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Thermo Scientific Surveyor LC Pump Plus Manuals
Manuals and User Guides for Thermo Scientific Surveyor LC Pump Plus. We have
1
Thermo Scientific Surveyor LC Pump Plus manual available for free PDF download: Hardware Manual
Thermo Scientific Surveyor LC Pump Plus Hardware Manual (144 pages)
Brand:
Thermo Scientific
| Category:
Water Pump
| Size: 7 MB
Table of Contents
Table of Contents
11
Preface
15
Related Documentation
15
Safety and Special Notices
15
Good Laboratory Practices
16
Contacting Us
18
Chapter 1 Introduction
19
Functional Description
20
Vacuum Degasser Assembly
21
Solvent Proportioning Assembly
21
Pump Head Assemblies
21
Table
21
Purge Manifold Assembly
27
Pulse Dampening Assembly
28
Status Leds
29
Flow Control
30
Specifications
33
Chapter 2 Installation
35
Installation Checklist
36
Unpacking and Inspecting the Instrument
37
Placing the Pump on the Laboratory Benchtop
37
Connecting the Back Panel Cables
38
System Synchronization Cable
39
Ethernet Cable
40
Unit ID Setting
40
Connecting the Solvent Lines
40
Low-Pressure Solvent Reservoir Lines
41
High-Pressure Solvent Line between the Pump and the Autosampler
45
Powering on the LC Pump for the First Time
46
Preparing the LC Pump for Daily Operation
47
Calibrating the LC Pump
47
Chapter 3 Software Instrument Configuration
49
Adding the Pump to the Chromquest Instrument Configuration
49
Pump Configuration Options in the Chromquest Data System
50
Autosampler Input Signals in the Chromquest Data System
54
Adding the Pump to the Thermo Foundation Instrument Configuration
55
Pump Configuration Options in the Thermo Foundation Instrument
55
Configuration
55
Autosampler Input Signals in the Thermo Foundation Instrument Configuration
57
Chapter 4 Maintenance
59
Maintenance Schedule
60
Maintenance Page in the Chromquest Data System
61
Opening the Maintenance Page in the Chromquest Data System
61
Recording Maintenance in the Chromquest Data System
62
Setting the Pistons to the Maintenance Position from the Chromquest Data System
63
Maintenance Page in the Xcalibur Data System
63
Opening the Maintenance Page in the Xcalibur Data System
64
Recording Maintenance in the Xcalibur Data System
65
Data System
65
Rinsing the Pistons
66
Cleaning the Check Valves
68
Pumping Isopropyl Alcohol through the Check Valves
68
Sonicating the Check Valves
69
Maintaining the Pump Head Assemblies
72
Replacing the Piston Seals
73
Replacing the Wash Seals
80
Cleaning and Replacing a Piston
84
Cleaning and Replacing a
84
Replacing the Line Filter Frit
86
Replacing the Solvent Reservoir Filter
88
Purging Air from the Solvent Lines or the Pump Heads
89
Opening the Drain Valve
89
Using the Purge Feature
90
Replacing the Drain Valve Knob O-Ring
93
Replacing the Fuses
94
Figure
94
Chapter 5 Diagnostic Tests and Calibration Options
97
Flow Rate Accuracy Check
97
Pressure Pulsation Check
99
Checking the Pressure Pulsation of the LC Pump
99
Troubleshooting the Cause of Excessive Pressure Variation
100
Proportioning Accuracy Check
101
Proportioning Accuracy Test-Preparation
101
Proportioning Accuracy Test-Conditions
102
Proportioning Accuracy Test-Running
103
Analyzing the Test Results
104
Gradient Delay Volume Check
106
Calibration Options
108
Compressibility
108
Pressure Recorder Full Scale
110
Flow Rate Adjustment (Alpha)
111
Pressure Sensor Adjustment
111
Pressure Transducer Zero
111
Chapter 6 Troubleshooting
113
Troubleshooting Tips
114
General System Troubleshooting
114
LC Pump Troubleshooting Guide
116
Pump Pulsation
118
Normal Pressure Pulsation
118
Abnormal Pressure Pulsation
118
Baseline Noise at Low Pressures (under 40 Bar)
119
Insufficient Solvent Flow from the LC Pump Outlet
119
Pump Cavitation
119
Blocked Proportioning Valve
120
Blocked Check Valve
120
Irreproducible Retention Times
120
Chapter 7 Accessories and Replaceable Parts
121
Surveyor LC Pump Accessory Kit
122
Replacement Parts Required for Routine Maintenance
123
Nonconsumable Replacement Parts
124
Replacement Parts Required for Nonroutine Maintenance
125
Solvent Interconnect Kit
126
Other Parts and Assemblies
126
Appendix A Firmware
127
Copying the Firmware Files from the Chromquest CD
128
Updating the Ethernet Firmware for the LC Pump
129
Preparing the LC Pump to Download the Ethernet Firmware
129
Downloading the Communication Firmware Files
130
Returning the LC Pump to Normal Operation
132
Updating the CPU Firmware for the LC Pump
132
Preparing the LC Pump for a CPU Firmware Upgrade
133
Using the Flash ROM Update Utility to Update the CPU Firmware
135
Index
139
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