Metrohm 917 Coulometer Manuals

Manuals and User Guides for Metrohm 917 Coulometer. We have 4 Metrohm 917 Coulometer manuals available for free PDF download: Manual, Tutorial, Manual - Short Instructions

Metrohm 917 Coulometer Manual (338 pages)

Coulometer

Brand: Metrohm | Category: Laboratory Equipment | Size: 6 MB

Table of Contents
5
1 Introduction

15
- Instrument Description
  15
- Titration and Measuring Modes
  15
- Connectors
  16
- Intended Use
  16
- About the Documentation
  16
- Symbols and Conventions
  17
2 Safety Instructions

18
- General Notes on Safety
  18
- Electrical Safety
  18
- Tubing and Capillary Connections
  19
- Flammable Solvents and Chemicals
  19
- Recycling and Disposal
  20
3 Overview of the Instrument

21
- Front of the Instrument
  21
- Figure 1 Front
  21
- Rear of the Instrument
  22
- Figure 2 Rear
  22
4 Installation

23
5 Titrations

42
- Coulometric Water Content Determination According to Karl Fischer (KFC)
  42
- Bromine Index Determination (BRC)
  43
6 Operation

44
- Switching the Instrument on and off
  44
- Fundamentals of Operation
  45
- Touch-Sensitive Screen
  45
- Display Elements and Controls
  46
- Status Display
  47
- Entering Text and Numbers
  48
7 System Settings

50
- General System Settings
  50
- Selecting the Dialog Language
  50
- Setting the Date, Time and Local Time
  51
- System-Specific Dialog Options
  52
- User Administration
  55
- Editing the User Configuration
  57
- Creating an Identification Profile
  60
- Defining Login Options
  61
- Password Options
  63
- Modification Options
  65
- Reasons
  65
- Audit Trail
  66
- Measured Value Display
  68
- Acoustic Signals
  68
8 Reagents

69
- Editing Reagent Data
  69
- Reagent Monitoring
  70
9 Sensors

73
- Adding a New Sensor
  74
- Editing the Sensor Data
  74
- Monitoring the Working Life
  75
10 Device Manager

77
- Adding a New Device
  78
- Configuring the Instrument
  78
- Coulometer
  79
- E-Mail
  80
- PC/LIMS Report
  81
- Shared Memory
  82
- TCP/IP Settings
  84
- Metrohm Control Instruments
  85
- Properties - Measuring Input
  86
- Properties - MSB Connector
  87
- Properties - Peripheral Devices
  88
- Printer
  88
- PDF Settings
  90
- Network Printer
  91
- More Options
  92
- Balance
  93
- USB/RS-232 Adapter
  94
- PC Keyboard
  96
- Barcode Reader
  98
11 File Manager

100
- Managing Files
  100
- Copying a File
  102
- Renaming a File
  102
- File Properties
  103
- External Storage Medium
  104
- Figure 16 Directory Structure on the External Storage Medium
  105
- Creating Backups / Restoring Data
  106
- Restoring Data
  106
12 GLP Manager

108
- Automatic System Test
  109
- Test Tools
  109
- GLP Tests for Measurement and Titration
  110
- Parameter Description
  111
- System Validation
  114
- Parameter Description
  115
- System Monitoring
  118
- Service Interval
  118
- Backup Interval
  118
13 Common Variables

120
14 Templates

126
- Sample Data
  126
- Sample Identification List
  127
- Sample Assignment Table
  128
- Custom Result Templates
  130
- Editing Result Templates
  131
- Input Lines
  134
- Editing the Input Signal
  135
- Output Lines
  136
- Editing the Output Signal
  138
- Report Header
  139
15 Methods

141
- Creating a New Method
  141
- Saving a Method
  142
- Loading a Method
  143
- Editing a Method
  144
- Inserting a Command
  145
- Method Options
  146
- Start Options
  147
- Stop Options
  148
- Sample Data
  149
- Method Properties
  152
- Note
  154
- Saving a Determination Automatically
  154
16 Electronic Signatures

157
- Signing Methods/Determinations Electronically
  157
- Deleting Electronic Signatures
  158
17 Control

159
18 Favorites

163
- Creating Favorites
  164
- Editing Favorites
  164
19 Sample Data

167
- Entering Sample Data in the Main Dialog
  167
- Requesting Sample Data at the Start of the Determination
  168
20 Sample Table

170
- General
  170
- Editing Sample Data
  173
- Properties
  175
21 Determination Run

