Thermo Scientific Orion Star User Manual

Thermo Scientific Orion Star User Manual

Designed for electrochemistry measurements in the field or in the laboratory
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Orion Star
Star Plus Meter
User Guide
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Summary of Contents for Thermo Scientific Orion Star

  • Page 1 Orion Star ™ Star Plus Meter User Guide • English • Español • Français • Deutsch • Italiano...
  • Page 2 FAST QC, GAP, GLPcal, GLPcheck, GLPdoc, ISEasy, KAP, LabConnect, LogR, Low Maintenance Triode, Minimum Stir Requirement, MSR, NISS, One-Touch, One-Touch Calibration, One-Touch Measurement, Optimum Results, Orion Star, Pentrode, pHuture MMS, pHuture Pentrode, pHuture Quatrode, pHuture Triode, Quatrode, QuiKcheK, rf link, ROSS Resolution, SAOB, SMART AVERAGING, Smart CheK, SMART STABILITY, Stacked, Star Navigator 21, Stat Face, The Enhanced Lab, ThermaSense, Triode, TRIUMpH, Unbreakable pH, Universal Access are trademarks of Thermo Fisher.
  • Page 3: Table Of Contents

    Dissolved Oxygen Temperature Display and Calibration . . . . . . . . . . . . . . . . . . . .EN-29 Thermo Scientific Orion Star...
  • Page 4 ISE Setup Menu Features . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .EN-68 Thermo Scientific Orion Star...
  • Page 5 . Built to meet the demands of busy, multiple user laboratory or plant environments, all Orion Star and Star Plus series meters are microprocessor controlled, which aids in the delivery of accurate and precise measurements . The waterproof portable meters can even withstand submersion for short periods of time .
  • Page 6: Chapter I Introduction

    Meter Features To better meet the needs of users in environmental protection and control, food and beverage, pharmaceutical and consumer product laboratories, the Orion Star and Star Plus series meters include these key features: Password Protected Methods – The meter will save up to ten custom •...
  • Page 7: Chapter Ii Display

    Display Chapter II General Description Throughout a given process, the display on an Orion Star or Star Plus series meter provides temperature and calibration data . The temperature appears in the left, top corner of the display . The icon indicates that a calibration mode or calibration setup menu is active .
  • Page 8 Note: If a measurement line is not needed, press to move the arrow icon to the measurement line that is not needed and press until the measurement line is completely blank. EN-4 Thermo Scientific Orion Star and Star Plus Series Meter User Guide ™...
  • Page 9: Chapter Iii Keypad

    Chapter III General Description The keypad layout is the same for all Orion Star and Star Plus series meters . The portable and 2-Star benchtop meters have nine keys . The 3-Star, 4-Star and 5-Star benchtop meters have 10 keys due to the addition of the stir key –...
  • Page 10: Key Definitions

    If the arrow icon points to the Turns the stirrer on and off . top line and the displayed units are ISE, pressing the key will enter the ISE setup screen . EN-6 Thermo Scientific Orion Star and Star Plus Series Meter User Guide ™...
  • Page 11: Chapter Iv Preparation

    . Refer to the diagram in the Connecting the Electrodes section . Batteries can be installed in the benchtop Orion Star or Star Plus series meters, so the meter setup settings are protected if the meter is disconnected from the wall outlet or a brief power outage occurs .
  • Page 12: Installing The Batteries

    Preparation nstalling the Batteries Orion Star and Star Plus series meters use four AA alkaline batteries . Do not use lithium or rechargeable batteries . Improper installation of non-alkaline batteries could create a hazard . Note: For benchtop meters, the installation of batteries is not required if the unit will always be connected to a power source via the universal power supply.
  • Page 13: Connecting The Electrodes

    9 pin AUTO-STIR probe pH, ORP miniDIN, or ISE Portable Meter Electrode Connections 8 pin miniDIN, RS232 Cond or ATC BNC, 9 pin miniDIN, pH, ORP or ISE Thermo Scientific Orion Star and Star Plus Series Meter User Guide EN-9 ™...
  • Page 14: Turning On The Instrument

    . Immediately remove any spilled substance from the meter using the proper cleaning procedure for the type of spill . EN-10 Thermo Scientific Orion Star and Star Plus Series Meter User Guide ™...
  • Page 15: Chapter V Meter Setup

