Related Manuals for Sonation DBO-TF-FIS
Summary of Contents for Sonation DBO-TF-FIS
- Page 1 Sonation Sonation lab solutions. lab solutions. DOUBLE BARREL OVEN DBO-TF-FIS Analytics Operators Manual...
- Page 2 CE Declaration of Conformity CE Déclaration de Conformité CE Dichiarazione di Conformità Der Hersteller / The manufacturer / Le fabricant / Il fabbricante Sonation GmbH Alte Schulstr. 39 – 88400 Biberach - Deutschland erklärt hiermit, dass die Produkte herewith declares that the products déclare par la présente que le produits...
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Page 3: Table Of Contents
Column Oven (upper and lower part) ........................6 Regulator ................................6 HV-Switch ................................6 2.2 Scope of delivery ............................... 7 Double Barrel Oven DBO-TF-FIS ..........................7 2.3 Available accessories ..............................7 Mounting Kit for Thermo Fisher Flex Ion Source ES071 ..................7 Mounting Kit for Thermo Fisher Flex Ion Source ES072 ..................7 Micro-Tee with HV-connector ..........................7 HV-cable with 2mm connector.......................... -
Page 4: Safety
Column Oven DBO-TF-FIS User manual 1 Safety 1.1 Important safety instructions Please read these operating instructions carefully before using the product. It contains important notes on Installa- ƒ tion and usage. The user manual is part of the product. Keep it in a safe place. If the product is sold, rented or passed on in any other ƒ way, the user manual must be included. Heed all warnings. These point out dangers and give recommendations for accident prevention. ƒ Only install the unit in locations expressly recommended by the manufacturer. ƒ If condensation forms after unpacking, allow at least 2 hours for the unit to acclimatize. ƒ This device may only be operated at sockets with protective earth. ƒ Make sure that you cannot trip over the mains cable and that the cable is not disconnected, is pinched, torn off or ƒ squeezed. Only use accessories expressly recommended by the manufacturer. ƒ Leave all maintenance work to an experienced service technician. Servicing or repairs are required if there is visible ƒ damage, if the power cord or plug is damaged, if liquid has been spilled inside the apparatus, if the apparatus has been exposed to rain, if it does not perform as expected, or if it has fallen. Only use connection cables or extension cables that are approved for the maximum permissible total current or ƒ... -
Page 5: Who May Use And Operate The Column Oven
User manual Column Oven DBO-TF-FIS Use with damaged supply lines. ƒ Outdoor use. ƒ 1.5 Who may use and operate the column oven Physically and mentally healthy persons who have fully read and understood the instructions for use may use and ƒ operate the column oven as long as they are not affected by medication or drugs. 1.6 Safety signs and symbols Safety symbols on the device and in the user manual The “general mandatory sign” indicates that you should behave attentively. Marked information in this user manual is intended to draw your particular attention. You will receive important information on functions, settings and procedures. Failure to do so may result in malfunction of the equipment or its surroundings. ƒ The “general warning sign” indicates danger points or possible dangerous situations. Marked infor- mation in this user manual applies to your special attention. You will receive important information on safety-relevant matters. Failure to do so may result in personal injury, malfunction of the device or the environment. ƒ The warning sign “Hot surface” indicates a potentially hot surface. Non-observance may cause burns. It is essential that you observe the safety instructions in the operating instructions. ƒ The warning sign “Warning of electrical voltage” indicates potential hazards due to electrical volt- age. The positions on the device marked with this symbol and the information in these operating instructions are intended to draw your particular attention. You will receive important information... -
Page 6: Product Description
Column Oven DBO-TF-FIS User manual 2 Product description 2.1 Overview The double barrel oven DBO-TF-FIS allows the parallel usage of two independant analytical columns. As loading, equil- ibration and washing steps can be alternated, the utilization and throughput of the mass spectrometer can be signifi- cantly increased. Column Oven (upper and lower part) ❶ ❶ ❻ ❻ ❷ ❷ ❸ ❸ ❹ ❹ ❺ ❺ Fig. 1: Column oven (top and bottom part) ❶ ❶ ❷ ❷ ❸ ❸... -
Page 7: Scope Of Delivery
User manual Column Oven DBO-TF-FIS 2.2 Scope of delivery Double Barrel Oven DBO-TF-FIS 1 x Column oven (top and bottom part with 4 column pins) ƒ 1 x Regulator ƒ 1 x HV-switch with 2 x M4x40 mounting screws and 2 x 24mm plastic sleeves ƒ 1 x HV-cable: Source to HV-switch ƒ 1 x Oven control cable: Regulator to oven ƒ 1 x HV control cable: Regulator to HV-switch ƒ... -
Page 8: Hardware
Column Oven DBO-TF-FIS User manual Installation 2.4 Hardware ƒ Before installing the oven make sure the high voltage (spray voltage) has been turned off. The oven can be used with the ES071 and the ES072 version of the Thermo Fisher Flex Ion Source. To be able to use the oven at the respective source, the corresponding mounting kit is required (see „2.3 Available accessories“). Installation of the ES071 mounting kit First the original acrylic safety shield has to be removed. After ƒ removing the two screws on the shield clamp it can be dis- mounted. Also the two camera holders have to be dismounted by remov- ƒ... -
