1. Manuals
  2. Brands
  3. Agilent Technologies Manuals
  4. Thermostat
  5. 1260 Infinity II
  6. User manual

Agilent Technologies 1260 Infinity II User Manual

Gpc/sec column thermostat
Hide thumbs Also See for 1260 Infinity II:
Table of Contents

Advertisement

Quick Links

Download this manual
Agilent 1260 Infinity II
GPC/SEC Column Thermostat
User Manual

Advertisement

Table of Contents
loading

Related Manuals for Agilent Technologies 1260 Infinity II

Summary of Contents for Agilent Technologies 1260 Infinity II

  • Page 1 Agilent 1260 Infinity II GPC/SEC Column Thermostat User Manual...
  • Page 2 Copyright maximum extent permitted by procedure, practice, or the like that, if applicable law, Agilent disclaims all © Agilent Technologies, Inc. 2023 not correctly performed or adhered to, warranties, either express or implied, No part of this manual may be...
  • Page 3 In this Guide…. This manual covers the Agilent 1260 Infinity II GPC/SEC Column Thermostat (G7886A). This manual is intended for laboratory technicians who are responsible for control and day-to-day maintenance of the Column Thermostat. It is assumed that the user of this manual has basic knowledge of how to use general purpose GPC/SEC laboratory equipment and is familiar with standard laboratory terminology.

  • Page 4: Table Of Contents

    Setup Waste Connection Start the Column Thermostat Maintenance General Cleaning Check for Leaks Replace Fuses Service Parts for Maintenance Columns Thermostat Appendix Storage, Packaging and Recycling Waste Electrical and Electronic Equipment (WEEE) Directive Agilent Technologies on Internet GPC/SEC Column Thermostat User Manual...

  • Page 5: Introduction

    Introduction Introduction Safety Instructions General Safety Site Requirements Power Considerations System Operation and Maintenance Solvent Information Handling Leak and Waste Applications: Quality Control Safety Symbols About the Column Thermostat Identification of Parts Instrument – Front Instrument – Rear Options Cooling Option Specifications This chapter provides an overview of the most important functions and options of the Column Thermostat.

  • Page 6: Safety Instructions

    Introduction Safety Instructions In this manual, Warning / Caution messages are always indicated using the following conventions: A warning alerts you to situations that could cause physical injury or death. WARNING Do not proceed beyond a warning until you have fully understood and met the indicated conditions.
  • Page 7 Introduction Adhere to quality control procedures and the following equipment guidelines when using the system: General Safety The system is intended to be used in a regulated laboratory environment with WARNING • trained operators following good laboratory practices. Use this system ONLY for its intended use. Use of the system for any other •...
  • Page 8 Introduction Site Requirements Pay attention to the weight of the Column Thermostat. The instrument WARNING • weighs 17 kg (37.5 lbs) or 12.5 kg (28 lbs), without cooling option. Use proper lifting techniques to avoid potential injuries. Ensure that you can handle the weight of the load.
  • Page 9 Introduction Bench Space The module dimensions and weight (see Table “Physical Specifications” on page 18) allow you to place the module on almost any desk or laboratory bench. It needs additional 10 cm (3.9 inches) space on right-hand side and approximately 6 cm (2.4 inches) in the rear for air circulation and electric connections.
  • Page 10 Introduction System Operation and Maintenance WARNING Temperatures inside the Column Thermostat may be high. Touching the • panels inside the Column Thermostat may cause burns. Make sure the actual temperature inside the Column Thermostat has decreased to a safe value of, for example, 25°C before you open the front door to prevent injuries. Use of biological materials, viral samples and needles may carry a significant •...
  • Page 11 Introduction Solvent Information WARNING The solvents used may be flammable and toxic and may carry a significant • health risk. Therefore, the room in which the system is installed should be well ventilated to prevent that solvent vapors cause a fire. Do not allow solvents to accumulate in the system.
  • Page 12 Introduction Handling Leak and Waste Liquids associated with this instrument may be classified as carcinogenic, WARNING biohazardous, flammable, or radioactive. Dispose of waste (samples, solvents, device) in accordance with a regulated waste disposal program. Follow a regulated, approved waste disposal program and never dispose of solvents through the municipal sewage system.

