control of SpectraSensors and are the responsibilities of the system designer and user. –...

  • Page 16: Spectrasensors Overview

    Most SS1000 analyzer systems are configured for use at extractive natural gas sampling stations. How the Analyzer Works The SS1000 analyzer employs tunable diode laser absorption spectroscopy (TDLAS) to detect the presence of trace substances in process gases.
  • Page 17 Introduction GAS OUT DETECTOR I(λ) LASER (λ) TRACE GAS ABSORPTION α(λ) GAS IN Figure 1–1 Schematic of a typical laser diode absorption spectrometer. Due to their inherent structure, the molecules in the sample gas each have characteristic natural frequencies (or resonances). When the output of the laser is tuned to one of those natural frequencies, the molecules with that particular resonance will absorb energy from the incident beam.
  • Page 18 SS1000 Operator’s Manual Figure 1–2 Typical raw signal from a laser diode absorption spectrometer with and without mirror contamination. Figure 1–3 Typical normalized absorption signal from a laser diode absorption spectrometer. – Tel: +44 (0)1943 878877 Email: info@ima.co.uk Web: www.ima.co.uk...
  • Page 19 (ppb) detection levels are possible (depending on target and background species) at real-time response rates (on the order of 1 second). All SpectraSensors TDL gas analyzers employ the same design and hardware platform. Measuring different trace gases such as H...
  • Page 20 SpectraSensors TDL analyzers the most reliable gas analyzer platform with the lowest total cost of ownership.

  • Page 21: What Should Be Included In The Shipping Box

    What Should be Included in the Shipping Box The contents of the box should include: • The SpectraSensors SS1000 • This Operator’s Manual with instructions on setting up and operating the analyzer •...

  • Page 22: Tools

    9/16" open-end wrench. Setting up the Analyzer The SS1000 analyzer is manufactured for temporary installation at a sampling point. Place the analyzer at a location relatively free of vibration and close to the sampling point. Choose a shaded area or use an optional analyzer hood (or equivalent) to minimize sun exposure.

  • Page 23: To Connect The Sample Supply Line

    Secure tubing to appropriate structural supports as required. 9. Check all connections for gas leaks. SpectraSensors recommends using a liquid leak detector. Do not exceed 10 psig (0.7 barg) in sample cell. Damage to cell may result.

  • Page 24: To Connect The Sample Return

    For connections with previously swaged ferrules, thread the nut to the previously pulled up position, then tighten slightly with a wrench. Secure tubing to appropriate structural supports as required. 6. Check all connections for gas leaks. SpectraSensors recommends using a liquid leak detector. Conditioning the SCS Tubing...

  • Page 25: Connecting Electrical Power To The Analyzer

    The analyzer can be connected to a serial port on a computer with the factory-supplied external serial cable. If the receiving computer has only a USB port available, a USB-to-serial adapter can be used. SpectraSensors recommends RadioShack P/N 26-183. ®...
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  • Page 27: 3: Operating The Analyzer

    15 while showing the firmware version, release date and measurement type [Dual Peak (DP) or Direct Measurement (DM)] on the bottom line. Initializing... v2.41 08-12-09 – SS1000 Operator’s Manual Tel: +44 (0)1943 878877 Email: info@ima.co.uk Web: www.ima.co.uk UK Distibution by IMA Ltd...

  • Page 28: Powering Down The Analyzer

    SS1000 Operator’s Manual 3. After initialization, the LCD displays the Normal Mode screen with four lines (the third of which is blank for single-channel units). <NORMAL MODE> H2O: 1.0256lb/mmscf P: 954.4mb T: 76.1F 4. Enable Peak Tracking following the procedure outlined in “To change parameters in Mode 2”...

  • Page 29: Modes Defined

    Operating the Analyzer The SpectraSensors keypad is shown in Figure 3–1. To activate any functions on the keypad, press the mode key # followed by a number on the keypad to specify a mode. You must press the # key before pressing a number or function key to trigger a response from the keypad.

  • Page 30: Mode 1: (Normal Mode)

    SS1000 Operator’s Manual Mode 1: (Normal Mode) Continuously displays updated measurements. Press the # key followed by the 1 key. The measurements displayed are: • H2O — Concentration in units selected in Mode 2. • P — Pressure in the sample cell in units selected in Mode 2.