178
22 Live Modifications

181
23 Results and more Determination Data

186
- More Determination Data
  187
- Details
  188
- Messages
  190
- Local Common Variables
  190
- Determination Properties
  191
- Loading a Determination
  193
- Determination List
  194
- Saving a Determination
  198
- Curves
  199
- Recalculation and Reevaluation
  201
24 Statistics

202
25 Result Table

207
- Properties
  208
- Saving the Result Table
  212
- Loading the Result Table
  212
26 Printing

213
- General Report Options
  215
- Settings of the Individual Reports
  216
- List of All Printable Reports
  217
27 Manual Control

221
- Opening and Closing the Manual Control
  222
- Measuring
  223
- Parameter Description
  224
- Dosing
  225
- Continuous Dosing
  226
- Dosing Fixed Volumes
  228
- Preparing
  229
- Emptying
  230
- Filling
  230
- Replacing Reagent
  230
- Stirring
  231
- Remote
  232
28 Parameter

234
- Coulometric Karl Fischer Titrations (KFC)
  234
- Control Parameters
  234
- Titration Parameters
  237
- Stop Conditions
  237
- Conditioning
  238
- Cell
  240
- Sensor
  241
- Stirrer
  242
- Bromine Index Determination (BRC)
  243
- Control Parameters
  243
- Titration Parameters
  246
- Stop Conditions
  247
- Conditioning
  247
- Cell
  249
- Sensor
  250
- Stirrer
  251
- Measurements (MEAS)
  252
- Measuring Parameters
  252
- Sensor
  254
- Stirrer
  256
- Evaluations (EVAL)
  257
- Fixed Endpoint Evaluation (EVAL FIX-EP)
  258
- Minimum and Maximum Evaluation (EVAL MIN/MAX)
  259
- Figure 17 Evaluation of Minimum and Maximum
  259
- Rate Evaluation (EVAL RATE)
  260
- Calculations
  261
- Calculations (CALC)
  261
- Calculations (CALC LIVE)
  267
- Formula Editor
  269
- Reports (REPORT)
  275
- General Report Options
  276
- Settings of the Individual Reports
  277
- List of Reports
  278
- Dosing and Liquid Handling
  280
- Preparing an Exchange or Dosing Unit (PREP)
  280
- Emptying a Dosing Unit (EMPTY)
  281
- Dosing a Specified Volume (ADD)
  282
- Liquid Handling (LQH)
  287
- Communication
  290
- Scanning Remote Lines (SCAN)
  290
- Setting Remote Lines (CTRL)
  291
- Scanning the RS-232 Interface (SCAN RS)
  293
- Defining RS-232 Commands (CONTROL RS)
  294
- Automation
  294
- Creating a Subsequence (SUBSEQ)
  294
- Miscellaneous Commands
  297
- Controlling a Stirrer (STIR)
  297
- Pausing the Method Run (WAIT)
  298
- Scan Data (REQUEST)
  299
- Defining an Acoustic Signal (BEEP)
  300
- Signing a Determination (SIGN)
  300
- Canceling the Method Run (END)
  300
29 Operation and Maintenance

301
- System Initialization
  301
- Maintenance
  302
30 Troubleshooting

303
- Editing Methods
  303
- Sample Table
  303
- Results/Statistics
  303
- Printing
  304
- Manual Control
  304
- Titration Stand with Pump
  305
- Coulometric Karl Fischer Titration
  305
31 Appendix

308
- Dosing Unit
  308
- Maximum Dosing and Filling Rate
  308
- Default Parameters for Preparing (PREP) and Emptying (EMPTY)
  308
- Exchange Unit
  309
- Maximum Dosing and Filling Rate
  309
- Default Parameters for Preparing (PREP)
  309
- Stirring Rate
  309
- Balance
  310
- Figure 18 Rotational Speed Depending on the Stirring Rate
  310
- Remote Interface
  311
- Pin Assignment of the Remote Interface
  311
- Figure 19 Connectors of the Remote Box
  311
- Figure 20 Pin Assignment of Remote Socket and Plug
  311
- Result Variables as Parameter Setting
  314
- Using Audittrailviewer
  315
- Installing Audittrailviewer
  315
- Opening the Audit Trail
  316
- Contents of the Audit Trail
  317
- Filtering the Audit Trail
  318
- Exporting the Audit Trail
  319
- Diagnosis
  319
- LCD Test
  320
- Formatting an External Storage Medium
  320
- Removing an External Storage Medium
  321
- Adjusting the Touch Screen
  321
- Testing the Touch Screen
  322
- Software Update
  323
- Files)
  323
- Service
  326
- Arithmetic Algorithms in the Coulometer
  326
32 Technical Specifications

