Digital Data Systems (Pty) Ltd. CAL3K Advanced Bomb Calorimeters www.ddscalorimeters.com Table of Contents: 1 INTRODUCTION ........................1 PURPOSE OF THIS MANUAL ................1 HOW TO USE THIS MANUAL ................1 1.2.1 WARNING SYMBOL .................. 1 1.2.2 INFORMATION (NOTE) SYMBOL ..............1 2 USER INFORMATION AND HELP AIDS ..................
Digital Data Systems (Pty) Ltd. CAL3K Advanced Bomb Calorimeters www.ddscalorimeters.com INTRODUCTION Digital Data Systems (Pty) Ltd (dds) specializes in the design and manufacture of scientific bomb calorimeter systems for various types of industries and applications from the coal mining industry to educational institutes.
Digital Data Systems (Pty) Ltd. CAL3K Advanced Bomb Calorimeters www.ddscalorimeters.com SYSTEM COMPONENTS THE CAL3K-F SYSTEM CHECK LIST The system consists of the following: Received 3K-F CAL3K-F Calorimeter 3K-MAN-KT CAL3K-F Calorimeter Installation Kit Included in Kit: 3K-1-055 3K External 12V/1.5A Power Supply 3K-1-117 Balance Cable 3K-1-084...
Digital Data Systems (Pty) Ltd. CAL3K Advanced Bomb Calorimeters www.ddscalorimeters.com THE 3K-F CALORIMETER WITH EXTERNAL OXYGEN FILLING The CAL3K-F uses the Dynamic method (Isothermal) of determination while still using the DRY method. The prepared vessel is filled with oxygen in the external filling station and placed in the calorimeter and the lid is closed.
Digital Data Systems (Pty) Ltd. CAL3K Advanced Bomb Calorimeters www.ddscalorimeters.com THE 3K-5 BAYONET VESSEL The ignition and burning process is contained within a chamber so that the energy released can be measured in the form of heat. The Vessel has temperature sensors built into it, so that the temperature rise can be measured.
Digital Data Systems (Pty) Ltd. CAL3K Advanced Bomb Calorimeters www.ddscalorimeters.com INSTALLATION UNPACKING AND INSPECTION There are no special precautions to be taken when unpacking your system. The following check list is for your convenience: Locate and tick-off the various system components as indicated on the CAL3K-F Check List as per above.
Digital Data Systems (Pty) Ltd. CAL3K Advanced Bomb Calorimeters www.ddscalorimeters.com SETTING UP 4.2.1 PREREQUISITES Prior to installation of the CAL3K-F System, the User must provide the following: A mains outlet for the 3K-F Calorimeter and a mains outlet for the 3K-2 Air Cooler power supplies. A supply of oxygen at a pressure of 3.0Mpa (30bars) (3000Kpa) within 4 meters of the 3K-F Calorimeter.
Digital Data Systems (Pty) Ltd. CAL3K Advanced Bomb Calorimeters www.ddscalorimeters.com 4.2.3 ASSEMBLING THE CAL3K-F The unit is shipped with a set of spares and some items required for operation. The operational items need to be assembled before the unit is operational. The reason we ship the lid unlatched is due to customs purposes.
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Digital Data Systems (Pty) Ltd. CAL3K Advanced Bomb Calorimeters www.ddscalorimeters.com 2. The Lid stop will also need to be fitted to the back panel of the calorimeter. a. First unscrew the back panel as shown in the picture below. b. Fit the Lid Stop onto the back panel as shown in the picture below using the screws supplied.
Digital Data Systems (Pty) Ltd. CAL3K Advanced Bomb Calorimeters www.ddscalorimeters.com SAFETY PRECAUTIONS CALORIMETER (3K-F) • Connect the safety earth to the EARTH STUD on the back of the instrument. This is required when the external power supply fails • Do not open the CAL3K for any reason whatsoever! There are no serviceable parts inside the unit.
Digital Data Systems (Pty) Ltd. CAL3K Advanced Bomb Calorimeters www.ddscalorimeters.com • NOTE: With some applications you may need to fill the Vessel to less than 3000KPA e.g. 1500KPA (15 bar), however this is only applicable when you have a sample which is highly combustible, for example with wood related samples.
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Digital Data Systems (Pty) Ltd. CAL3K Advanced Bomb Calorimeters www.ddscalorimeters.com A SUITABLE INSPECTION WARNING PERIOD OF 2000 FIRINGS, AND A STOP OPERATING LIMIT OF • 2500 FIRINGS ARE PRE-PROGRAMMED FROM THE FACTORY THE VESSEL MUST BE INSPECTED AT REGULAR INTERVALS DEPENDING ON THE USE. A SUITABLE INSPECTION PERIOD CAN BE SET (By your agent!) AND THE UNIT WILL ISSUE AN INSPECTION WARNING AND SOON AFTER THIS IT WILL SHUT-DOWN THE OPERATION.
Digital Data Systems (Pty) Ltd. CAL3K Advanced Bomb Calorimeters www.ddscalorimeters.com DAILY SAFETY STEPS The 3K-5 vessel is a high-pressure apparatus, and should be treated with care. • Handle the vessel over a table or solid surface. • Do not drop a vessel. •...
Digital Data Systems (Pty) Ltd. CAL3K Advanced Bomb Calorimeters www.ddscalorimeters.com WARRANTY – FOR NEW PRODUCTS PURPOSE OF PRODUCT WARRANTY Any part of a product is subject to ageing and eventual failure. These failures occur during normal use. The purpose of a warranty is to protect the Owner against a part failure caused by manufacturing defects in workmanship, material or design for a specific time.
Digital Data Systems (Pty) Ltd. CAL3K Advanced Bomb Calorimeters www.ddscalorimeters.com WARRANTY – REPAIRED PRODUCTS Any “dds” scientific product that has been repaired has a warranty period of 30 Days from date of shipment for the Repair request only. If something else goes wrong that is not part of the original Repair, the warranty does not apply.