  • Page 31: Mode 5: (Not Used)

    Operating the Analyzer • Powr: Shows the laser power detected at the absorption peak in A/D counts. Acceptable values are between 1000 and 2000. A number below 1000 may indicate that either the optics need to be cleaned or there is an alignment problem. A value below 200 will cause a Power Fail.

  • Page 32: Mode Test: (System Test)

    SS1000 Operator’s Manual Mode TEST: (System Test) Provides basic diagnostic test results indicating that the laser power, pressure/temperature sensors, and the infrared spectrum that the system records for analysis are all nominal. Press the # key followed by the TEST key.

  • Page 33: Table 3-1 Measurement And Control Parameters

    Default = 4 ments to include in a running average i l i off, on, or reset DO Alarm Setup Not applicable for SS1000 Alarm Setpoint Not applicable for SS1000 4-20 mA Alarm Action Not applicable for SS1000 4-20 mA % Test...

  • Page 34: Measurement And Control Parameters Defined

    SS1000 Operator’s Manual Measurement and Control Parameters Defined S Factor <SET PARAMETER MODE> S Factor 1.00000 Enter a value The S Factor parameter is a user definable value that enables adjustment (without affecting the factory calibration) of the analyzer response (or slope) in the field [see “Adjusting Analyzer Reading to Match Specific...

  • Page 35: Logger Rate

    Operating the Analyzer Logger Rate <SET PARAMETER MODE> Logger Rate Enter a value For applications where an external data logger is employed, use the logging rate to set the number of measurements to include in the running average. The display and the current loop output will each have a value representing the running average of the concentration over a number of measurements equal to Logger Rate.

  • Page 36: Pressure Unit

    SS1000 Operator’s Manual Pressure Unit <SET PARAMETER MODE> Pressure Unit 0:mb1:Torr2:kPa3:psi The Pressure Unit parameter designates the display units for the measured absolute pressure in the cell. There are four choices: 0 for millibar, 1 for Torr, 2 for kPa, and 3 for psia.

  • Page 37: Modbus Address

    Operating the Analyzer Modbus Address <SET PARAMETER MODE> Modbus Address Enter a value(1-250) The Modbus Address parameter sets the analyzer address for when the analyzer is used as a Modbus device. Addresses from 1 to 250 can be used. Modbus Mode <SET PARAMETER MODE>...

  • Page 38: User Sample Id

    SS1000 Operator’s Manual User Sample ID <SET PARAMETER MODE> User Sample ID Enter a value The User Sample ID parameter assigns a numeric identification to the data enabling SCADA or DCS systems to associate the data with a particular sample point.

  • Page 39: To Adjust The Analyzer Reading

    To adjust the analyzer reading: 1. Validate the analyzer using one or two concentration standards [see “Validating the Analyzer” on page 3-15]. SpectraSensors recommends validating the analyzer using only O & CO in CH . Bottles of test gas with certified concentrations of approximately 20% and 80% of full scale are recommended for two point validation.
  • Page 40 SS1000 Operator’s Manual 3. Press the 0 key followed by the * key to turn peak tracking off. Press the # key followed by the 1 key to return to Mode 1. 4. Press the # key followed by the 2 key. The LCD prompts for a <SET PARAMETER MODE>...

  • Page 41: Faults

    Operating the Analyzer 11. Scroll through the parameters by pressing the * key until arriving at the Peak Tracking parameter. <SET PARAMETER MODE> Peak Tracking 0:O 1:Track 2:Reset 12. Press the 1 key followed by the * key to turn peak tracking on. Press the # key followed by the 1 key to return to Mode 1.

  • Page 42: Calibrating The Analyzer

    Calibrating the Analyzer Calibrating the analyzer is typically not required under normal circumstances. SpectraSensors calibrates each analyzer to a National Institute of Standards and Technology (NIST) traceable standard before shipping the unit to the end user. Because SpectraSensors analyzers use a non-contact form of measurement, they are relatively insensitive to contamination, are quite rugged and virtually maintenance free ensuring years of reliable service.