    8 . Repeat steps 2 through 7 to program a new setup option or press to exit the setup menu and return to the measurement mode . Note: Refer to Appendix A for a description of the special setup menu features. Thermo Scientific Orion Star and Star Plus Series Meter User Guide EN-11 ™...
  • Page 16: Setup Menu Table

    Meter Setup Setup Menu Table – The following table is for the complete line of Orion Star and Star Plus meters. Meters may not include all of the options listed in this table. Top Line Middle Line Bottom Line Setup Menu Description (default setting, method specific) pH measurement resolution (0.01, yes)
  • Page 17 ISE calibration points (100, no) Conductivity calibration points (3, no) AUt0 C0nd 0, 1, 2, 3 AUt0 n0SA 0 to 47 Number of sample beakers (1, no) Thermo Scientific Orion Star and Star Plus Series Meter User Guide EN-13 ™...
  • Page 18: General Menu Settings

    . 8 . Repeat steps 3 through 7 to change another general setting or press return to the measurement mode . EN-14 Thermo Scientific Orion Star and Star Plus Series Meter User Guide ™...
  • Page 19: Time And Date Settings

    . 8 . Repeat steps 3 through 7 to change another time and date setting or press to return to the measurement mode . Thermo Scientific Orion Star and Star Plus Series Meter User Guide EN-15...
  • Page 20: Auto-Read ™ , Continuous Or Timed Measurement Settings

    . 8 . Repeat steps 3 through 7 to change another measurement setting or press to return to the measurement mode . EN-16 Thermo Scientific Orion Star and Star Plus Series Meter User Guide ™...
  • Page 21: Selecting The Measurement Parameter

    Note: If a measurement line is not needed, press to move the arrow icon to the measurement line that is not needed and press until the measurement line is completely blank. Thermo Scientific Orion Star and Star Plus Series Meter User Guide EN-17 ™...
  • Page 22: Method Setup

    . Press to select a new method number . c . Press to save the method number and press to return to the measurement mode . EN-18 Thermo Scientific Orion Star and Star Plus Series Meter User Guide ™...
  • Page 23: Ph Technique

    . 8 . Repeat steps 3 through 7 to change another pH setting or press to return to the measurement mode . Thermo Scientific Orion Star and Star Plus Series Meter User Guide EN-19 ™...
  • Page 24: Ph Calibration

    . b . For a two or more point calibration, the meter will automatically proceed to the measurement mode after the slope is displayed . EN-20 Thermo Scientific Orion Star and Star Plus Series Meter User Guide ™...
  • Page 25: Ph Measurement

    4 . Once all of the samples have been measured, rinse the electrode with distilled or deionized water and blot it dry . Consult the electrode user guide for proper storage techniques . Thermo Scientific Orion Star and Star Plus Series Meter User Guide EN-21...
  • Page 26: Ph Temperature Display And Calibration

    3 . When the reading stabilizes, the arrow icon and the first digit will flash . Enter the temperature by pressing to adjust each digit and to move to the next digit . 4 . Press to save and end the calibration . EN-22 Thermo Scientific Orion Star and Star Plus Series Meter User Guide ™...
  • Page 27: Relative Mv And Orp Calibration

    5 . Press to save and end the calibration . The millivolt offset will be displayed and the meter will automatically proceed to the measurement mode . Thermo Scientific Orion Star and Star Plus Series Meter User Guide EN-23 ™...
  • Page 28: Mv, Relative Mv And Orp Measurement

    4 . Once all of the samples have been measured, rinse the electrode with distilled or deionized water and blot it dry . Consult the electrode user guide for proper storage techniques . EN-24 Thermo Scientific Orion Star and Star Plus Series Meter User Guide ™...
  • Page 29: Dissolved Oxygen Technique

    . 8 . Repeat steps 3 through 7 to change another dissolved oxygen setting or press to return to the measurement mode . Thermo Scientific Orion Star and Star Plus Series Meter User Guide EN-25...
  • Page 30: Dissolved Oxygen Calibration

