Micromeritics SMART VACPREP Operator's Manual
  1. Manuals
  2. Brands
  3. Micromeritics Manuals
  4. Industrial Equipment
  5. Smart VacPrep
  6. Operator's manual

Micromeritics SMART VACPREP Operator's Manual

Intelligent vacuum sample preparation system
Hide thumbs Also See for SMART VACPREP:
Table of Contents

Advertisement

Quick Links

Download this manual
™
S
V
P
MART
AC
REP
I
V
S
P
S
NTELLIGENT
ACUUM
AMPLE
REPARATION
YSTEM
O
M
PERATOR
ANUAL
067-42801-01
June 2022
(Rev A)

Advertisement

Table of Contents
loading
Need help?

Need help?

Do you have a question about the SMART VACPREP and is the answer not in the manual?

Questions and answers

Related Manuals for Micromeritics SMART VACPREP

Summary of Contents for Micromeritics SMART VACPREP

  • Page 1 ™ MART NTELLIGENT ACUUM AMPLE REPARATION YSTEM PERATOR ANUAL 067-42801-01 June 2022 (Rev A)
  • Page 2 Copyright The software described in this manual is furnished under a license agreement and may be used or copied only in accordance with the terms of the agreement. ____________________________________________________________________________ Copyright © 2014 - 2022. Micromeritics Instrument Corporation. All rights reserved.
  • Page 3 MICROMERITICS shall not be liable for consequential or other type damages resulting from the use of any of its products other than the liability stated above. This warranty is in lieu of all other warranties, express or implied, including but not limited to, the implied warranties of merchantability or fitness for use.
  • Page 4 The company has R&D and manufacturing sites in the USA, UK, and Spain, and direct sales and service operations throughout the Americas, Europe, and Asia. Micromeritics systems are the instruments-of-choice in more than 10,000 laboratories of the world’s most innovative companies and prestigious government and academic institutions.
  • Page 5 4356 Communications Drive Norcross, GA / USA / 30093-2901 Phone: 1-770-662-3636 Fax: 1-770-662-3696 www.Micromeritics.com Instrument Service or Repair Phone: 1-770-662-3666 International: Contact your local distributor or call 1-770-662-3666 Service.Helpdesk@Micromeritics.com Micromeritics Application Support Support@Micromeritics.com Smart VacPrep Operator Manual 067-42801-01 (Rev A) — June 2022...

  • Page 6: General Safety

    When inspecting the instrument, ensure that the safety labels have not become worn or damaged. The Smart VacPrep has a safety shield. Ensure it is in place when operating the instrument.
  • Page 7 General Safety NTENDED The Smart VacPrep degasser is an advanced six-port system that utilizes vacuum to prepare samples by heating and evacuation. Each of the ports may be operated independently. Samples may be added or removed from degas ports without disturbing the treatment of other samples undergoing preparation.
  • Page 8 EFUP (for example, battery modules) and are marked to reflect such. The Environmentally Friendly Use Period is valid only when the product is operated under the conditions defined in the product manual. Smart VacPrep Operator Manual 067-42801-01 (Rev A) — June 2022...

  • Page 9: About This Manual

    About this Manual BOUT THIS ANUAL The following can be found on the Micromeritics web page (www.Micromeritics.com). Parts and Accessories Error Messages Vacuum Pump Guide (PDF) The following symbols or icons indicate safety precautions and/or supplemental information and may appear in this manual: NOTE —...

  • Page 11: Table Of Contents

    2 - 10 List Files 2 - 11 Menu Structure 2 - 11 Smart VacPrep Configuration 2 - 12 Add or Remove a Smart VacPrep 2 - 13 Unit Selection 2 - 14 Software Setup 2 - 14 Software Uninstall...
  • Page 12 6 - 8 Sample Tube for HPVA 6 - 10 Remove the Smart VacPrep Sample Port Fitting 6 - 10 Attach an HPVA Sample Tube to the Smart VacPrep 6 - 11 Smart VacPrep Fuse 6 - 11 7 Data Logging...

  • Page 13: About The Smart Vacprep

    The degas program may be started or terminated by using software installed on the computer attached to the analysis instrument or with buttons on the front panel of the Smart VacPrep. The Rapid-Start mode on each port allows the operator to attach the sample tube with heating mantle and immediately start degassing a sample.
  • Page 14 1 About the Smart VacPrep Smart VacPrep Components Description Component Located on the left side panel. Use to connect an Ethernet switch. Ethernet port (not shown) Covers the bottom of the sample tube while degassing is in process. Heating Mantles Located on the back of the unit. Powers the unit on or off.