  • Page 43: 4: Serial Port Communications

    7. Click OK to establish the connection. Once connected, the data will start streaming through the Hyperterminal Window as shown in Figure 4–4. – SS1000 Operator’s Manual Tel: +44 (0)1943 878877 Email: info@ima.co.uk Web: www.ima.co.uk UK Distibution by IMA Ltd...
  • Page 44 SS1000 Operator’s Manual Figure 4–1 Connection Description window. Figure 4–2 Connect To window. – Tel: +44 (0)1943 878877 Email: info@ima.co.uk Web: www.ima.co.uk UK Distibution by IMA Ltd...
  • Page 45 Serial Port Communications Figure 4–3 COM Properties window. Figure 4–4 Hyperterminal window with streaming data. – Tel: +44 (0)1943 878877 Email: info@ima.co.uk Web: www.ima.co.uk UK Distibution by IMA Ltd...

  • Page 46: To Capture And Save Data From The Serial Port

    SS1000 Operator’s Manual The data string is comma and space delimited with a carriage return and includes: • Concentration - analyte concentration (user selected units) • Pressure - cell pressure (user selected units) • Temperature - cell temperature (user selected units) •...

  • Page 47: Viewing Diagnostic Data With Microsoft Excel

    Serial Port Communications 3. Once capturing is in place, enter Mode 6 by pressing # key followed by the 6 key. Dump Stats Mode... Index: 0 The index shown on the LCD display counts by 50’s from 0 to 511 in a few seconds and the screen displays: Mode 4.
  • Page 48 SS1000 Operator’s Manual SpectraSensors HardHat: v2.31 Single 08-08-08 3181 3830 2699 3727 2007 3493 1359 3207 <<Information Deleted>> 3150 4095 3153 4095 3157 4095 Computational Statistics v2.31 Single 08-08-08 Ambient counts after averaging Voltage: -1368 Temperature: -1532 Pressure: -206 ac counts after averaging...
  • Page 49 Serial Port Communications Peak Track Temp Max: 60 PT Matrix: 1 fc0 Background Coeff: 1.00000E+00 fc1 Background Coeff: 0.00000E+00 fc2 Background Coeff: 0.00000E+00 fc3 Background Coeff: 0.00000E+00 fp0 Background Corr: 1.00000E+00 fp1 Background Corr: 0.00000E+00 fp2 Background Corr: 0.00000E+00 fp3 Background Corr: 0.00000E+00 pp2f Direction: 1 Ref Peak Range Min: -180 Ref Peak Range Max: -80...
  • Page 50 SS1000 Operator’s Manual Figure 4–7 a) Opening a data file in Excel. b) Setting data type in Text Import Wizard. – Tel: +44 (0)1943 878877 Email: info@ima.co.uk Web: www.ima.co.uk UK Distibution by IMA Ltd...
  • Page 51 Serial Port Communications Figure 4–8 a) Setting Tab and Space as delimiters. b) Highlighting imported data for plotting in Excel. – Tel: +44 (0)1943 878877 Email: info@ima.co.uk Web: www.ima.co.uk UK Distibution by IMA Ltd...

  • Page 52: Modbus Communications Protocol

    SS1000 Operator’s Manual Figure 4–9 Chart Wizard - Step 1 window. lines look like the normal serial output data received before the Mode 6 command was entered. Look for the three columns of numbers at the bottom of the file.
  • Page 53 Serial Port Communications 3000 2500 2000 1500 Series1 Series2 1000 -100 600 -150 -500 Figure 4–10 a) Data file plot in Excel. b) Format Data Series window. – Tel: +44 (0)1943 878877 Email: info@ima.co.uk Web: www.ima.co.uk UK Distibution by IMA Ltd...

  • Page 54: Framing/Protocol

    (RTU) in supervisory control and data acquisition (SCADA) systems. The SpectraSensors analyzer acts as a slave in a master/slave(s) network of devices. It can receive queries from a master and send responses back using either Gould Modbus RTU protocol or Daniel Extended Modbus RTU protocol.

  • Page 55: Reading/Writing In Gould Modbus Mode

    Other writable registers can only be downloaded or changed by SpectraSensors support personnel using a User Level 2 (L2) password. To enable Modbus communications: 1. Confirm that the serial cable has been properly connected. See “Connecting the Output Signals”...
  • Page 56 SS1000 Operator’s Manual 4. Press the * key repeatedly until the Modbus Address parameter is displayed. <SET PARAMETER MODE> Modbus Address Enter a value(1-250) 5. Enter the desired Modbus Address and press the * key to store the value and cycle to the Modbus Mode parameter.

