PEAK INSTRUMENTS C-7000 Series Operating Manual

PEAK INSTRUMENTS C-7000 Series Operating Manual

Spectrophotometer
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C-7000 Series User Manual
PEAK INSTRUMENTS INC.
C-7000 Series Spectrophotometer
Operating Manual and Maintenance Guide
PEAK INSTRUMENTS INC.
Version 1701

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Summary of Contents for PEAK INSTRUMENTS C-7000 Series

  • Page 1 C-7000 Series User Manual PEAK INSTRUMENTS INC. C-7000 Series Spectrophotometer Operating Manual and Maintenance Guide PEAK INSTRUMENTS INC. Version 1701...
  • Page 2: Table Of Contents

    C-7000 Series User Manual PEAK INSTRUMENTS INC. CONTENTS Spectrophotometer Overview ..........................1 1. Basic Operating Principle ............................1 2. Performance Indicator Definitions ...........................3 3. Application ................................4 4. Using conditions ...............................4 II. Product Features and Installation ........................5 1. Features ..................................5 2. Performance Indicators ............................6 3.
  • Page 3 C-7000 Series User Manual PEAK INSTRUMENTS INC. VII. Time Scan (Kinetics)……………………………………………………………………………………………………………….………………………..…20 1. Function description ..............................20 2. Time scanning parameters set ..........................20 3. Data test .................................21 4. Data list ..................................21 5. Slope calculation..............................22 VIII. Multi-wavelength Test ............................22 1. Function description ...............................22 2.
  • Page 4: Spectrophotometer Overview

    C-7000 Series User Manual PEAK INSTRUMENTS INC. I. Spectrophotometer Overview 1. Basic Operating Principle 1) The nature of absorption: spectrophotometric analysis method is the use of substances to choose a different wavelength of light absorption characteristics established. Typically using a prism or grating to obtain monochromatic light that passes through the continuous monochromatic solution, the solution was measured and the absorption of each wavelength, the absorption spectrum curve obtained.
  • Page 5 C-7000 Series User Manual PEAK INSTRUMENTS INC. monochromatic, at low concentrations, curve remains linear, but larger concentrations, with concentration increases, AC curve bend more serious, there is Beer's law applies only to dilute solutions F. Stray light, stray light entering the detector means is unnecessary components to be tested at other wavelengths outside the range of the wavelength spectral bandwidth.
  • Page 6: Performance Indicator Definitions

    C-7000 Series User Manual PEAK INSTRUMENTS INC. 2. Performance Indicators Definitions 1) Optical system: usually refers to the formal structure of the optical system, at present, domestic and international institutions often used as a photometer industry type and CT auto collimation two structures;...
  • Page 7: Application

    C-7000 Series User Manual PEAK INSTRUMENTS INC. 6) Stray light: wavelength of stray light is irradiated onto the non-selection signal generated by the detector. It is an important source of photometric analysis of errors, stray light limit the accuracy of the General Assembly high concentration solution analysis.
  • Page 8: Product Features And Installation

    C-7000 Series User Manual PEAK INSTRUMENTS INC. vibrations; nearby fan of the instrument should be left enough space to exhaust smoothly. Instrument is best to use a single power outlet, power should ensure good grounding. Doing so may result in equipment not working properly.
  • Page 9: Performance Indicators

    C-7000 Series User Manual PEAK INSTRUMENTS INC. 2. Performance Indicator Model C-7000V C-7000UV Screen 7-inch TFT screen. Wavelength 320 - 1100nm 190 - 1100nm Range Slit Width Wavelength ±0.3nm ±0.3nm Accuracy Wavelength ≤0.2nm ≤0.2nm Repeatability Photometric 0.3%T (0-100%T) , ±0.002A(0-0.5A) , ±0.004A(0.5-1A)
  • Page 10: Main Functions

    C-7000 Series User Manual PEAK INSTRUMENTS INC. 3. Main Functions...
  • Page 11: Structure Introduction