  • Page 13: Safety Symbols

    Introduction Safety Symbols The following safety symbols are attached to the cover on the back of the instrument. They are intended to alert you to the following safety information. Table 1 Safety Symbols Symbol Description The apparatus is marked with this symbol when the user should refer to the instruction manual in order to protect risk of harm to the operator and to protect the apparatus against damage.

  • Page 14: About The Column Thermostat

    Introduction About the Column Thermostat Almost every parameter defining a chromatographic separation is temperature dependent. For that reason, the Column Thermostat offers a stable and precise temperature control. The Column Thermostat optimizes your GPC/SEC assay by using forced air. The Column Thermostat features: quick heating ...

  • Page 15: Identification Of Parts

    Introduction Identification of Parts The temperature inside the Column Thermostat may be hot! WARNING Make sure the temperature in the Column Thermostat has decreased to a safe value before opening the front door. Instrument – Front Figure 1 Column Thermostat – front (multiple column setup) Status LED Fans;...
  • Page 16 Introduction Instrument – Rear Figure 2 Column Thermostat – rear Ethernet OUT (serial) (not used) IN (serial) (not used) I/O connector Ventilation holes; do not obstruct! Fuse box, power connector, voltage selector, ON/OFF switch: “I” indicates Power ON, “O” indicates Power OFF Any other instruments connected to this instrument must be approved to a WARNING suitable safety standard and must include reinforced insulation from the...

  • Page 17: Options

    Introduction Options The following options are available for the Column Thermostat: Cooling Option Temperature range from 5°C up to 90°C.  Without cooling option Temperature range from ambient +10°C up to 90°C.  GPC/SEC Column Thermostat User Manual...

  • Page 18: Specifications

    Introduction Specifications Table 2 Physical Specifications Type Specification Comments Dimensions (height × 600 x 170 x 345 mm width × depth) Weight 17 kg / 12.5 kg without cool option (37.5 lbs / 28 lbs) Operating altitude up to 2000 m Operating temperature 5 - 40°C Operating humidity...
  • Page 19 Introduction Table 3 Performance Specifications Type Specifications Temperature range With cool option: 5°C - 90°C, with 1°C increments 5°C - 75°C Without cool option: Ambient +10°C - 90°C, with 1°C increments Note that ambient temperature and humidity influence the NOTE lower temperature limit of the Column Thermostat.

  • Page 20: Using The Column Thermostat

    Using the Column Thermostat Using the Column Thermostat Setup Mains Power Connection Setup Solvent Connections Setup Nut and Ferrule Connections Setup Waste Connection Start the Column Thermostat This chapter explains the status of the Column Thermostat when the device is initialized.

  • Page 21: Setup Mains Power Connection

    Using the Column Thermostat Setup Mains Power Connection Before plugging in the power cable: WARNING Check the voltage setting of the Column Thermostat! Power supply and protective earth WARNING The system must be connected to a suitable mains power supply with a correctly installed protective earth conductor.

  • Page 22: Setup Solvent Connections

    Using the Column Thermostat Setup Solvent Connections Make the required solvent connections. The solvent lines can be lead to the outside of the instrument, between the door and door sealing. Setup Nut and Ferrule Connections Connect tubing that transports acidic solvents always with the provided tubing CAUTION fixators! Only use the provided nuts and ferrules;...
  • Page 23 Using the Column Thermostat If L is too short, this may result in Leakage  Dead volume at the end of the ferrule (a ‘mixing chamber’).  Every ferrule type needs an appropriate length of tubing to connect it to the column, depending on the depth of the connection port.
  • Page 24 Using the Column Thermostat Use a column to gently tighten the fitting which forces the ferrule to seat onto the tubing or capillary. Don't overtighten. Overtightening will shorten the lifetime of the fitting. NOTE Loosen the nut and verify that the ferrule is correctly positioned on the tubing or capillary.

  • Page 25: Setup Waste Connection

    Using the Column Thermostat Setup Waste Connection Make a connection from the Column Thermostat leakage drain to a waste bin. CAUTION Figure 4 Column Thermostat – front (single column setup) Column Leakage Drain GPC/SEC Column Thermostat User Manual...