  • Page 57: Table 4-1 Modbus Register Map

    7102 47203 Float R/W L1 Pipeline Pressure 7104 47207 Float 9999.9 R/W L1 4 mA span Not applicable for SS1000 20 mA span Not applicable for SS1000 Zero Offset 7151 47301 Float -100000 100000 R/W L2 Span Not applicable for SS1000...

  • Page 58: Modbus Accessible Parameter Definitions

    Short R/W L1 Logger Rate 3202 43202 Short R/W L1 Peak Tracking 3203 43203 Short R/W L1 Alarm Action Not applicable for SS1000 Temperature Unit 3205 43205 Short R/W L1 Pressure Unit 3206 43206 Short R/W L1 Concentration Unit 3207...
  • Page 59 Serial Port Communications • S Factor Offset – offset adjustment enabling the analyzer to be tuned to match a specific calibration standard without affecting the factory calibration. • Pipeline Pressure – sets the pressure used in calculating dew point. The pressure unit is mb when setting this parameter via Modbus communications and as set by the Pressure Unit parameter when setting via the front panel.
  • Page 60 User Level 1 password is downloaded to this register. Likewise, those registers denoted as R/W L2 can only be modified if the level 2 password is downloaded to this register. Level 2 registers are reserved for SpectraSensors personnel use only. – Tel: +44 (0)1943 878877 Email: info@ima.co.uk Web: www.ima.co.uk...

  • Page 61: Ss1000 Operator's Manual

    It is recommended the supply lines be Do not use plastic tubing of any kind for sample lines. Plastic tubing is permeable to moisture and other substances which can contaminate the sample stream. SpectraSensors recommends using 1/4" O.D x0.035" wall thickness, seamless stainless steel tubing.

  • Page 62: Contamination

    Secure tubing to appropriate structural supports as required. 8. Check all connections for gas leaks. SpectraSensors recommends using a liquid leak detector. Do not exceed 10 psig (0.7 barg) in sample cell. Damage to cell may result.

  • Page 63: Cleaning The Mirrors

    Secure tubing to appropriate structural supports as required. 8. Check all connections for gas leaks. SpectraSensors recommends using a liquid leak detector. Cleaning the Mirrors If contamination makes its way into the cell and accumulates on the internal optics, a Power Fail will result.

  • Page 64: To Clean The Mirrors

    9. Look inside the sample cell at the top mirror using a flashlight to ensure that there is no contamination on the top mirror. Due to its proximity to the optical head, SpectraSensors does not recommend cleaning the top mirror. If the top mirror is visibly contaminated, contact your factory service representative.

  • Page 65: Excessive Sampling Gas Temperatures And Pressures

    Troubleshooting 14. With gentle, uniform pressure, wipe the mirror from one edge to the other with the cleaning cloth only once and only in one direction to remove the contamination. Discard the cloth. Never rub an optical surface, especially with dry tissues, as this can mar or scratch the coated surface.

  • Page 66: To Check The Pkdf And Pkd1 Values

    SS1000 Operator’s Manual To check the PkDf and PkD1 values: For Channel A, press the # key followed by the 4 key to enter Mode 4 (System Diagnostic Parameters - Channel A) or press the # key followed by the 5 key PP2F:8190 PkDf:34.00...

  • Page 67: Instrument Problems

    Troubleshooting press the * key to enter the number to enter Mode 2 (Set Parameter <SET PARAMETER MODE> S Factor 1.00000 Enter a value Mode - Channel A) or Mode 3 (Set Parameter Mode - Channel B). 2. Press the * key to cycle through the screens until the Peak Tracking parameter appears.

  • Page 68: Checking The Fuses

    Disclaimers SpectraSensors accepts no responsibility for consequential damages arising from the use of this equipment. Liability is limited to replacement and/or repair of defective components. This manual contains information protected by copyright. No part of this guide may be photocopied or reproduced in any form without prior written consent from SpectraSensors.
  • Page 69 Troubleshooting purpose, shall apply to the goods or services hereunder, other than the repair and replacement warranty above. Seller shall in no event be liable to Buyer or any third party for any damage, injury or loss, including loss of use or any direct or indirect incidental or consequential damages of any kind.