    C-7000 Series User Manual PEAK INSTRUMENTS INC. 4. Structure Introduction Overall structure consists of three parts: optical system, power system and micro-computer system. 1) Top view: 2) Bottom view:...
  • Page 12 C-7000 Series User Manual PEAK INSTRUMENTS INC. 3) Light Path Diagram 4) Important part of the instrument A. Power Board: The 220V50Hz/110V60Hz power conversion and regulation outside access to the necessary equipment:-11.5V (tungsten lamp power), +12 V (fan power, electrical power), +5 V (computer system power), + /- 15V (signal board power supply), deuterium lamp filament preheating and lit power deuterium lamp is lit up and the power breakdown.
  • Page 13: Instrument Installation

    C-7000 Series User Manual PEAK INSTRUMENTS INC. calibration curve, the slit is too small, flux decreased, reducing the signal to noise ratio, affect the measurement accuracy, the slits there are two general representation of the width, the actual width of the slit of a knife-edge between the two expressed (in mm), the other to represent the bandwidth of spectral bands (in nm).
  • Page 14: Key Definitions And Basic Operation

    C-7000 Series User Manual PEAK INSTRUMENTS INC. III. Key Definitions and Basic Operation 1. Button panel schematic diagram 2. Button function description Button name Button functional description Menu key under each function 【MENU】 Print output button 【PRINT】 File storage button 【SAVE】...
  • Page 15: Basic Operation

    C-7000 Series User Manual PEAK INSTRUMENTS INC. 3. Basic operation 1) How to adjust the blank In any test interface, put the cuvette containing the reference solution into cuvette slot, and pull it into light path., press 【Zero】 key to adjust the blank.
  • Page 16: Printer Check

    C-7000 Series User Manual PEAK INSTRUMENTS INC. 5. Printer check Check the printer interface device is working properly. The result is displayed correctly √, an error is displayed result is ×, the buzzer alarm. 6. Tungsten lamp examination Open the instrument tungsten light source, check the operating parameters of tungsten lights are working properly.
  • Page 17: Photometric Measurement

    C-7000 Series User Manual PEAK INSTRUMENTS INC. Note: After power on the instrument, the instrument will automatically self-test and initialization until after initialization is complete, the instrument will warm up for 20 minutes, 20 minutes warm-up time or press [ESC] to skip preheating case, the instrument being prompted preparatory work environment, which is the instrument re- calibration dark current, set the working parameters, etc., and then enter the main menu.
  • Page 18: Set Wavelength

    C-7000 Series User Manual PEAK INSTRUMENTS INC. 3. Set wavelength Set the current working wavelength range 190nm-1100nm, press the up and down button to open wavelength setting window, press [0] - [9] to enter the desired wavelength, press [CLEAR] to clear the input, press [ENTER] to confirm.
  • Page 19: Delete Data

    C-7000 Series User Manual PEAK INSTRUMENTS INC. 6. Delete data Delete files Press [CLEAR] button, delete files prompt box will pop up, this operation will delete all the test data currently under test. Select [Yes], the file will be deleted all the data, select [No] will return the test window.
  • Page 20: Open The File

    C-7000 Series User Manual PEAK INSTRUMENTS INC. 8. Open the file In photometric measurement interface will be displayed by the Load button to open the window, open the window has all the photometric data file list. Select the appropriate data file and press [ENTER], the file will be read into all the test data, and then automatically enters the measurement mode.
  • Page 21: Set Parameter

    C-7000 Series User Manual PEAK INSTRUMENTS INC. 1. Build standard curve To use several configured standard samples, input the concentration of sample standard, collect the absorbance of standard sample, through the relationship between concentration and absorbance is calculated curve parameters, use this parameter to measure the concentration of the sample.
  • Page 22: Sample Measurement

    C-7000 Series User Manual PEAK INSTRUMENTS INC. Put various standard samples into cuvette holder orderly, and enter the concentration value of each sample, then press [enter] key, read the absorbance of the sample. The input is completed, the data of the standard sample is calculated automatically according to the parameters of the curve, displayed on the screen.
  • Page 23: Time Scan (Kinetics)