    – A manual calibration is performed using a water sample with a known concentration of dissolved oxygen . This method can be used to calibrate the dissolved oxygen probe to the value achieved by a Winkler titration . EN-26 Thermo Scientific Orion Star and Star Plus Series Meter User Guide ™...
  • Page 31 . d . If a zero point calibration is performed, the meter will display 0 .00 and automatically return to the measurement mode . Thermo Scientific Orion Star and Star Plus Series Meter User Guide EN-27...
  • Page 32: Dissolved Oxygen Measurement

    . Press again to turn off the stirrer before removing the probe and stirrer from the sample . EN-28 Thermo Scientific Orion Star and Star Plus Series Meter User Guide ™...
  • Page 33: Dissolved Oxygen Temperature Display And Calibration

    (% saturation), dissolved oxygen (mg/L), barometric pressure (no icon), sample temperature (no icon), electrolyte solution/membrane temperature (no icon, after number) or a blank line . Thermo Scientific Orion Star and Star Plus Series Meter User Guide EN-29 ™...
  • Page 34 3 . When the reading stabilizes, the arrow icon and the first digit will flash . Enter the temperature by pressing to adjust each digit and to move to the next digit . 4 . Press to save and end the calibration . EN-30 Thermo Scientific Orion Star and Star Plus Series Meter User Guide ™...
  • Page 35: Rdo Cap Overview

    5 . Press until is displayed on the bottom line . 6 . Press to print the RDO cap information . Press to return to the measurement mode . Thermo Scientific Orion Star and Star Plus Series Meter User Guide EN-31 ™...
  • Page 36: Rdo Optical Dissolved Oxygen Setup Menu

    . 8 . Repeat steps 3 through 7 to change another dissolved oxygen setting or press to return to the measurement mode . EN-32 Thermo Scientific Orion Star and Star Plus Series Meter User Guide ™...
  • Page 37: Setup Menu For Rdo Optical Dissolved Oxygen Sensor

    RDO sensor calibration information, for the RDO sensor factory calibration information, for the RDO sensor slope information, the RDO method information and for the general RDO sensor information . Thermo Scientific Orion Star and Star Plus Series Meter User Guide EN-33 ™...
  • Page 38 1210178953 (05-07-2008 16:49:13) expiration 1241736553 (05-07-2009 22:49:13) probe_mfg_time 1208440800 (04-17-2008 14:00:00) write_count pass_count expire 0x01 days_left 364.3 probe_reading 149.529243 temp_reading 24.942651 state general_event 0x00 internal_event 0x00 internal_state internal_retry 0x00 EN-34 Thermo Scientific Orion Star and Star Plus Series Meter User Guide ™...
  • Page 39: Rdo Optical Dissolved Oxygen Calibration

    10% saturation or 1 mg/L . 2 . Allow the RDO sensor and calibration standard (water saturated air, air saturated water, Winkler standard or oxygen-free solution) to reach equilibrium . Thermo Scientific Orion Star and Star Plus Series Meter User Guide EN-35...
  • Page 40 . d . If a zero point calibration is performed, the meter will display 0 .00 and automatically return to the measurement mode . EN-36 Thermo Scientific Orion Star and Star Plus Series Meter User Guide ™...
  • Page 41: Rdo Optical Dissolved Oxygen Measurement

    4 . Once all of the samples have been measured, rinse the RDO sensor with distilled or deionized water and blot it dry . Consult the RDO sensor user guide for proper storage techniques . Thermo Scientific Orion Star and Star Plus Series Meter User Guide EN-37...
  • Page 42: Rdo Optical Dissolved Oxygen Temperature Display And Calibration

    3 . When the reading stabilizes, the arrow icon and the first digit will flash . Enter the temperature by pressing to adjust each digit and to move to the next digit . 4 . Press to save and end the calibration . EN-38 Thermo Scientific Orion Star and Star Plus Series Meter User Guide ™...
  • Page 43: Conductivity Technique

    . 8 . Repeat steps 3 through 7 to change another conductivity setting or press return to the measurement mode . Thermo Scientific Orion Star and Star Plus Series Meter User Guide EN-39...
  • Page 44: Conductivity Calibration

    . Once the value is set, press until the decimal point is in the correct location . EN-40 Thermo Scientific Orion Star and Star Plus Series Meter User Guide ™...
  • Page 45: Conductivity Measurement