  • Page 15: Specifications For The Smart Vacprep

    Specifications for the Smart VacPrep PECIFICATIONS FOR THE MART Backfill Options Automatic Capacity 6 ports Degas Method Heat and vacuum Determined by selected elapsed time after achievement of selec- Evacuation Period ted low pressure target Evacuation Rate Selectable evacuation rate from 1.0 to 50.0 mmHg/s...
  • Page 16 1 About the Smart VacPrep Environment 10 to 35 ºC operating; 0 to 50 ºC non-operating Temperature Maximum rate of change of 2 °C per hour Humidity 20 to 80% relative, non-condensing Indoor only (not suitable for wet locations) Indoor or Outdoor Use...
  • Page 17 Specifications for the Smart VacPrep Computer Requirements Operating System Windows 10 or higher operating system is required. The application should not be installed on a network drive with shared access. Multiple users cannot operate the application at the same time.

  • Page 18: Check Seal And Transeal

    1/2 in. and 12 mm sample tubes. Instructions for using the Check Seal or TranSeal are included with the ordered part. The Smart VacPrep is shipped from the factory with Check Seal openers installed inside each sample tube port.

  • Page 19: About The Software

    BOUT THE OFTWARE The Smart VacPrep software is installed as a part of the analyzer installation or it can be installed as a standalone unit. During installation, an IP address will be assigned to the unit allowing the unit to connect automatically during startup. Up to three additional degasser units can be installed when running Micromeritics analyzer analysis software.

  • Page 20: Export Files

    1. Select a .DEG file to be exported. 2. Click Export and select export preferences. Smart VacPrep Operator Manual 2 - 2 067-42801-01 (Rev A) — June 2022...

  • Page 21: Instrument Status

    When the displayed value is 30 or less, the value is displayed in red. Red negative numbers display if maintenance is past due. Smart VacPrep Operator Manual 2 - 3 067-42801-01 (Rev A) — June 2022...
  • Page 22 At 110% and above, only the red LED is lit and attention is required. Smart VacPrep fields and buttons not listed in this table; see Common Fields and Buttons on page 2 - Smart VacPrep Operator Manual 2 - 4 067-42801-01 (Rev A) — June 2022...

  • Page 23: Show Log

    Select the logs to display. Analysis / Calibration / Message Smart VacPrep fields and buttons not listed in this table; see Common Fields and Buttons on page 2 - Smart VacPrep Operator Manual 2 - 5 067-42801-01 (Rev A) — June 2022...

  • Page 24: Show Schematic

    Selections Open Valve. Green indicates an open valve. Closed Valve. Yellow indicates a closed valve. Servo Valve. Closed. Servo Valve. Open. Sample Tube. Cannot be manually controlled. Smart VacPrep Operator Manual 2 - 6 067-42801-01 (Rev A) — June 2022...
  • Page 25 Set. Select to set the following: Enable or disable temperature control Control sample temperature Control furnace temperature Cool the sample to less than 50 °C Set heater power percent Smart VacPrep Operator Manual 2 - 7 067-42801-01 (Rev A) — June 2022...

  • Page 26: Show Status

    Skips the current degas operation. Skip Indicates the current status of the degas. Status Smart VacPrep fields and buttons not listed in this table; see Common Fields and Buttons on page 2 - Smart VacPrep Operator Manual 2 - 8 067-42801-01 (Rev A) — June 2022...

  • Page 27: Keyboard Shortcuts

    Ctrl + S Opens the online help operator manual. Opens the File Selector window. Cascades open windows. Tiles all open application windows. Opens the File List window. Shift + F2 Smart VacPrep Operator Manual 2 - 9 067-42801-01 (Rev A) — June 2022...

  • Page 28: Libraries

    However, when deleting files or folders from within a library, they are deleted from their original file storage location. Deleted files and folders can be recovered from the Recycle Bin located on the Windows desktop. Smart VacPrep Operator Manual 2 - 10 067-42801-01 (Rev A) — June 2022...

  • Page 29: List Files

    Use to manage open windows and display a list of open windows. A Window checkmark appears to the left of the active window. Provides access to the embedded operator manual, the Micromeritics web Help page (www.Micromeritics.com), and information about the application.

  • Page 30: Smart Vacprep Configuration

    2 About the Software MART ONFIGURATION Prep [n] > Configuration Displays the Smart VacPrep configuration and software versions. Unit Configuration Description Selections Click to display the board ID. This button is disabled if the instrument Board ID [button] is busy.