329
- Touch Screen
  329
- Measuring Inputs
  330
- Generator Electrode
  330
- Indicator Electrode
  330
- Temperature Sensor
  330
- Determination Range
  331
- Resolution
  331
- Reproducibility
  331
- Internal Stirrer
  331
- Pump
  331
- Interfaces and Connectors
  332
- Power Supply
  332
- Declarations of Conformity
  332
- Ambient Temperature
  333
- Reference Conditions
  333
- Dimensions
  333
33 Accessories

334
Index

335

Metrohm 917 Coulometer Tutorial (67 pages)

Brand: Metrohm | Category: Laboratory Equipment | Size: 3 MB

Metrohm 917 Coulometer Manual - Short Instructions (45 pages)

Brand: Metrohm | Category: Measuring Instruments | Size: 1 MB

Table of Contents
5
1 About These Short Instructions

9
2 Introduction

10
- Instrument Description
  10
- Titration and Measuring Modes
  10
- Connectors
  11
- Intended Use
  11
- About the Documentation
  11
- Symbols and Conventions
  12
3 Safety Instructions

13
- General Notes on Safety
  13
- Electrical Safety
  13
- Tubing and Capillary Connections
  14
- Flammable Solvents and Chemicals
  14
- Recycling and Disposal
  15
4 Overview of the Instrument

16
- Front of the Instrument
  16
- Figure 1 Front
  16
- Rear of the Instrument
  17
- Figure 2 Rear
  17
5 Installation

18
6 Operation

37
- Switching the Instrument on and off
  37
- Fundamentals of Operation
  39
- Touch-Sensitive Screen
  39
- Display Elements and Controls
  40
- Status Display
  41
- Entering Text and Numbers
  42
7 Maintenance

44

Metrohm 917 Coulometer Manual - Short Instructions (35 pages)

Coulometer

Brand: Metrohm | Category: Laboratory Equipment | Size: 2 MB

Table of Contents
5
1 About These Short Instructions

9
2 Introduction

10
- Instrument Description
  10
- Titration and Measuring Modes
  10
- Connectors
  11
- Intended Use
  11
- About the Documentation
  11
- Symbols and Conventions
  12
3 Safety Instructions

13
- General Notes on Safety
  13
- Electrical Safety
  13
- Tubing and Capillary Connections
  14
- Flammable Solvents and Chemicals
  14
- Recycling and Disposal
  15
4 Overview of the Instrument

16
- Front
  16
- Rear
  17
5 Installation

18
6 Technical Specifications

30
- Touch Screen
  30
- Measuring Inputs
  31
- Generator Electrode
  31
- Indicator Electrode
  31
- Temperature Sensor
  31
- Determination Range
  32
- Resolution
  32
- Reproducibility
  32
- Internal Stirrer
  32
- Interfaces and Connectors
  32
- Power Supply
  33
- Safety Specifications
  33
- Electromagnetic Compatibility (EMC)
  33
- Ambient Temperature
  34
- Reference Conditions
  34
- Dimensions
  34
Index

35

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Metrohm 917 Coulometer Manuals

Metrohm 917 Coulometer Manual (338 pages)

Table of Contents

1 Introduction

2 Safety Instructions

3 Overview of the Instrument

4 Installation

5 Titrations

6 Operation

7 System Settings

8 Reagents

9 Sensors

10 Device Manager

11 File Manager

12 GLP Manager

13 Common Variables

14 Templates

15 Methods

16 Electronic Signatures

17 Control

18 Favorites

19 Sample Data

20 Sample Table

21 Determination Run

22 Live Modifications

23 Results and more Determination Data

24 Statistics

25 Result Table

26 Printing

27 Manual Control

28 Parameter

29 Operation and Maintenance

30 Troubleshooting

31 Appendix

32 Technical Specifications

33 Accessories

Index

Metrohm 917 Coulometer Tutorial (67 pages)

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Metrohm 917 Coulometer Manual - Short Instructions (45 pages)

Table of Contents

1 About These Short Instructions

2 Introduction

3 Safety Instructions

4 Overview of the Instrument

5 Installation

6 Operation

7 Maintenance

Metrohm 917 Coulometer Manual - Short Instructions (35 pages)

Table of Contents

1 About These Short Instructions

2 Introduction

3 Safety Instructions

4 Overview of the Instrument

5 Installation

6 Technical Specifications

Index

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