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3K-F
INSTALLATION GUIDE
VERSION NO: 6
DATE: 2023
MANUFACTURED BY:

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Summary of Contents for DDS Calorimeters CAL3K-F

  • Page 1 3K-F INSTALLATION GUIDE VERSION NO: 6 DATE: 2023 MANUFACTURED BY:...
  • Page 2: Table Of Contents

    INFORMATION (NOTE) SYMBOL .............. 1 USER INFORMATION AND HELP AIDS ................... 1 SYSTEM COMPONENTS ......................2 THE CAL3K-F SYSTEM CHECK LIST ..............2 THE 3K-F CALORIMETER WITH EXTERNAL OXYGEN FILLING ......3 THE 3K-2 AIR COOLER ................. 3 THE 4K-4 THREAD VESSEL ................4 THE 3K-3 OXYGEN FILLING STATION .............
  • Page 3: Introduction

    PURPOSE OF THIS MANUAL It serves as a short introduction to the CAL3K-F system and the various components. It explains the very basics of operation and guides you to perform hardware tests and do the first determination. It relies on the DEFAULT setting and the factory calibration.
  • Page 4: System Components

    Digital Data Systems (Pty) Ltd. CAL3K Advanced Bomb Calorimeters www.ddscalorimeters.com SYSTEM COMPONENTS THE CAL3K-F SYSTEM CHECK LIST The system consists of the following: Received 3K-F CAL3K-F Calorimeter 3K-MAN-KT CAL3K-F Calorimeter Installation Kit Included in Kit: 3K-1-055 3K External 12V/1.5A Power Supply...
  • Page 5: The 3K-F Calorimeter With External Oxygen Filling

    The air cooler will cool the vessel in approximately 6-8 minutes to the specified setting. The operation of the cooler can be set via the USB port and the CAL3K-F application software or from the CAL3K-F The cooler is factory configured before shipment.
  • Page 6: The 4K-4 Thread Vessel

    The filling speed is adjustable to suit the sample material. Width 220mm Height 450mm Depth 300mm Weight 4.5Kg CAL3K-F Installation Guide V5 2022 Website: www.ddscalorimeters.com...
  • Page 7: Installation

    There are no special precautions to be taken when unpacking your system. The following check list is for your convenience: Locate and tick-off the various system components as indicated on the CAL3K-F Check List as per above. Unpack and inspect all the system components such as the 3K-F Calorimeter, 3K-2 Air Cooler, 3K-3 Filling Station and the 4K-4 THREAD Vessels according to the instructions in the relevant sections in this document.
  • Page 8: Setting Up

    The 3K-F Calorimeter is a desktop unit, which can be installed wherever the laboratory space permits, with two restrictions: The CAL3K-F system, consisting of 3K-F Calorimeter, 3K-2 Air Cooler, should be connected to a mains circuit without heavy inductive or SCR switched equipment. It is safe to have balances or other small electronic apparatuses on the same circuit.
  • Page 9: 4.2.3 Assembling The Cal3K-F

    The reason we ship the lid unlatched is due to customs purposes. If customs officials wish to inspect inside the CAL3k-F calorimeter the lid is locked therefore we must ship with the lid and latches loose so that customs can inspect.
  • Page 10 First unscrew the back panel as shown in the picture below. b. Fit the Lid Stop onto the back panel as shown in the picture below using the screws supplied. c. Fit the back panel back as indicated in the picture below. CAL3K-F Installation Guide V5 2022 Website: www.ddscalorimeters.com...
  • Page 11: Testing

    • Secure the pipe into the quick connector and screw the connector to the pressure regulator side. Secure the pipe nuts to the pressure regulator side, then clamp the ferrule to the high pressure pipe on the gauge block side. CAL3K-F Installation Guide V5 2022 Website:...
  • Page 12: 6.2.1 High Pressure Oxygen

    Should the Oxygen supply be in another room, make sure there is a high pressure shut off valve near the 3K-3 Filling Station installation. COOLER (3K-2) • There are no user serviceable parts inside. CAL3K-F Installation Guide V5 2022 Website: www.ddscalorimeters.com...
  • Page 13: Vessel (4K-4)

    • Do not use any tools to open or close the vessel. If the vessel fails to deflate use the pre-scribed ‘emergency deflate’ procedure as outlined in the CAL3K-F Operations Manual, which uses the 3K-3-18 EMERGENCY DEFLATE tool (3K-3-18).
  • Page 14: Daily Safety Steps

    • Do not use any tools to open or close the vessel. If the vessel fails to deflate use the pre-scribed ‘emergency deflate’ procedure as outlined in the CAL3K-F Operations Manual. • Use the provided De-filler cap only, part number: 3K-3-22.
  • Page 15: Warranty - For New Products

    User. The manufacturer is not responsible for any damages, consequential, indirect or direct, or loss whatsoever, resulting out of electrical shock, Vessel explosion, or any other cause. CAL3K-F Installation Guide V5 2022 Website:...
  • Page 16: Warranty - Repaired Products

    All serial numbers on any relevant “dds” Scientific product need to remain on the product at all times, or warranty will be void. Warranty will also be void if any of the branding stickers or decals have been removed and/or the colour of the Scientific product has been changed in any way. CAL3K-F Installation Guide V5 2022 Website:...
  • Page 17: Warranty Registration Form

    NAME (printed): ____________________________ WITNESS: ____________________________ I have read, understood and accepted the conditions of this warranty, the details of which are printed in this Manual. CUSTOMER’S SIGNATURE: __________________________________________________ NAME (printed): __________________________________________________ DATE: ___________________________________________ CAL3K-F Installation Guide V5 2022 Website: www.ddscalorimeters.com...

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