  • Page 31: Add Or Remove A Smart Vacprep

    DD OR EMOVE A MART A Smart VacPrep unit must be removed from one application before it can be added to another application if they are running on the same subnet. Add a Smart VacPrep File > Add Smart VacPrep 1.

  • Page 32: Unit Selection

    The IP address for the computer and the IP address specified in the setup program must match. The IP address must be 192.168.77.100. Smart VacPrep Operator Manual 2 - 14 067-42801-01 (Rev A) — June 2022...

  • Page 33: Software Uninstall

    Micromeritics application are correctly installed. If UAC is not enabled, right-click the setup.exe installer file and select Run as administrator. The most current version of the instrument software can be found on the Micromeritics web page (www.Micromeritics.com).

  • Page 35: Operate The Smart Vacprep

    The six ports are represented by row numbers. Ports that are busy are grayed out and disabled. 1. Open a .SMP or .DEG file for each Smart VacPrep port to be used. If using the Check Seal, see the instructions included with the Check Seal [part number 350-42802-00].

  • Page 36: Evacuate Ports

    3 Operate the Smart VacPrep Degas ports can also be canceled using buttons on the Smart VacPrep unit. Press Select on the unit to select the port, then press the Cancel button. VACUATE ORTS Prep [n] > Evacuate Ports Evacuate Ports...

  • Page 37: Backfill Ports

    1. Enter the backfill pressure in the Backfill pressure field. 2. Select the ports to be backfilled. 3. Click Start to start the process or Cancel to stop the process. Smart VacPrep Operator Manual 3 - 3 067-42801-01 (Rev A) — June 2022...

  • Page 38: Quickstart Degas Conditions

    ONDITIONS Prep [n] > QuickStart Degas Conditions Use to enter commonly used degas conditions for each Smart VacPrep port without the need for a sample file. Degassing can then be started using the front panel buttons on the Smart VacPrep unit.
  • Page 39 9. Install the safety shield. 10. Press the Select button for the port to be degassed. A blue LED is lit. 11. Press the Start button on the Smart VacPrep panel to start the degas process for all ports that have a blue LED lit.
  • Page 40 3 Operate the Smart VacPrep UICK TART EGAS ONDITIONS INTO A AMPLE QuickStart Degas Conditions can be copied into a sample file. See the Degas Conditions section of the analyzer operator manual. Degas Conditions Description Selections Use to copy the degas conditions settings from the selected Copy QuickStart Smart VacPrep unit and port.

  • Page 41: Load Quickstart Degas Conditions Into A Sample File

    Vacuum level. Evacuation time starts when the vacuum level is reached. Smart VacPrep fields and buttons not listed in this table; see Common Fields and Buttons on page 2 - Smart VacPrep Operator Manual 3 - 7 067-42801-01 (Rev A) — June 2022...

  • Page 43: Calibration

    Use to perform system calibration. This option evacuates the system and zeros the pressure transducer. Disabled calibration options can be accessed only with the assistance of an authorized Micromeritics Service Representative. Click Start to begin the process. Smart VacPrep Operator Manual 4 - 1 067-42801-01 (Rev A) — June 2022...

  • Page 44: Servo Valve

    The pressure transducer should be calibrated before starting this calibration procedure. Click Start. The window closes when the calibration is complete. Click Cancel to stop the calibration process. Smart VacPrep Operator Manual 4 - 2 067-42801-01 (Rev A) — June 2022...

  • Page 45: Diagnostics

    Displays previously run diagnostic service tests. Separate directories store tests run once, daily, weekly, and monthly. Diagnostic test report files have a .SVT file extension and are stored in the ...\Service directory. Smart VacPrep Operator Manual 5 - 1 067-42801-01 (Rev A) — June 2022...

  • Page 47: Maintenance

    Safe operation and handling of the instrument, supplies, and accessories is the responsibility of the operator. Do not modify this instrument without the authorization of a Micromeritics service per- sonnel. When lifting or relocating the instrument, use proper lifting and transporting devices for heavy instruments.

  • Page 48: Safe Servicing

    Contact your Micromeritics Service Representative. ERVICING Do not modify this instrument without the authorization of a Micromeritics service per- sonnel. To ensure safe servicing and continued safety of the instrument after servicing, service personnel...

  • Page 49: Parts And Accessories

    The Vacuum Pump Guide can be found on the Micromeritics web page (www.Micromeritics.com). OWER The Smart VacPrep is designed to operate with line voltage of 100/120/230/240VAC ±10, 50/60 Hz through a standard wall receptacle. Noise-free power of the correct voltage and frequency, with a safety earth ground, should be available through a standard wall receptacle.