    . Press again to turn off the stirrer before removing the probe and stirrer from the sample . Thermo Scientific Orion Star and Star Plus Series Meter User Guide EN-41 ™...
  • Page 46: Conductivity Temperature Display And Calibration

    3 . When the reading stabilizes, the arrow icon and the first digit will flash . Enter the temperature by pressing to adjust each digit and to move to the next digit . 4 . Press to save and end the calibration . EN-42 Thermo Scientific Orion Star and Star Plus Series Meter User Guide ™...
  • Page 47 . 8 . Repeat steps 3 through 7 to change another ISE setting or press to return to the measurement mode . Thermo Scientific Orion Star and Star Plus Series Meter User Guide EN-43 ™...
  • Page 48: Chapter Xi Ise Technique

    . b . For a two or more point calibration, the meter will automatically proceed to the measurement mode after the slope is displayed . EN-44 Thermo Scientific Orion Star and Star Plus Series Meter User Guide ™...
  • Page 49: Ise Measurement

    4 . Once all of the samples have been measured, rinse the electrode with distilled or deionized water and blot it dry . Consult the electrode user guide for proper storage techniques . Thermo Scientific Orion Star and Star Plus Series Meter User Guide EN-45...
  • Page 50: Ise Temperature Display And Calibration

    3 . When the reading stabilizes, the arrow icon and the first digit will flash . Enter the temperature by pressing to adjust each digit and to move to the next digit . 4 . Press to save and end the calibration . EN-46 Thermo Scientific Orion Star and Star Plus Series Meter User Guide ™...
  • Page 51: Chapter Xii Data Archiving And Retrieval

    . The 5-Star Plus meters have a 500 point datalog . The 2-Star meter has a 50 point datalog and all Orion Star meters have a 200 point datalog . The Star Plus meter printouts have been enhanced to include additional information .
  • Page 52: Datalog Deletion Setting

    . Note: If the datalog is not required, set the datalog deletion setting to prevent the error 038 (datalog full) message. EN-48 Thermo Scientific Orion Star and Star Plus Series Meter User Guide ™...
  • Page 53: Viewing And Printing The Datalog And Calibration Log

    The 3-Star, 4-Star and 5-Star Plus meters have been enhanced to include a calibration log view feature in addition to the datalog view, datalog print and calibration log print features . The Orion Star meters include the datalog view, datalog print and calibration log print features .
  • Page 54 . To interfacing the meter with a computer: The Orion Star and Star Plus meters can send measurement and calibration data to a computer in a comma delimited format that is easy to parse in computer programs like Excel .
  • Page 55: Declaration Of Conformity

    4-Star Plus RDO Optical DO/pH Meter 3-Star Plus RDO Optical DO Meter Equipment Class: Measurement, control and laboratory Benchtop models are EMC Class A Portable models are EMC Class D Thermo Scientific Orion Star and Star Plus Series Meter User Guide EN-51 ™...
  • Page 56: Weee Compliance

    Member State and this product should be disposed of or recycled through them . Further information on compliance with these Directives, the recyclers in your country, and information on Thermo Scientific Orion products which may assist the detection of substances subject to the RoHS Directive are available at www .thermo .com/WEEERoHS .
  • Page 57: Chapter Xiv Troubleshooting

    BNC shorting cap is firmly attached to the BNC meter input. This error code usually occurs if the BNC shorting cap is missing or not fully connected to the BNC meter input during the meter self test. Thermo Scientific Orion Star and Star Plus Series Meter User Guide EN-53...
  • Page 58: Meter Error Codes

    The autosampler is unable to receive a signal from the meter. Review the Signal Error meter setup parameters and make sure that the baud rate of the meter is set to 1200. EN-54 Thermo Scientific Orion Star and Star Plus Series Meter User Guide ™...
  • Page 59 Verify that the RDO cap on the RDO sensor was properly installed, not Sensor Failure expired and not tampered with. Connect another, known working RDO sensor to the meter. Thermo Scientific Orion Star and Star Plus Series Meter User Guide EN-55 ™...
  • Page 60: General Troubleshooting