Page 9: Installation Of The Hv-Switch
User manual Column Oven DBO-TF-FIS Fig. 6: Mounting the HV-switch to the source Fig. 7: Attaching the oven to the source Installation of the HV-switch The HV switch has to be attached to the source as shown on Fig. 6. To do so, first remove the original screws from the bottom of the source, then insert the sleves and mount the HV-switch with the provided screws. Attaching the oven to the source Place the mounting bar of the oven onto the XYZ-manipulator and fix it with the provided screw and nut as shown on Fig. 7. If the XYZ-manipulator won’t stay in place, this is due to the weight of the oven. The friction of the manipulator can be regulated with adjusting screws. So just increase the friction until the oven stays in position. Connecting the cables Power supply 24V/200W Flex Ion Regulator Oven Source HPLC HV-OUT1 To column 1... -
Page 10: Software
Column Oven DBO-TF-FIS User manual Connect the two high voltage cables (2 x Sonation P/N PRSO-HV-LE-HI) to the “COL1 OUT” and “COL2 OUT” of the HV ƒ switch. The other ends are connected later to the columns using the micro T-pieces with HV connector. If you use the Thermo liquid junction kit (P/N ES269) the HV cables are already installed to the also included cross pieces. In this case connect them later as discribed in 3.1 „Column loading and applying the HV via liquid junction“ on page 10. Connect the contact closure cable (Thermo P/N 6000.1004) between the HPLC and the “CC HV” input on the regula- ƒ tor. Please see Thermo Fisher tech note 73671 for detailed information. Connect the 24-Volt power supply to the power connector on the regulator. The wide side of the plug faces the top ƒ... -
Page 11: Using Co-Control
User manual Column Oven DBO-TF-FIS Slide the cross holders onto the sliding rails with the columns facing the inlets of the oven. In most cases it works ƒ best to use the lateral and one of the frontal rails. When using the two frontal mounting rails, make sure that the high-voltage connectors point outwards, otherwise there is not enough space to connect the high-voltage cables. Now place the columns inside the oven. Longer columns can be wound around the column pins as needed. Therefor ƒ the column pins can be placed in any of the designated positions. The end of each column is led out at one outlet each and held in position by the clamping mechanism. Place the ƒ columns in a way that the tips are about 5mm apart. Now reinstall the top part of the oven and plug in the power cord from the power supply to a wall outlet. -
Page 12: Maintenance And Care
Column Oven DBO-TF-FIS User manual 4 Maintenance and Care Maintenance The product is basically maintenance-free but not wear-free. If a wear-related defect should occur, please contact your dealer or Sonation directly to clarify the further steps. Cleaning Use a soft, damp cloth to clean the surfaces. Aggressive solvents, bases or acids must not be used for cleaning. 5 Final Disposal Dispose the product in accordance with local and national safety and environmental regulations. The product contains electronic components, cables, metals, plastics, etc. and has to be disposed in accordance with applicable environmental regulations of the respective country. The disposal of the product in Germany is subject to the Elektro-G (RoHS) and in the European area of the EU Directive 2002/95/EC or the respective national legislation. The product can also be returned to the seller for disposal. In this case the cost of transport, including the packaging costs shall be borne by the buyer. Please notify the seller of the return within 14 days before the expected arrival. 6 Technical data Temperature control range Standard range: 15°C - 60°C (59°F - 140°F) Extended range: 15°C - 80°C (59°F - 176°F) Temperature control rate Heating: 30°C to 50°C: Less than 90s Cooling: 50°C to 30°C: Less than 180s... -
Page 13: Faq - Frequently Asked Questions
User manual Column Oven DBO-TF-FIS 7 FAQ - Frequently Asked Questions My PC does not have any COM ports / no available COM ports. Can I run the oven anyhow? Yes. Please use the provided USB to serial converter to install a virtual com-port. I‘ve successfully connected to the oven but can still see no temperature. What is wrong? Please ensure that your oven is closed properly. When the oven is open or even not properly closed, the temperature sensor cannot be read. Is it possible to set up higher temperatures than 60°C or lower temperatures than 15°C? Yes, it is possible. Please ask Sonation for an option code, but remember that the lifetime of the Peltier-elements will be lowered because of the additional thermal stress. The temperature of the oven fluctuates / oscillates some degrees around the setpoint. What’s wrong? The most common cause is that the upper part of the oven sits not properly on the lower part, so the thermal connec- tion is bad. Please check if the column or other things are trapped between the upper and lower part. Page 13... - Page 14 Säulenofen DBO-TF-FIS Originalbetriebsanleitung This page is intentionally left blank Seite 14...
- Page 15 Originalbetriebsanleitung Säulenofen DBO-TF-FIS This page is intentionally left blank Seite 15...
- Page 16 Sonation Sonation Sonation GmbH Tel.: +49 (0) 7351 30038-39 Alte Schulstraße 39 E-Mail: mail@sonation.com lab solutions. lab solutions. D-88400 Biberach www.sonation.com IMPROVE YOUR SCIENCE Rev. 300029_000_00 www.sonation.com 07. Dec. 2020...
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