  • Page 50: Preventive Maintenance

    AINTENANCE Perform the following preventive maintenance procedures to keep the analyzer operating at peak performance. Micromeritics also recommends that preventive maintenance procedures and calibration be performed by a Micromeritics Service Representative every 12 months. Frequency Maintenance Required Clean a needed or every 6 months.

  • Page 51: Guidelines For Connecting Gases

    500 psi (3500 kPa) on the high-pressure gauge. Contaminants absorbed to the walls of the cylinder will desorb as the pressure decreases. Ensure the gas cylinder is closed before connecting to the analyzer. Smart VacPrep Operator Manual 6 - 5 067-42801-01 (Rev A) — June 2022...

  • Page 52: Replace A Gas Cylinder

    6. Use an appropriate wrench to loosen the nut at the regulator connector nut then remove the regulator from the cylinder. 7. Replace the protective cap on the depleted cylinder. Disconnect the retaining strap and move the cylinder to an appropriate location. Smart VacPrep Operator Manual 6 - 6 067-42801-01 (Rev A) — June 2022...
  • Page 53 Gauge should indicate Analyzer 10 - 15 psig (69 - 103 kPag) Smart VacPrep Exceeding the maximum recommended air pressure could cause personal injury or damage the instrument. Smart VacPrep Operator Manual 6 - 7 067-42801-01 (Rev A) — June 2022...

  • Page 54: Sample Tube Installation

    Sample Tube for HPVA on page 6 - 10 for instruc- tions on converting the Smart VacPrep to accommodate the HPVA sample tubes. 1. While holding the degas port plug, turn the connector nut counter-clockwise to loosen. Remove both the plug and the nut.
  • Page 55 9. After installing the sample tubes, install the safety shield around the sample tubes and heat- ing mantles to minimize the risk of receiving a burn by touching hot components. Smart VacPrep Operator Manual 6 - 9 067-42801-01 (Rev A) — June 2022...

  • Page 56: Sample Tube For Hpva

    AMPLE ITTING 1. Use a 3/4 in. open-end wrench to turn the Smart VacPrep degas port connector nut counter- clockwise. Remove the Smart VacPrep port adapter and store for future use. 2. Remove the two plastic end protective covers from the VCO to ASAP adapter [part number: P02-25874-00].

  • Page 57: Attach An Hpva Sample Tube To The Smart Vacprep

    3. Place a Seal Frit in the long end of the VCO adapter. 4. Insert the long end of the Fitting VCO adapter into the Smart VacPrep degas port. Hand tighten the connector nut by turning the adapter clockwise. Tighten again with a 3/4 in.

  • Page 59: Data Logging

    7 Data Logging OGGING The Smart VacPrep has the added capability to collect real time transient data (pressure, vacuum level, time, and temperatures) during sample degas when connected to the Flex analyzer or ASAP 2020 analyzer. This document provides: installation instructions for the PuTTY client and outlines how to access and use the data file, installation instructions for Python components and outlines how the captured data can be handled using Python scripts.
  • Page 60 The PuTTY application can be started before the analyzer starts collecting data — it will be waiting until data output from the analyzer begins. Smart VacPrep Operator Manual 7 - 2 067-42801-01 (Rev A) — June 2022...

  • Page 61: Data File Column Descriptions

    D. 'port 1 temperature (C)'; E. 'port 2 temperature (C)'; F. 'port 3 temperature (C)'; G. 'port 4 temperature (C)'; H. 'port 5 temperature (C)'; I. 'port 6 temperature (C)'; Smart VacPrep Operator Manual 7 - 3 067-42801-01 (Rev A) — June 2022...

  • Page 62: Install Python Components

    Python. 3. Install MatPlotLIB (for graphical display of the data) Download URL: http://www.lfd.uci.edu/~gohlke/pythonlibs/#matplotlib Download file: matplotlib-1.2.1rc1.win32-py3.2.exe MatPlotLIB version 1.2.1 is compatible with NumPY from Step 2. Smart VacPrep Operator Manual 7 - 4 067-42801-01 (Rev A) — June 2022...

  • Page 63: Sample Python Code

    ASCII art created by the PuTTY program, and the second row of data are the column labels — neither of which are numerical data. Smart VacPrep Operator Manual 7 - 5...
  • Page 64 (:) in the fourth column. plt.plot(x,y,'ko') plt.ylabel('Pressure (Torr)') plt.xlabel('time (minutes)') plt.show() The above code shows the syntax for plotting. The label 'ko' indicates filled black circles. Smart VacPrep Operator Manual 7 - 6 067-42801-01 (Rev A) — June 2022...

Table of Contents