    . Problem: I cannot tell if I have the Star Plus meter or the Orion Star meter . Solution: When the meter is powered on, the Star Plus meters with enhanced...
  • Page 61 Verify that the cell constant is correct for the conductivity probe that is connected to the meter . Verify that the cell type selected in the setup menu is set to Std . Thermo Scientific Orion Star and Star Plus Series Meter User Guide EN-57...
  • Page 62 United States call 978 .232 .6000 or fax 978 .232 .6031 . In Europe, the Middle East and Africa, contact your local authorized dealer . For the most current contact information, visit www .thermo .com/contactwater . For the latest application and technical resources for Thermo Scientific Orion products, visit www .thermo .com/waterapps . Warranty For the most current warranty information, visit www .thermo .com/water .
  • Page 63: Chapter Xv Meter Specifications

    Enclosure (designed to meet) IP67 (portable meter) IP54 (benchtop meter) * TÜV and UL certifications are pending for all Star Plus RDO optical dissolved oxygen meters . ® Thermo Scientific Orion Star and Star Plus Series Meter User Guide EN-59 ™...
  • Page 64 Indoor use only Meter Parameter Specifications The following meter parameter specifications are for the complete line of Orion Star and Star Plus series meters . Single parameter, dual parameter and some multi- parameter meters will not include all of the parameters listed in this section .
  • Page 65 0 to 45 ppt Barometric Pressure 450 to 850 mm Hg Calibration Types Water saturated air, air saturated water, manual (Winkler), zero point Probe Type RDO optical Thermo Scientific Orion Star and Star Plus Series Meter User Guide EN-61 ™...
  • Page 66 The 4-Star and 5-Star RDO meters will have the standard temperature specifications when used with an electrode other than the RDO sensor. Note: Specifications are subject to change without notice. EN-62 Thermo Scientific Orion Star and Star Plus Series Meter User Guide ™...
  • Page 67: Ordering Information

    ® 1213310 4-Star Plus RDO optical DO/pH portable meter with batteries and user guide 1213320 5-Star Plus RDO optical DO/pH/conductivity portable meter with batteries and user guide Thermo Scientific Orion Star and Star Plus Series Meter User Guide EN-63 ™...
  • Page 68 DuraProbe conductivity probe with 1 µS/cm to 200 mS/cm range and 3 meter cable 013016MD Conductivity probe with 0.01 µS/cm to 300 µS/cm range and 1.5 meter cable Visit www.thermo.com/water for additional meter kits, accessories, electrodes and solutions. EN-64 Thermo Scientific Orion Star and Star Plus Series Meter User Guide ™...
  • Page 69: Appendix A Meter Setup Menu Features

    Setup Menu Features Automatic buffer recognition The Orion Star and Star Plus pH meters are capable of automatically recognizing pH 1 .68, 4 .01, 6 .86, 7 .00, 9 .18, 10 .01 and 12 .46 buffers during a pH calibration . During...
  • Page 70: Conductivity Setup Menu Features

    5 °C, 10 °C, 15 °C, 20 °C or 25 °C (Orion Star meters have a reference temperature of 15 °C, 20 °C or 25 °C only) . The temperature compensation can be set as linear for most aqueous samples, non-linear for ultra pure and low ionic strength samples or off for non-temperature compensated conductivity measurements .
  • Page 71 5.64 Total Dissolved Solids (TDS) The Orion Star and Star Plus conductivity meters measure TDS as the total amount of dissolved inorganics in a solution . The dissolved inorganics carry a current that is measured by the conductivity probe . Since there is a direct relationship between conductivity and TDS, conductivity readings are used to estimate the presence of inorganics .
  • Page 72: Ise Setup Menu Features

    SE Setup Menu Features Concentration Range The Orion Star and Star Plus ISE meters can be set for a high or low ISE concentration range that is used to determine the calibration stability criteria . If a high ISE concentration range is selected, the meter will perform a normal calibration with no delay in displaying the calibration standard value .
  • Page 73 Environmental Instruments Water Analysis Instruments North America 166 Cummings Center Beverly, MA 01915 USA Toll Free: 1-800-225-1480 Tel: 1-978-232-6000 Dom. Fax: 1-978-232-6015 Int’l Fax: 978-232-6031 Europe P.O. Box 254, 3860 AG Nijkerk Wallerstraat 125K, 3862 BN Nijkerk, Netherlands Tel: (31) 033-2463887 Fax: (31) 033-2460832 Asia Pacific Blk 55, Ayer Rajah Crescent...

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