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940 Professional IC Vario ONE/SeS/Prep 1
Metrohm 940 Professional IC Vario ONE/SeS/Prep 1 Manuals
Manuals and User Guides for Metrohm 940 Professional IC Vario ONE/SeS/Prep 1. We have
1
Metrohm 940 Professional IC Vario ONE/SeS/Prep 1 manual available for free PDF download: Manual
Metrohm 940 Professional IC Vario ONE/SeS/Prep 1 Manual (126 pages)
Brand:
Metrohm
| Category:
Laboratory Equipment
| Size: 9 MB
Table of Contents
Table of Contents
5
Introduction
11
Instrument Description
11
Intended Use
13
Safety Instructions
14
General Notes on Safety
14
Electrical Safety
14
Tubing and Capillary Connections
15
Flammable Solvents and Chemicals
15
Recycling and Disposal
15
Symbols and Conventions
16
Overview of the Instrument
17
Front
17
Figure 1 Front
17
Rear
19
Figure 2 Rear
19
Feed-Throughs for Capillaries and Cables
20
Figure 3 Feed-Throughs on the Door
21
Figure 4 Openings for Capillaries and Cables
22
Figure 5 Ducts for Capillaries
23
Installation
24
Setting up the Instrument
24
Packaging
24
Checks
24
Location
24
Capillary Connections in the IC System
24
Removing the Handle
27
Removing Transport Locking Screws
28
Figure 6 Removing the Transport Locking Screws
28
Connecting the Drainage Tubing and Leak Sensor
29
Installing the Drainage Tubing
29
Connecting the Leak Sensor
31
Column Thermostat
31
Connecting the Eluent Bottle
32
Figure 7 Installing the Eluent Bottle Cap
32
Figure 8 Installing Tubing Weighting and Aspiration Filter
34
Connecting the Eluent Degasser
36
Installing the High-Pressure Pump
36
Figure 9 High-Pressure Pump with Purge Valve
36
Installing an Inline Filter
37
Installing the Pulsation Absorber
37
Figure 10 Inline Filter
37
Injection Valve
38
Figure 11 Pulsation Absorber
38
Figure 12 Exchanging the Sample Loop
39
Metrohm Suppressor Module (MSM)
40
Inserting the Rotors
41
Connecting the Metrohm Suppressor Module (MSM)
44
Figure 13 Metrohm Suppressor Module (MSM) - Connection Capillaries
44
Metrohm CO Suppressor (MCS)
48
General Information on the MCS
48
Connecting the MCS
49
Figure 14 Connecting the MCS
49
Installing Adsorption Cartridges
50
Installing the Conductivity Detector
53
Installing the Amperometric Detector
54
Connecting the Sample Degasser (Optional)
54
Peristaltic Pump
56
Installing the Peristaltic Pump
56
Figure 15 Peristaltic Pump
56
Mode of Operation for the Peristaltic Pump
60
Connecting the Instrument to a Computer
61
Connecting the Instrument to the Power Grid
62
Initial Start-Up
63
Connecting and Rinsing the Guard Column
65
Connecting the Separation Column
67
Conditioning
71
Operation
73
Operation and Maintenance
74
IC System
74
Operation
74
Care
74
Maintenance by Metrohm Service
74
Shutting down and Recommissioning
75
Capillary Connections
76
Servicing the Door
76
Column Thermostat - Replacing the Capillaries
76
Figure 16 Column Thermostat
77
Handling the Eluent
78
Manufacturing Eluent
78
Changing the Eluent
79
Servicing the Eluent Degasser
79
Notes on Operating the High-Pressure Pump
80
Servicing the High-Pressure Pump
81
Figure 17 High-Pressure Pump - Parts
81
Figure 18 High-Pressure Pump - Cross-Section
88
Figure 19 Tool for Piston Seal (6.2617.010)
89
Figure 20 Removing the Piston Cartridge from the Pump Head
89
Figure 21 Inserting the Piston Seal into the Tool
90
Figure 22 Parts of the Piston Cartridge
91
Servicing the Inline Filter
94
Figure 23 Inline Filter - Removing the Filter
95
Servicing the Pulsation Absorber
97
Injection Valve
97
Metrohm Suppressor Module (MSM)
97
Notes for Operating the Metrohm Suppressor Module (MSM)
97
Taking Care of the Suppressor Housing
98
Servicing the Metrohm Suppressor Module (MSM)
98
Figure 24 Parts of the Metrohm Suppressor Module (MSM)
98
Servicing the Metrohm CO 2 Suppressor (MCS)
106
Replacing the CO 2 Adsorption Cartridge CW
106
Servicing the Detector
107
Rinsing the Sample Path
107
Peristaltic Pump
108
Notes on Operating the Peristaltic Pump
108
Servicing the Peristaltic Pump
109
Separation Column
110
Separating Efficiency
110
Figure 25 Pump Tubing Connection - Replacing the Filter
110
Protecting the Separation Column
111
Storing the Separation Column
111
Regenerating the Separation Column
111
Quality Management and Qualification with Metrohm
112
Troubleshooting
113
Technical Specifications
118
Reference Conditions
118
Instrument
118
Ambient Conditions
118
Housing
119
Weight
119
Leak Sensor
119
Column Thermostat
119
Eluent Degasser
120
High-Pressure Pump
120
Injection Valve
121
Metrohm Suppressor Module (MSM)
121
Metrohm CO
121
Detector
122
Sample Degasser
122
Peristaltic Pump
122
Power Connection
122
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