    C-7000 Series User Manual PEAK INSTRUMENTS INC. VII. Time Scan (Kinetic) 1. Function description Scan time (kinetic) function is a fixed time interval to the trend in absorbance or transmittance of the test current, and displayed on the map. Select time scanning (kinetic) menu option press [ENTER].
  • Page 24: Data Test

    C-7000 Series User Manual PEAK INSTRUMENTS INC. 3. Data test Press [START] to start measuring. the current real-time map will be on the screen. 4. Data list Press [Menu] key to check the scanning data after scanning finish.
  • Page 25: Slope Calculation

    C-7000 Series User Manual PEAK INSTRUMENTS INC. Slope calculation After scanning, press [Menu] key to set starting time and end time for slope calculate. VIII. Multi-Wavelength Test 1. Function description Multi-wavelength for the user is needed to test a sample while measuring the transmittance or absorbance at a wavelength setting of several functions, the user interface can be placed in this first sample obtained values for several wavelengths simultaneously, thus simplifying user operation processes.
  • Page 26: Set Parameter

    C-7000 Series User Manual PEAK INSTRUMENTS INC. 2. Set parameter 1) Set the number of wavelength measurement When you select a multi-wavelength test capability will be prompted to enter the number of the instrument wavelength. 2) Set test wavelength After setting the number of wavelengths measuring wavelength will enter the setup interface, this interface input wavelength values of all measured using the number keys, lost a good point [ENTER] after confirming then lose the next one, until all shall be measured wavelengths losers.
  • Page 27: System Setup

    C-7000 Series User Manual PEAK INSTRUMENTS INC. IX. System Setup...
  • Page 28: Dark Current Measurements

    C-7000 Series User Manual PEAK INSTRUMENTS INC. 1. Dark current measurements Long time operation of instrument probably lead to drift of dark current. this function can make correction for full range of dark current. Please make sure to cover the sample chamber lid when test dark current.
  • Page 29: Time And Date Settings

    C-7000 Series User Manual PEAK INSTRUMENTS INC. 3. Time and date settings Set the time and date of the instrument, set the year, month, day, hour, minute, second. By the arrow keys to select the year, month, day, hour, minute, second, through the numeric keys currently selected content. Press Enter to confirm your entry, press Esc to abandon input.
  • Page 30: General

    C-7000 Series User Manual PEAK INSTRUMENTS INC. 5. General 6. File system...
  • Page 31: Usb Storage Device

    C-7000 Series User Manual PEAK INSTRUMENTS INC. 7. USB storage device 8. Restore factory settings This operation will restore all system configuration information, this operation does not affect the system baseline and data files.
  • Page 32: System Information

    C-7000 Series User Manual PEAK INSTRUMENTS INC. 9. System information You can view software version and hardware version information. X. Instrument Care and Maintenance 1. Routine precautions Any instrument is concerned, the correct use is the best safeguard for equipment maintenance, with emphasis on...
  • Page 33: Instrument Care And Maintenance

    C-7000 Series User Manual PEAK INSTRUMENTS INC. 2. Instrument Care and Maintenance 1) Check the sample chamber lens: regular checks on both sides of the sample chamber is about bias in quartz lens position, look at whether fingerprints and other stains, if stains serious impact on the accuracy of the measured...
  • Page 34: Self-Test Failure

    C-7000 Series User Manual PEAK INSTRUMENTS INC. 2. Self-test failure Failures Causes Solutions Opening the housing service personnel Loose electrical line filter under the guidance of re-seated Opening the housing service personnel Optocoupler line filter loose under the guidance of re-seated...
  • Page 35: Light Source Replacement

    C-7000 Series User Manual PEAK INSTRUMENTS INC. XII. Light source replacement Note: To make the instrument work, choose to replace original parts! ! ! Device names mentioned in this chapter and its location, please refer to Chapter 2 Section 4 describes where to find the structure.
  • Page 36: Deuterium Lamp Replacement

    C-7000 Series User Manual PEAK INSTRUMENTS INC. 2. Deuterium lamp replacement 1)Turn off the instrument and unplug the power cord and disconnect the equipment on both sides of the four screws fastening the shell and the shell gently remove the left vertical against the instrument. (Note: The...

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