  • Page 70: Table A-2 Potential Instrument Problems And Solutions

    Perhaps the existing tubing needs to be replaced with stainless steel flexible tubing. Capture diagnostic data and send the file to SpectraSensors (see “To read diagnostic data with HyperTermi- nal” on page 4-4). Possible alignment problem. Contact a factory sales representative for service information.
  • Page 71 Return to Mode 1 by press- ing the # key followed by the 1 key and see if the fault has changed. Capture diagnostic data and send the file to SpectraSensors (see “To read diagnostic data with HyperTermi- nal” on page 4-4). –...
  • Page 72 Reset the peak tracking (see “Peak Tracking Reset Procedure” on page A-5). Capture diagnostic data and send the file to SpectraSensors (see “To read diagnostic data with HyperTermi- nal” on page 4-4). P/T Fail Check that the actual pressure in the measurement cell is within specification (see Table B–1 on page B–1 or...
  • Page 73 Match Specific Standard(s)” on page 3-12. Capture diagnostic data and send the file to SpectraSensors (see “To read diagnostic data with HyperTermi- nal” on page 4-4). Reading seems to always be high by a See “Adjusting Analyzer Reading to fixed percentage Match Specific Standard(s)”...
  • Page 74 Check for contamination in the sample system, especially if the readings are much higher than expected. Capture diagnostic data and send the file to SpectraSensors (see “To read diagnostic data with HyperTermi- nal” on page 4-4). Gas concentration is greater than or Reading goes to full scale equal to full scale value.

  • Page 75: Appendix B: Specifications

    Appendix B: Specifications Table B–1 SS1000 moisture in natural gas analyzer specifications. Performance 0.5–20 lbs/MMSCF (10–422 ppmv) Concentration (H i l i ± ± Display updates every second Response time Application Data Environmental Temperature Range -4 to 122 °F (-20 to 50 °C) Standard 14 to 140 °F (-10 to 60 °C) Optional...

  • Page 76: Table B-2 Ss1000 Carbon Dioxide In Natural Gas Analyzer Specifications

    SS1000 Operator’s Manual Table B–2 SS1000 carbon dioxide in natural gas analyzer specifications. Performance 0–10% Concentration (CO i l i ± Display updates every second Response time Application Data Environmental Temperature Range -4 to 122 °F (-20 to 50 °C) Standard 14 to 140 °F (-10 to 60 °C) Optional...
  • Page 77 Specifications – Tel: +44 (0)1943 878877 Email: info@ima.co.uk Web: www.ima.co.uk UK Distibution by IMA Ltd...
  • Page 78 SS1000 Operator’s Manual FU S E (F 2) Figure B–2 Fuse location on DC to DC converter. – Tel: +44 (0)1943 878877 Email: info@ima.co.uk Web: www.ima.co.uk UK Distibution by IMA Ltd...

  • Page 79: Spare Parts

    Specifications Spare Parts Below is a list of spare parts for the SS1000 Operator’s Manual analyzer with recommended quantities for 2 years of operation. Due to a policy of continuous improvement, parts and part numbers may change without notice. Not all parts listed are included on every analyzer.
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  • Page 81: Index

    NDEX Absorption 1–4, 1–5 Gas sampling line A–2 Absorption coefficient 1–5 Gas standard 3–15 Absorption profile 1–5 Hardware 2–1 Absorption spectrometer 1–4 HyperTerminal 4–1 Absorption spectroscopy 1–4 Import stored data into spreadsheet 4–5 Accessories. See Options. Incident intensity 1–5 Acetone A–2 Initialization period 3–1 Acetone-impenetrable gloves A–3, A–4 Installation 2–1...
  • Page 82 SS1000 Operator’s Manual Output Signal Temperature Unit 3–9, 3–10, Serial output 2–5 4–17 Parameters User Analyzer ID 3–11, 4–17 Calibration User Component ID 3–12, 4–17 C0 4–17 User Sample ID 3–12, 4–17 C1 4–17 Password 3–6, 3–14, 4–13, 4–16, 4–18, C2 4–17...
  • Page 83 Tel: +44 (0)1943 878877 Email: info@ima.co.uk Web: www.ima.co.uk UK Distibution by IMA Ltd...

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