  • Page 26: Start The Column Thermostat

    Using the Column Thermostat Start the Column Thermostat The following properties can be found when initializing the Column Thermostat: Instrument is controlled remotely by the software,  the control LED: on,  heating/cooling: off,  Status LED: Green = normal operation ...

  • Page 27: Maintenance

    Maintenance Maintenance General Cleaning Check for Leaks Replace Fuses Service This chapter describes the maintenance of the Column Thermostat. GPC/SEC Column Thermostat User Manual...
  • Page 28 Maintenance Note that this section only describes basic maintenance procedures. Do not attempt to service the Column Thermostat beyond the scope of maintenance described in this manual. The temperature inside the Column Thermostat may be high. WARNING Make sure the actual temperature inside the Column Thermostat has decreased to a safe value of e.g.

  • Page 29: General Cleaning

    Maintenance General Cleaning Clean the outside and compartment of the Column Thermostat using a dry cloth or damp cloth with isopropyl alcohol or water. Make sure that no liquid enters the inside of the Column Thermostat. GPC/SEC Column Thermostat User Manual...

  • Page 30: Check For Leaks

    Maintenance Check for Leaks Regularly check connections for signs of leakage. If leakages are visible, a connection may have come loose. For more information about the setup of nut and ferule connections, see section “Setup Nut and Ferrule Connections” on page 22. GPC/SEC Column Thermostat User Manual...

  • Page 31: Replace Fuses

    Maintenance Replace Fuses If you need to replace fuses, disconnect the instrument from the power WARNING source by removing the mains power cord. Make sure that you install fuses of the same type and rating (for details, refer to section “Physical Specifications”...

  • Page 32: Service

    Maintenance Service The Column Thermostat must be serviced in case: It has been subjected to severe shock(s).  Solvent has been spilled into the instrument.  It does not operate as specified.  It shows a change in performance.  Do not attempt to service the Column Thermostat beyond the scope of CAUTION maintenance described in this manual.

  • Page 33: Parts For Maintenance

    Parts for Maintenance Parts for Maintenance Columns Thermostat This chapter provides information on parts material required for the Column Thermostat. GPC/SEC Column Thermostat User Manual...

  • Page 34: Columns Thermostat

    Parts for Maintenance Columns Thermostat The following spare parts are available for the Column Thermostat: Table 5 Options Description 1400-3863 Column clip large 1400-3864 Column clip medium 1400-3864 Column clip micro 2110-1674 Fuse 5AT, IEC 60127-2, UL/CSA approved GPC/SEC Column Thermostat User Manual...

  • Page 35: Appendix

    Appendix Appendix Storage, Packaging and Recycling Decontamination General Instructions for Disposal Hazardous Substances Waste Electrical and Electronic Equipment (WEEE) Directive Agilent Technologies on Internet This chapter provides additional information on storage, legal, and web. GPC/SEC Column Thermostat User Manual...

  • Page 36: Storage, Packaging And Recycling

    Appendix Storage, Packaging and Recycling If the Column Thermostat needs to be stored, or if it must be shipped to a different location, proceed as follows: Switch off the Column Thermostat when no measurement is running and it is set to ambient temperature. Disconnect the column from the tubing.

  • Page 37: Waste Electrical And Electronic Equipment (Weee) Directive

    Appendix Waste Electrical and Electronic Equipment (WEEE) Directive This product complies with the European WEEE Directive marking requirements. The affixed label indicates that you must not discard this electrical/electronic product in domestic household waste. Do not dispose of in domestic household waste. NOTE To return unwanted products, contact your local Agilent office, or see http://www.agilent.com for more...

  • Page 38: Agilent Technologies On Internet

    Appendix Agilent Technologies on Internet For the latest information on products and services visit our worldwide web site on the Internet at: https://www.agilent.com GPC/SEC Column Thermostat User Manual...
  • Page 39 In This Book The manual describes the following: Product Description  Specifications  Start of the Column Thermostat  Maintenance Procedures  Spare Parts  www.agilent.com © Agilent Technologies, Inc. 2023 Edition 06/2023 D0029605 Rev. A...

Table of Contents